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Figure 2
The red line is a corrected smoothing spline fit using leave-one-out cross-validation on all temperature difference measurements between the measuring point and the inside of the capillary. Several heating ramps of 0.10, 0.16, 0.25, 0.33 and 0.50°C s−1 as well as heating using maximum power output and a couple of stepped ramps were performed at several capillary positions and thermocouple positions. In orange, the local standard deviation of the measurements.

Journal logoJOURNAL OF
APPLIED
CRYSTALLOGRAPHY
ISSN: 1600-5767
Volume 54| Part 1| February 2021| Pages 371-375
https://doi.org/10.1107/S1600576720014776
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