Figure 9
Examples of fits (red line) to XRD data (blue), along with individual phase contributions, obtained for (top) fast- and (middle and bottom) slow-cooling-rate experiments. The two slow-cooling-rate patterns were collected two weeks apart on days 167 and 181, respectively, of the long-duration experiment and show the development of NMS16 via the Bragg peak at ∼2° 2θ, as also indicated in Fig. 7. Data collected at 15 keV (0.824603 Å) and 25 keV (0.49388 Å, average) for the fast- and slow-cooling-rate experiments, respectively |