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Figure 3
Synthesis of the NAG-NAM disaccharide. Reagents and conditions: (a) Et3SiH, I2, 0°C, 2 h; (b) AgTf, RT, 18 h; (c) NaOMe, MeOH, RT, 1 h; hydrazine hydrate, EtOH, 80°C, 2 h; pyridine, acetic anhydride, RT, 18 h; (d) 0.5 M KOH, dioxane, RT, 48 h; H2, Pd/C, EtOH:HOAc:water; RT, 18 h.

IUCrJ
Volume 4| Part 2| March 2017| Pages 185-198
ISSN: 2052-2525
https://doi.org/10.1107/S2052252517000367