Figure 8
In situ slit-smeared USAXS/SAXS data for SCMO collected from 673 to 1098 K (400 to 825°C) under a flow of 4% mass H2/96% mass N2 gas, together with associated phase fraction variations plotted as a function of temperature for species formed during the reduction of SCMO. (Estimated standard uncertainties are smaller than the data traces for the USAXS/SAXS data and are given by the vertical bars for the composition variations.) Also shown in the right-hand plot are the expected reduction reactions for this system [in addition see Witt et al. (2020)]. |