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Figure 4
(a) Normalized Cu K edge XANES collected at each sample temperature (as indicated) for which AXRPD data were subsequently collected from the Cu–MAZ system experiencing an O2 flow. (b) A comparison (250°C) of the results of LCA analysis and residuals. (c) Partitioning of CuII speciation between hydrated (black) and dehydrated (red) states as a function of temperature as derived from LCA analysis of the Cu K edge XANES.

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