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Figure 4
(a) Progression of the relative integrated Bragg intensity, [\tilde I]relBragg, in stages III and IV, normalized to the value at the beginning of stage III ([{\tilde I_{\rm Bragg}}/{\tilde I_{\rm Bragg,\,{O_2}\,injection}}]). (b) Progression of the lattice parameter. For clarity, [\tilde I]relBragg and the corresponding lattice parameter are only depicted after the addition of O2 to the N2 gas flow after the final calcination temperature has been reached.

Journal logoJOURNAL OF
APPLIED
CRYSTALLOGRAPHY
ISSN: 1600-5767
Volume 56| Part 3| June 2023| Pages 801-809
https://doi.org/10.1107/S1600576723003886
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