Operando anomalous X-ray powder diffraction interleaved with X-ray absorption spectroscopy using a scanning 2D imaging detector on the XMaS beamline: design, implementation and performance

Wardecki, D.; Thompson, P.B.J.; Mlekodaj, K.; Dowsett, M.G.; Adriaens, M.; Knorpp, A.J.; Dejoie, C.; Góra-Marek, K.; van Bokhoven, J.A.; Newton, M.A.; Rzepka, P.

doi:10.1107/S1600576725007022

Journal of Applied Crystallography Journal of Applied
Crystallography

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Figure 1
Experimental arrangement for the measurement of anomalous XRPD using a scanning flat-panel detector, showing how it is interleaved with transmission XAS. (a) The mounting of the flat-panel detector and ion chambers on independent arms on one axis (in the direction of the X-ray beam) of a six-circle Huber diffractometer. (b) and (c) Schematic representations indicating the direction and range of movement of the flat-panel (Pilatus) detector.

JOURNAL OF
APPLIED
CRYSTALLOGRAPHY

ISSN: 1600-5767

Volume 58| Part 5| October 2025| Pages 1778-1788

https://doi.org/10.1107/S1600576725007022

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