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Figure 5
Unit-cell volume of crystalline phases observed during the three regions of the synthesis process. (a) Rock salt-type cubic phases, (b) layered phases during the temperature ramp and (c) layered phases observed during a 2 h dwell at the targeted annealing temperature. Here, the different values of the volumes are also due to the different thermal expansion at the temperatures chosen for annealing.

Journal logoJOURNAL OF
APPLIED
CRYSTALLOGRAPHY
ISSN: 1600-5767
Volume 56| Part 4| August 2023| Pages 1066-1075
https://doi.org/10.1107/S1600576723004909
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