Figure 12
Chemical shift as a function of dilution (A→F) of 14 in CDCl3. In F, δ 6.88 (H2, H6 of 1), δ 6.74 (H4 of 6), δ 6.55 (H2, H6 of 6). A significant upfield shift of the H2, H6 protons of 1, combined with overall line-narrowing is observed upon dilution from E to F. |