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Figure 6
(a) Final PDF obtained from the in situ experiment after 15 min using varying Qmax values from 12 to 22 Å−1. (b) Variation in refined parameters (I: Biso,Zr; II: Biso,O; III: particle diameter; IV: unit-cell volume) within the last 60 s of the in situ experiment using varying Qmax values. The dashed gray line is the values obtained using Qmax = 18 Å−1. The error bars correspond to the mathematical standard uncertainty obtained from the least-squares minimization.

Journal logoJOURNAL OF
APPLIED
CRYSTALLOGRAPHY
ISSN: 1600-5767
Volume 58| Part 2| April 2025| Pages 495-503
https://doi.org/10.1107/S1600576725001694
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