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Figure 3
Experimental PXRD patterns (solid lines) for the solid solutions NA2·FAxSA1−x (NA-SS) as obtained by ball-milling synthesis. For comparison, calculated patterns from single-crystal data are also shown (dashed lines) for the pure co-crystals NA2·SA (bottom, data collected at 120 K, CSD refcode DUZPAQ; the difference between the acquisition temperature and the room-temperature experimental data is responsible for the shift observable at higher 2θ) and NA2·FA (top, CSD refcode EDAPOQ).

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