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Figure 1
(a) Variation in the observed precursor PDF across all ten repetitions. The black line is a simulation of the model proposed by Kløve et al. (2022BB34) and the structure inset is a visual representation of the precursor solution structure (O: red; Zr: light green; Cl: dark green). (b) 2D contour plot of the PDFs obtained for the first 40 s after heat is applied. The gray dashed line marks 10 s. (c) Fit of the PDF after 10 s. Note that (b) and (c) are constructed with a broken axis to highlight the low-r region.

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CRYSTALLOGRAPHY
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