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Figure 3
Variation of refined parameters during the final minute of the experiment [(a) Biso,Zr, (b) Biso,O, (c) unit-cell volume] for each repetition compared with the average value across all ten repetitions. The error bars correspond to the mathematical standard uncertainty obtained from the least-squares minimization.

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APPLIED
CRYSTALLOGRAPHY
ISSN: 1600-5767
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