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Figure 6
Experimental apparatus. (Top) In situ fast-freeze measurements; view is towards the incident X-ray beam, showing the sample capillary, the orientation of the liquid nitrogen (LN2) cryostream and the position sensitive detector (PSD). (Middle) Slow in situ cooling rate cold cell installed in the I11 Long-Duration Experiments facility; view is towards the incident beam direction and shows the large exit window (EW), calibration standard (CS) housing and X-ray flight tube (FT) for when other long-duration cells are being measured. (Bottom) Schematic showing the cold cell's interior sample chamber formed by diamond windows held between o-rings and mounted in a cooled copper block, located within the large insulated housing. [Full details given by Thompson et al. (2018BB175).]

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