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Figure 1
XRD patterns obtained with Co Kα radiation using setup (i). Data modelled according to the Pawley method, with Voigtian line profiles: (a) pristine FeCr powder, and after (b) 8 h, (c) 32 h and (d) 64 h ball milling. The insets show an amplified view of the 110 reflection. Effect of the ball-milling time on (e) lattice parameter and (f) integral breadth in the traditional WH plot [dashed lines refer to equation (1[link]), see main text for details].

Journal logoJOURNAL OF
APPLIED
CRYSTALLOGRAPHY
ISSN: 1600-5767
Volume 58| Part 5| October 2025| Pages 1764-1777
https://doi.org/10.1107/S1600576725006946
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