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Figure 3
Peak diffraction profiles from intact samples (a) S51-NB, (b) S52-NB and (c) S1-NB. Tables in each diagram outline information for peaks identified using the WAXS fit tool in the Irena software. For each peak, the tables include center (2θ units), width (2θ units) and d spacing (ångström). Errors are less than 10% for each parameter. In each table, bold numbers highlight data used in crystallite-size calculation. These crystallite-size estimations are explained in Section S1.

Journal logoJOURNAL OF
APPLIED
CRYSTALLOGRAPHY
ISSN: 1600-5767
Volume 56| Part 6| December 2023| Pages 1692-1706
https://doi.org/10.1107/S1600576723008889
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