Figure 5
Solid-state 13C CP/MAS (column A) and 23Na (column B) MAS NMR spectra measured at 313 K. Resonance assignments are shown for AH and MH (labelling according to Scheme 1). The assignments for DH-I and DH-II are clear by analogy. Spectra are also shown for sodium ibuprofen dihydrate (top), which has a similar structure to DH-II in the Na+/H2O region (see text). |