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Figure 3
(a) Two-dimensional diffraction patterns of silver behenate powder collected in a 1 mm borosilicate capillary tube at 10 mrad optics. The (00l) planes are highlighted for clarity in the inset. (b) Rietveld fitting of the silver behenate diffraction pattern; the experimental data are in black, the fitted profile is in red and the difference plot is in blue. Inset is the 004 diffraction peak to highlight peak shape and the FWHM and Δ peak position against 2θ. |