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Figure 3
Rietveld refinement profiles using XRD data of pyrite concentrate powder as (a) an unground control, and prepared by (b) hand grinding, (c) grease loading and (d) 7 min ball milling. The relative percentage differences between the observed (Io) and calculated (Ic) intensities are shown beneath each profile. Rietveld refinement residuals for each sample preparation are given in Table S2.

Journal logoJOURNAL OF
APPLIED
CRYSTALLOGRAPHY
ISSN: 1600-5767
Volume 55| Part 6| December 2022| Pages 1572-1582
https://doi.org/10.1107/S1600576722009888
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