A multipurpose laboratory diffractometer for operando powder X-ray diffraction investigations of energy materials

Geßwein, H.; Stüble, P.; Weber, D.; Binder, J.R.; Mönig, R.

doi:10.1107/S1600576722003089

Journal of Applied Crystallography Journal of Applied
Crystallography

IUCr IT WDC

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Figure 5
PXRD patterns of the NIST SRM660b LaB₆ line-profile standard in a 0.5 mm capillary collected with the multipurpose diffractometer at a sample-to-detector distance of 50 cm, (a) with the Ge(111) monochromator and (b) without: experimental data (black crosses), fit (red line) and difference (residual, line below). The upper insets in (a) show the monochromatic Mo Kα₁ diffraction profiles and in (b) show the Mo Kα_1,2 doublet of the 111 and 421 LaB₆ peaks. FWHM [equation (3)