Figure 1
(a) A mechanical drawing of the XtaLAB Synergy Custom X-ray diffractometer, highlighting the large enclosure that houses the Cu rotating anode X-ray source, goniometer and 2D HPC detector. (b) A photograph of the inside of the X-ray enclosure highlighting the main components and the Raman probe. (c) A typical batch crystallization flow loop with capillary flow cell setup as shown in (b). (d) The continuous crystallization reactor geometry, including fReactor design (Guan et al., 2020; Manson et al., 2019; Chapman et al., 2017). |