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Figure 11
(a) Original and (b) pre-processed PDF profiles calculated from the hexagonal anhydrous rare-earth perchlorate Pr(ClO4)3 (Wickleder & Schäfer, 1999BB43), with the crystal cell parameters a = b = 9.336 Å and c = 5.849 Å. (c) Weight fractions determined by the unfolding procedure applied to monoatomic crystal cells and fitted with a third-order bidimensional polynomial (surface in red) and (d) scatter plot showing the fit residuals.

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APPLIED
CRYSTALLOGRAPHY
ISSN: 1600-5767
Volume 56| Part 6| December 2023| Pages 1841-1854
https://doi.org/10.1107/S1600576723008348
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