NMR crystallography: structure and properties of materials from solid-state nuclear magnetic resonance observables

Bryce, D.L.

doi:10.1107/S2052252517006042

Figure 3
In situ ¹H→¹³C cross polarization NMR spectra recorded as a function of time during the crystallization of m-aminobenzoic acid (m-ABA) from methanol, showing the region of the spectrum containing the peak for the carboxylate group. The known peak positions for the carboxylate groups in Forms I and III are highlighted by dashed lines. (a) The intensity contour plot showing all spectra recorded as a function of time during the in situ study. (b) Summation of the first two spectra (bottom) and the last two spectra (top) recorded during the in situ study. Figure from Harris et al. (2017