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Figure 8
In situ neutron powder diffraction of the reaction of palladium powder with deuterium at 360 (2) K. Top: pressure profile (left), diffraction data as false-colour plot with highest intensity in red and lowest intensity in blue (right). Bottom: Rietveld refinements (observed intensities, Iobs, in black, calculated intensities, Icalc, in red, difference, Iobs − Icalc, in blue, excluded region 72.6 ≤ 2θ ≤ 72.7° due to detector failure, 2 min per NUMOR; https://doi.org/10.5291/ILL-DATA.5-22-767) of the crystal structures of α-PdD0.024 (2) (NUMOR 145703, left, corresponding to orange line top right), α-PdD0.033 (4) and β-Pd0.518 (8) (NUMOR 145704, middle, corresponding to dark-green line top right), and β-PdD0.626 (6) (NUMOR 145748, right, corresponding to light-blue line top right).

Journal logoJOURNAL OF
APPLIED
CRYSTALLOGRAPHY
ISSN: 1600-5767
Volume 55| Part 1| February 2022| Pages 67-73
https://doi.org/10.1107/S1600576721012048
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