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Figure 11
Energy calibration of the diffraction beam via observation of a standard-material absorption edge. Intensity measurements were acquired using the imaging camera with a fixed KB mirror position. The large active area of the imaging scintillator enabled full beam capture, compensating for minor beam displacements caused by changes in the DCM configuration. Measurements were taken with and without the Mo foil in the beam path, allowing normalization of the transmitted intensity to account for flux variations across different Bragg angles. These variations arise from the energy-dependent efficiency of the DCM, KB mirrors and the source emission profile.

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APPLIED
CRYSTALLOGRAPHY
ISSN: 1600-5767
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