Figure 4
(a) The rutile average structure of Fe3+OF, in projection along [001] (O/F anions, A, are denoted by small red balls and the Fe atoms are in the FeA6 octahedra). (b) Close to [001], (c) 〈〉 and (d) 〈110〉 zone-axis EDPs of FeOF. Note the presence of G±∊[]* (∊ continuous) rods of diffuse intensity in (b) (indicated by white arrows) but their systematic absence in (d). Note also the apparent appearance of G±[]* `satellite reflections' [indicated by white arrows in (d)] arising from the G±∊[110]* diffuse rods cutting through the ZOLZ. |