Figure 5
(a) Powder XRD diffractograms of CaWO4 of a single scan and of averaged diffractograms over 2, 4, 8, 16 and 32 scans (with each scan having been recorded for 10 min exposure time). (b) Si(331) reflection with a single scan (Rp = 7.1%, = 32.1%) and 32 scans (Rp = 4.3%, = 22.2%) averaged (solid black line) and their fitted data (red points). (c) FWHM values for the Si(331) reflection with various averaged scans up to 32. |