Figure 4
Instrumental resolution for the area-detector diffraction setup with a sample-to-detector distance of 0.7 m, sample dimensions of 0.35 mm and an active detector thickness of 100 µm. The convolution according to equation (2), together with the individual contributions, are plotted for detector angles = 12, 22, 32 and 42°. A divergence of 0.3 mrad was assumed for the primary X-ray beam. The wavelength dispersion is given by Δλ = 2Γtan(θ)/E0(180/π) (2θ), where Γ and E0 are the lifetime broadening and the peak emission energy in eV (Cheary et al., 2004), respectively. |