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Figure 10
Detector misorientation. Individual diffraction calibration misorientation (left column) and corresponding frequency distributions (right column). The measurements from a LaB6 powder sample are repeated for different displacements of a capillary sample in the gravity direction while keeping the beam at constant KB position and with (A) the conventional transmission detector geometry and (B), (C) the detector tilted relative to the incoming beam. The calibrations were repeated including the energy (A), (B) as a free degree of freedom or (C), (D) fixed. (D) The misorientations measured with the same detector and sample configurations as (A)–(C) but also scanning the y axes with the KB position motion while keeping the sample steady. FE: front end.

Journal logoJOURNAL OF
APPLIED
CRYSTALLOGRAPHY
ISSN: 1600-5767
Volume 59| Part 1| February 2026| Pages 12-27
https://doi.org/10.1107/S1600576725009811
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