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Figure 4
Characterization by X-ray diffraction of the solid rod crystal produced using a protein concentration of 30 mg mL−1 in a 0.2 mm capillary after 8 weeks. Full 3D data sets, indicated by blue triangles or pink squares, were recorded at regular 200 µm intervals along the length shown. Above each of the points measured (boxes 1 to 8) the overall merged statistics for a 1.7 Å resolution cut-off are shown, with bracketed values after each number (H) denoting outer-shell parameter values. This sample shows a space-group transition between monoclinic (blue triangles) and orthorhombic (pink squares) symmetries, with the parameter values given below.

Journal logoJOURNAL OF
APPLIED
CRYSTALLOGRAPHY
ISSN: 1600-5767
Volume 58| Part 1| February 2025|
https://doi.org/10.1107/S1600576724011191
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