Figure 1
(a) Comparison of the PDF obtained from LaB6 standard powder samples in a Ø0.2 mm glass capillary using the DCM (orange curve) and the MLM (blue curve). (b) Enlargement of the PDF range 50–100 Å. (c) Refinement of the LaB6 structure (Pm3m) to the DCM PDF, where Qdamp and Qbroad are refined. (d) Refinement of the LaB6 structure (Pm3m) to the MLM PDF, where Qdamp and Qbroad are refined. In (c) and (d), the experimental PDF is shown in blue, the calculated PDF in red and the difference between them in green. |