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Figure 3
PDF analysis after heat treatment. The PDF of (a) 4 nm and (b) 3 nm nanocrystals after annealing at 400°C for 1 h in air. The misfit at the first Zr—Zr peak is magnified to improve visualization. The refined parameters can be found in Tables S7 and S8.

Journal logoJOURNAL OF
APPLIED
CRYSTALLOGRAPHY
ISSN: 1600-5767
Volume 58| Part 3| June 2025|
https://doi.org/10.1107/S1600576725001761
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