Sr2Pt8−xAs: a layered incommensurately modulated metal with saturated resistivity

Martino, E.; Arakcheeva, A.; Autès, G.; Pisoni, A.; Bachmann, M.D.; Modic, K.A.; Helm, T.; Yazyev, O.V.; Moll, P.J.W.; Forró, L.; Katrych, S.

doi:10.1107/S2052252518007303

research papers

IUCrJ

Volume 5| Part 4| July 2018| Pages 470-477

ISSN: 2052-2525

https://doi.org/10.1107/S2052252518007303

MATERIALS | COMPUTATION

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Sr₂Pt_8−xAs: a layered incommensurately modulated metal with saturated resistivity

^aLaboratory of Physics of Complex Matter, École Polytechnique Fédérale de Lausanne (EPFL), Lausanne CH-1015, Switzerland, ^bMax-Planck-Institute for Chemical Physics of Solids, Dresden 01187, Germany, and ^cNational Centre for Computational Design and Discovery of Novel Materials MARVEL, École Polytechnique Fédérale de Lausanne (EPFL), Lausanne CH-1015, Switzerland
^*Correspondence e-mail: edoardo.martino@epfl.ch, sergiy.katrych@epfl.ch

Edited by A. Fitch, ESRF, France (Received 26 February 2018; accepted 15 May 2018; online 8 June 2018)

The high-pressure synthesis and incommensurately modulated structure are reported for the new compound Sr₂Pt_8−xAs, with x = 0.715 (5). The structure consists of Sr₂Pt₃As layers alternating with Pt-only corrugated grids. Ab initio calculations predict a metallic character with a dominant role of the Pt d electrons. The electrical resistivity (ρ) and Seebeck coefficient confirm the metallic character, but surprisingly, ρ showed a near-flat temperature dependence. This observation fits the description of the Mooij correlation for electrical resistivity in disordered metals, originally developed for statistically distributed point defects. The discussed material has a long-range crystallographic order, but the high concentration of Pt vacancies, incommensurately ordered, strongly influences the electronic conduction properties. This result extends the range of validity of the Mooij correlation to long-range ordered incommensurately modulated vacancies. Motivated by the layered structure, the resistivity anisotropy was measured in a focused-ion-beam micro-fabricated well oriented single crystal. A low resistivity anisotropy indicates that the layers are electrically coupled and conduction channels along different directions are intermixed.

Keywords: platinum-based metallic compounds; incommensurately modulated structure; vacancies; Mooij correlation; composite materials; inorganic materials; density functional theory.

CCDC references: 1843351; 1843352; 1843353

1. Introduction

In the search for materials with novel electronic properties, the family of Pt-based ternary compounds is a good target because it is rich in various compositions, yet investigated only to a limited extent. In some, superconductivity and/or unconventional electronic properties have been reported, for example in SrPtAs (Nishikubo et al., 2011 ), SrPt₂As₂ (Kudo et al., 2010 ), SrPt₃P (Takayama et al., 2012 ), LaPt₅As (Fujioka et al., 2016 ), SrPt₆P₂ (Lv et al., 2014 ), SrPt₂Ge₂ (Ku et al., 2013 ), SrPtGe₃ (Miliyanchuk et al., 2011 ) and Ca₂Pt₃Si₅ (Takeuchi et al., 2009 ).

Our goal was to investigate the Sr–Pt–As ternary system in the Pt-rich area, which is largely unexplored. We started by targeting the hypothetical composition SrPt₃As, not yet synthesized, but analogous to SrPt₃P, which is known as a strongly coupled superconductor with a critical temperature T_C = 8.4 K (Takayama et al., 2012) and characterized by a high electron–phonon coupling (Zocco et al., 2015 ; Subedi et al., 2013 ).

The synthesis of this composition, where As replaces P, was the primary motivation for this work. A similar strategy led to the discovery of high-temperature superconductivity (with a T_C up to 55 K) in the Fe-based pnictides, when LaO_1−xF_xFeAs was synthesized because of the known parent superconducting compound LaOFeP, which has a much lower critical temperature (T_C = 4 K) (Kamihara et al., 2008 ).

We adopted a high-pressure synthesis route, through which we reproducibly synthesized the new compound Sr₂Pt_8−xAs. It has a layered structure built from covalently bonded polyanions analogous to Ce₂Pt₈As (Chizhov et al., 2009 ). The large number of ordered vacancies in Pt positions [x = 0.715 (5)] results in an incommensurately modulated (IM) structure. It is a fundamentally exciting question as to how these long-range ordered IM vacancies affect electronic transport properties. Do they act as random static defects which are at the origin of the Mooij correlation (Mooij, 1973 )? Does the IM structure introduce a gap in the electronic states like in quasi-two-dimensional (Sipos et al., 2008 ) or quasi-one-dimensional materials (Voit et al., 2000 )? To answer these questions, we performed a detailed refinement of the structure and calculated the density of states (DOS) using a density functional theory (DFT) approach. We also performed measurements of the electrical resistivity (ρ) and Seebeck coefficient (S) as a function of temperature. We did not observe the SrPt₃As phase as a result of our high-pressure synthesis, despite fine variation in the parameter space of pressure, temperature and reaction time.

2. Experimental

2.1. High-pressure synthesis

The crystals were grown using a high-pressure multi-anvil setup because of the high arsenic partial pressure at high temperatures. Two preparation routes were used: (i) a pre-reacted mixture of a near-binary eutectic composition of Pt₇As₃ was combined with strontium and platinum, or (ii) the combination of pure elements: Pt sponge (60 mesh, 99.98%, metallic basis), Sr dendritic pieces (99.95%, metallic basis), powdered As sponge (99.95%, metallic basis). Details of each step are reported in Table 1. The mixture of Pt₇As₃ (2 g, prepared according to the procedure described in Table 1, No. 1) was compressed into a pellet with the addition of Pt and Sr (final composition: SrPt₃As), sealed in a quartz glass tube at 202 hPa of Ar and heated according to No. 1a. The product was reground, compressed into a pellet and heated in a sealed quartz glass ampulla according to No. 1b. The product of No. 1b was placed in a boron nitride crucible and the crystals were grown by the self-flux method at high pressure (2.3 GPa, No. 1c). At the end of the synthesis, cooling to room temperature was realized by switching off the power supply.

Table 1
Details of the high-pressure synthesis of Sr₂Pt_8−xAs single crystals

No.	Composition	Components	Procedure
1	Pt₇As₃	7Pt + 3As	0.5 h→673 K (1h†)→3 h→803 K (2 h)→1 h→853 K (5 h)→3 h→893 K (50 h)→WQ‡
1a	SrPt₃As	⅓Pt₇As₃ (from No. 1) + ⅔Pt + Sr	4 h→873 K (1 h)→2 h→913 K (2 h)→1 h→923 K (2 h)→1 h→933 K (1 h)→1 h→943 K (2 h)→WQ
1b	SrPt₃As	Product 1a powdered and compressed into a pellet	1 h→943 K (20 min)→2 h→1023 K (2 h)→1 h→1073 K (0.5 h)→2 h→1113 K (10 h)→WQ
1c	SrPt₃As	Product 1b powdered and compressed into a pellet	2.3 GPa, 0.2 h →773 K→2 h→1423 K (0.7 h)→45 h→1323 K (20 h)→room temperature

†The annealing time in hours is given in parentheses.
‡WQ, water quenched.

2.2. X-ray diffraction

Single-crystal X-ray diffraction data collection was performed on a SuperNova (dual source) four-circle diffractometer (Agilent Technologies, USA) equipped with a CCD detector. Data reduction and analytical absorption correction were made using the CrysAlisPRO software package (Oxford Diffraction, 2014 $[Oxford Diffraction (2014). CrysAlisPRO. Agilent Technologies, Oxford.]$ ). The reciprocal space reconstructions supported the choice of the superspace group shown in Fig. 1. The crystal structure was solved by the charge-flipping method (Palatinus & Chapuis, 2007 ) and refined using the JANA2006 program package (Petříček et al., 2014 ). The outcome of the data analysis is given in Table 2, and further details are provided in the supporting information.

Table 2
Results of the X-ray study of Sr₂Pt_8−xAs [x = 0.715 (5)]

Crystal data
Chemical formula	AsPt_7.285Sr₂
M_r	1671.32
Crystal system, superspace group	Orthorhombic, Amma(00γ)ss0† (No. 63.1.13.11‡)
Temperature (K)	293
Wavevectors	q = 0.6038 (7)c*
a, b, c (Å)	7.9509 (4), 18.1042 (10), 5.6972 (3)
V (Å³)	820.08 (8)
Z	4
Radiation type	Mo Kα
μ (mm⁻¹)	140.54
Crystal size (mm)	0.01 × 0.006 × 0.002

Data collection
Diffractometer	SuperNova, Dual, Cu at zero, Atlas
Absorption correction	Multi-scan CrysAlis PRO, Agilent Technologies, Version 1.171.37.34. Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm.
No. of measured, independent and observed [I > 3σ(I)] reflections	10459, 1220, 781
No. of observed reflections: main, the first-order satellites	440, 341
R_int	0.092
(sin θ/λ)_max (Å⁻¹)	0.625

Refinement
R[F² > 3σ(F²)], wR(F²), S	0.0296, 0.0394, 1.32
R, wR for main reflections	0.0270, 0.0330
R, wR for satellites	0.0378, 0.0536
No. of reflections	1220
No. of parameters	54
Δρ_max, Δρ_min (e Å⁻³)	3.99, −3.31

†No. of the superspace group in the superspace group table created by Stokes et al. (2011

).
‡Symmetry operations: (1) x₁, x₂, x₃, x₄; (2) −x₁ + 1/2, −x₂ + 1/2, x₃ + 1/2, x₄; (3) −x₁, x₂, −x₃, −x₄ + 1/2; (4) x₁ + 1/2, −x₂ + 1/2, −x₃ + 1/2, −x₄ + 1/2; (5) −x₁, −x₂ + 1/2, −x₃ + 1/2, −x₄; (6) x₁ + 1/2, x₂, −x₃, −x₄; (7) x₁, −x₂ + 1/2, x₃ + 1/2, x₄ + 1/2; (8) −x₁ + 1/2, x₂, x₃, x₄ + 1/2.

Figure 1
Sections of reciprocal space with main and satellite reflections. The hklm indices correspond to the orthorhombic unit-cell parameters a = 7.95, b = 18.10, c = 5.70 Å and the modulation wavevector q = 0.6038c* (yellow arrows in insets). In (a) and (b), the intersections of white lines in the bottom right-hand quarters define strong main hkl0 reflections; strong satellites of the first order, 1kl1, and weak satellites of the second order, h0l2, are away from the intersections. In (c) and (d), the hk01 and hk02 satellites are shown separately. Weak satellites of the second order, hk02, can be observed only in the areas with low background.

2.3. DOS calculations

The first-principles calculation of the DOS was performed using DFT within the generalized gradient approximation as implemented in the Quantum Espresso package (Giannozzi et al., 2009 ). The computation was carried out on the commensurate superstructure approximation of the solved structure with 204 atoms in the unit cell using scalar relativistic ultrasoft pseudo potentials, a 3 × 2 × 2 k-points mesh and a planewave kinetic energy cut-off of 50 Ry for the wavefunctions.

The projected DOS was obtained by projecting the Kohn–Sham wavefunctions onto localized atomic orbitals.

2.4. Electrical resistivity and Seebeck coefficient

For precise measurements of the absolute electrical resistivity (ρ) and its anisotropy, we produced a micro-fabricated sample from a single crystal using a focused ion beam (FIB) (Moll, 2018 ). This approach has already proven its potential and reliability in the study of novel materials (Moll et al., 2010 ). The starting crystal, which was 150 × 150 × 50 µm in size, was first analysed by single-crystal X-ray diffraction to confirm the correct structure and identify the crystallographic axes.

The Seebeck coefficient (S) is the magnitude of the open circuit voltage induced across a material under a thermal gradient, and was measured according to the previously reported procedure (Jaćimović et al., 2013 ). For this experiment, we used a ceramic sample since S is not affected by grain boundaries, and the longer sample size guaranteed a well defined temperature gradient necessary for precise measurements. Both coefficients, ρ and S were measured in the 4.2–300 K temperature range.

3. Results

3.1. Determination of the incommensurately modulated structure of Sr₂Pt_8−xAs

The distribution of reflections in reciprocal space is shown in Fig. 1, and in more detail in Fig. S1 (see supporting information). The main Bragg peaks correspond to orthorhombic symmetry, and the satellite reflections indicate an IM structure. The unit-cell parameters are a = 7.95, b = 18.10 and c = 5.70 Å, with the modulation wavevector q = 0.6038 (7)c*. The reflection conditions (hklm: k + l = 2n; 0klm: m = 2n; h0lm: m = 2n; hk00: h = 2n) point to the (3 + 1)-dimensional superspace group Amma(00γ)ss0 [No. 63.1.13.11 after van Smaalen et al. (2013 ) and Stokes et al. (2011 )]. Two orders of the satellite reflections can be observed (Figs. 1 and S1), but second-order satellites are very weak, so the intensity (I) for only a few could be measured with meaningful significance [I > 3σ(I)]. Hence, only the first-order satellites were used in our calculations.

Based on main reflections only, the average structure was determined in the Amma space group (No. 63) with the reliability index R = 0.031. Five Pt, one Sr and one As site define the structure (Table S1), with the Pt5 site being partially occupied by about 68%. The low value of the reliability index for the average structure is a result of the specific structural modulations, which only slightly relate to the displacive modulations. Pt1 and As1 do not exhibit modulation because of symmetry restrictions; for a number of other atoms, allowed harmonics are zero within one standard deviation (Table S1). It should be noted that the very weak modulation of Pt5 along the a axis was constrained to zero because of the correlation with U11.

The strong intensities of the first-order satellite reflections (Fig. 1) are determined by the occupancy modulation of Pt5. Different possible models for the occupancy function are shown in Fig. 2. The harmonic function (Fig. 2a) gives a negative occupancy of about 30% in the t range and a high uncertainty of the value for the cosine component of the occupancy wave, ocos1 = 0.48 (14). The negative occupancy indicates a high probability of the crenel model, which determines either the presence or absence of the atom along the t axis. The instability of the cosine component can be explained by the pseudo-special position of Pt5 (∼1/2, y, ∼0). The harmonic function gives satisfactory results only with the constraint ocos1 = 0 (Fig. 2b). The crenel function (Fig. 2c) gives reasonable results without any restriction. The residual electron density (Δρ) calculated in the vicinity of the Pt5 position is analogous for all the models (Fig. 2). All of them are characterized by the similar reliabilities (R_main ≃ 0.027, R_sat ≃ 0.038, R_all ≃ 0.030). A smaller Δρ_max (4 versus 4.6 e Å⁻³) and the absence of any restrictions favour the crenel model. Hence, we can conclude that this model is the more suitable approximation for the Pt5 occupancy function.

Figure 2
Three possible models of the Pt5 occupancy function and the corresponding Fourier maps of the residual electron density (Δρ) calculated for the vicinity of the Pt5 position. (a) The harmonic function applied without any restriction, (b) the harmonic function constrained by ocos1 = 0 and (c) the crenel function; all of them give low values of Δρ. Red lines show the position modulation functions of Pt5. The black solid, dashed and dotted lines indicate positive, zero and negative contours, respectively, with a step of 0.5 eÅ⁻³.

Portions of the IM structure are shown in Figs. 3 and 4. Sr₂Pt_8−xAs can be described as Sr₂Pt₃As layers (blue background in Fig. 3) alternating with the Pt-only corrugated grids (red background in Fig. 3). The atomic arrangement in the Sr₂Pt₃As layer is a host network of AsPt₆ distorted bipyramids, with the As atom displaced along the apical direction (c axis in Fig. 3). The two apical distances are quite different, 2.33 and 3.37 Å (As–Pt1 in Fig. 4a); however, the remaining four, corresponding to the bipyramid bases, are all 2.45 Å (two As–Pt3 and two As–Pt2 in Fig. 4).

Figure 3
Sketch of the crystal structure of Sr₂Pt_8−xAs. (a) and (b) are portions of the Sr₂Pt_7.285As IM structure with the modulation wavevector q = 0.6038c*. (b) and (c) represent the commensurate superstructure approximation with q = 0.6c*. Different colours show five different atomic sites of Pt, Pt1, Pt2 and Pt3 (grey) forming a layer of edge-sharing AsPt₆ bipyramids (green) centred by As (blue background). This layer of AsPt₆ bipyramids is identical in both the IM structure and its commensurate approximation. Pt4 (brown) and Pt5 (blue) form the `metallic' corrugated grids (red background), which are aperiodic along the c axis in the IM structure. The short Pt–Pt contacts of 2.4–2.74 Å are shown by lines.

Figure 4
Interatomic distances in the Sr₂Pt_7.285As IM structure. (a) The t plot of the As–Pt and Pt–Pt distances. (b) A portion of the incommensurate structure with an indication of the most variable Pt5–Pt3 (red) and Pt5–Pt4 (blue) distances. (c) Variations of the Pt5–Pt3 and Pt5–Pt4 distances are determined by a wave of the Pt4 displacement along the a axis. The distances are indicated by identical colours in (a), (b) and (c).

Interatomic distances between neighbouring atoms show little variation in the IM structure, with the exception of those around Pt5 (Fig. 4b). The Pt5–Pt(3,4) distances are not only the most variable, but they are also shorter than in pure Pt (2.77 Å). Moreover, as it can be deduced from Fig. 4(b) that vacancies in the Pt5 position occur at the minimum in the Pt5–Pt3 distance (<2.42 Å). In other words, the strain induced by shortening of the Pt5–Pt3 distances defines the vacancy positions (Janssen et al., 2010 ). They are periodically located along the modulation wave (axis t in Fig. 4a), but aperiodically, i.e. long-range ordered, in the bulk of the crystal.

3.2. Density of states

In order to obtain insight into the electronic character of the compound, we calculated the DOS using DFT. The standard methodologies used to calculate electronic structures are not suitable for IM structures or structures with partially occupied sites. In order to provide a reasonable DOS estimation, we performed calculations on a commensurate superstructure approximation (Figs. 3b and 3c). The experimental data were approximated using a modulation wavevector q = 3/5c* = 0.6c* (instead of 0.6038c*), which corresponds to the supercell parameter c_sc = 5c (Fig. 3c). The two possible space groups, Pnca and Pncn, depending on the origin for the (3 + 1)-dimensional superspace (t₀), were tested. The best results with the reliability index R(all) = 0.033 were obtained with the Pncn space group. Since the modulations in the displacement of all atoms are very small in the IM structure, the commensurate approximant differs only for the vacancy distribution within the Pt5 positions (Fig. 3c). The composition of the approximant is Sr₂Pt_7.2As, slightly different from the real compound, Sr₂Pt_7.285As. For the commensurate analogue, the high DOS at the Fermi level (Fig. 5) clearly shows the metallic character of the compound and from the individual contribution of each ion, one can note that mainly the Pt d atomic orbitals contribute to electronic conduction, since they have the highest density at the Fermi level.

Figure 5
DOS calculated using DFT for the commensurate superstructure approximation, showing the contribution of each ion and Pt atomic orbital in a different colour. The high value of DOS at E_F indicates the metallic character of the compound.

3.3. Anisotropy of the electrical resistivity and the Seebeck coefficient

The manifestation of the high DOS seen above was investigated by means of electrical transport measurements. Initial measurements on ceramic samples from different syntheses showed a very weak temperature dependence of ρ (Fig. S2). In ceramic samples, crystallites are often randomly oriented and grain boundaries add an extrinsic contribution to the electrical resistivity, therefore we could not determine definitively whether the weak temperature dependence of ρ was an intrinsic property of the material.

The relevant measurements of ρ were obtained on a micro-fabricated and oriented single crystal, where the current paths along different crystallographic directions were designed with an FIB (see Fig. 6a). The observation of weak temperature dependence, a 5% change from 300 to 4.2 K (Fig. 6b), proves that this is an intrinsic property of the material, and not an artefact of grain boundary contribution or composition inhomogeneity. Thanks to the precise control of the sample geometry, the absolute value of 170 µΩ cm at 4.2 K for the resistivity along the a axis was determined with good accuracy.

Figure 6
Electrical resistivity anisotropy measured on a micro-fabricated single crystal of Sr₂Pt_8−xAs (purple in the SEM image). (a) The starting lamella were extracted from the single crystal following the identified crystallographic direction from X-ray diffraction. Electrical resistivity is measured along the a and b axes as a function of temperature. For the b axis, the voltage drop was measured at two positions with different geometrical factors (V_b1, V_b2). The current flows between the two leads (marked as I⁺ and I⁻). Colours are added to identify the micro-fabricated crystal (purple) and the sputtered gold top contacts (yellow). The crystal is fixed on a sapphire substrate by a drop of epoxy glue. (b) A nearly temperature-independent electrical resistivity was observed along both crystallographic directions. The resistivity is higher for current flow perpendicular to the layers. In the inset, resistivity curves normalized to their value at 300 K show identical temperature dependences.

These results (the large absolute value of ρ and its very weak temperature dependence) match very well the case of Mooij correlation, which shows a connection between the slope of the electrical resistivity (dρ/dT) and its absolute value in metals with a high a concentration of static defects (Mooij, 1973). Within the limit of low-defect concentration, the charge scattering on static defects adds a constant contribution to the electrical resistivity, described by Matthiessen's rule, and simply shifts ρ(T) upwards. In the opposite case of high-defect concentration, the resistivity temperature dependence decreases, and above a threshold value (ρ_TH) of 150–200 µΩ cm, its derivative (dρ/dT) changes sign from metallic (> 0) to non-metallic (< 0). This empirical relation between the slope and the value of the resistivity is known as the Mooij correlation, and it is closely related to the Ioffe–Regel criterion (Gurvitch, 1981 ) for metallicity and localization phenomena in metals. Such arguments have been developed for typical metallic systems, with carrier densities in the order of 10²³ cm⁻³.

Belitz and Schirmacher went beyond the phenomenology and gave a theoretical description of the temperature dependence of the electrical resistivity in strongly disordered metals (Belitz & Schirmacher, 1983 ). In their work, they proposed the following equation:

$[\sigma \left(T \right) = 1/\rho (T) = {e^2}\left[{(n/m)/({M_0} + {M_{T}}} ) + {L_0} + {L_{T}}\right] \eqno (1)]$

where L₀ and M₀ are the contributions to resistivity in the pristine sample, M_T is the generalized scattering rate attributed to the electron–phonon coupling and L_T is the phonon-assisted tunnelling rate of electrons. In their equation, the temperature dependence is given by electron–phonon scattering, as in any normal metal. The salient feature of strongly disordered systems is the occurrence of localizations, when the very short electron mean-free path localizes them at the same position. In this situation, scattering with phonons helps electrons to move, favouring the tunnelling between two distinct localization sites (L_T). This mechanism is at the origin of `semiconducting-like' resistivity in strongly disordered metals, since the phonon population, favouring electronic conduction, is thermally activated.

In the case of Sr₂Pt_8−xAs, vacancies are long-range-ordered, with a modulation wavevector that is incommensurate with the crystal structure, a case so far not considered for the Mooij correlation. However, from the viewpoint of conduction electrons, vacancies ordered with an incommensurate periodicity act as scattering centres, like statistically distributed point defects. In our measurements, resistivity has a value close to ρ_TH along the plane, and even goes above that for the b axis, yet dρ/dT is positive, as in a metal (Fig. 6b). However, there is no contradiction with the Mooij correlation, since Tsuei has shown that ρ_TH is not universal, the value at which the resistivity changes slope has a material specificity (Tsuei, 1986 ). This could very well apply to our compound.

A relevant analogy with our results can be drawn with the case of SrPt_3−yPd_yP (Hu et al., 2016 ). As pointed out in the crystal structure description, SrPt₃P can be seen as a parent compound of Sr₂Pt_8−xAs. Increasing Pd concentration in SrPt_3-yPd_yP reduces the ρ temperature dependence to less than 5% from 300 to 6 K, resembling our experimental data for the case of higher substitution (y = 0.4), which is very close to the vacancy concentration for Pt5. We suppose that the same mechanism occurs in the two compounds, where defects in the Pt sites (vacancies or substitutions) strongly affect the electronic transport properties.

From the measurements on the micro-fabricated sample, electrical resistivity in the two perpendicular directions differs only in their absolute value (despite the layered structure), and both have the same temperature dependence, as can be seen in the inset in Fig. 6(b). One can say that from an electronic point of view, the material is isotropic. The scattering of the high-density Pt vacancies affects the electronic transport in the same way in the directions parallel and perpendicular to the layers, homogenizing the resistivity tensor to have identical temperature dependences along different directions.

The Seebeck coefficient measurement confirms experimentally the expected metallic character (Fig. 7), and the localization effects seen in resistivity are absent in S. The low absolute value and linear temperature dependence are the fingerprints of a large bandwidth metal (Behnia, 2015 ). S in a metallic system can be described by Mott's formula:

$[{S} = {{{\pi }^{2}{k}_{\rm B}}\over{3e}}{{{k}_{\rm B}T}\over{{E}_{\rm F}}}. \eqno (2)]$

Following this equation, it is possible to approximate the Fermi energy from the linear part of S, evaluated to be in the 6 eV range. The inset of Fig. 7 shows S/T, which for metals is expected to be constant [see equation (2)]. Here it is temperature dependent, but this apparent non-metallicity is a result of the large intercept, probably coming from thermally activated additive contribution to S that freezes at temperatures lower than 50 K. The Seebeck coefficient at high temperatures (>50 K) can be described by the following equation:

$[{S}(T) = {S}_{0}T + A, \eqno (3)]$

where A is the thermally activated temperature-independent additive contribution. Both S₀ and A are negative.

Figure 7
The temperature dependence of the Seebeck coefficient confirms the metallic character. The inset shows S/T, usually plotted for metallic systems.

4. Conclusions

We have presented a new layered IM structure of Sr₂Pt_8−xAs [x = 0.715(5)], synthesized at high pressure. High-quality X-ray diffraction data helped us to refine the structure of the crystal. The compound has a strong off-stoichiometry, and the structural strain field, acting on the aperiodically distributed vacancies, results in an IM structure. The incommensurate potential of long-range ordered Pt vacancies are responsible for the almost temperature-independent electrical resistivity, described in the context of the Mooij correlation. This experimental result shows that such correlation, first thought to occur only in the presence of stochastic disorder, can manifest also for long-range ordered IM vacancies, opening up new possibilities for theoretical studies and understanding of the phenomena of electron localization in metals.

A detailed understanding of the role of structure modulation in complex materials is an important issue and we believe that one can get a better insight by studying structurally well defined (Zhou et al., 2016 ) crystalline materials with modulated structures similar to the present compound. For example, an important aspect of the physical properties would be the study of the optical conductivity. One could get an estimate of electronic relaxation time, or more importantly, if there is a resonance, a so-called pinned mode at finite energy that could manifest as a result of the incommensurate modulation.

Moreover, the analogous compound Ce₂Pt₈P (Chizhov et al., 2009) belongs to a homological series of Ce_n+mPt_5n+3mP_m compounds, and because of its strong similarity to the investigated compound, the existence of the Sr_n+mPt_5n+3mAs_m homological series is highly probable, suggesting that many more interesting compounds are still yet to be discovered.

Supporting information

CCDC references: 1843351; 1843352; 1843353

Crystal structure: contains datablocks global, I, II, III. DOI: https://doi.org/10.1107/S2052252518007303/fc5025sup1.cif

Supporting information file. DOI: https://doi.org/10.1107/S2052252518007303/fc5025sup2.pdf

Computing details top

For all structures, data collection: CrysAlis PRO, Agilent Technologies, Version 1.171.37.34 (release 22-05-2014 CrysAlis171 .NET) (compiled May 22 2014,16:03:01); cell refinement: CrysAlis PRO, Agilent Technologies, Version 1.171.37.34 (release 22-05-2014 CrysAlis171 .NET) (compiled May 22 2014,16:03:01); data reduction: CrysAlis PRO, Agilent Technologies, Version 1.171.37.34 (release 22-05-2014 CrysAlis171 .NET) (compiled May 22 2014,16:03:01); molecular graphics: Brandenburg, K. & Putz, H. (2005). DIAMOND Version 3. Crystal Impact GbR, Postfach 1251, D-53002 Bonn, Germany.

(I) top

Crystal data top

AsPt_7.285Sr₂	F(000) = 2709
M_r = 1671.3	D_x = 13.537 Mg m⁻³
Orthorhombic, Amma(00γ)ss0†	Mo Kα radiation, λ = 0.71073 Å
q = 0.603800c*	Cell parameters from 3790 reflections
a = 7.9509 (4) Å	θ = 3.8–26.4°
b = 18.1042 (10) Å	µ = 140.54 mm⁻¹
c = 5.6972 (3) Å	T = 293 K
V = 820.08 (7) Å³	Plate, metallic dark black
Z = 4	0.01 × 0.01 × 0.002 mm

† Symmetry operations: (1) x₁, x₂, x₃, x₄; (2) −x₁+1/2, −x₂, x₃, x₄; (3) −x₁, x₂, −x₃, −x₄+1/2; (4) x₁+1/2, −x₂, −x₃, −x₄+1/2; (5) −x₁, −x₂, −x₃, −x₄; (6) x₁+1/2, x₂, −x₃, −x₄; (7) x₁, −x₂, x₃, x₄+1/2; (8) −x₁+1/2, x₂, x₃, x₄+1/2; (9) x₁, x₂+1/2, x₃+1/2, x₄; (10) −x₁+1/2, −x₂+1/2, x₃+1/2, x₄; (11) −x₁, x₂+1/2, −x₃+1/2, −x₄+1/2; (12) x₁+1/2, −x₂+1/2, −x₃+1/2, −x₄+1/2; (13) −x₁, −x₂+1/2, −x₃+1/2, −x₄; (14) x₁+1/2, x₂+1/2, −x₃+1/2, −x₄; (15) x₁, −x₂+1/2, x₃+1/2, x₄+1/2; (16) −x₁+1/2, x₂+1/2, x₃+1/2, x₄+1/2.

Data collection top

SuperNova, Dual, Cu at zero, Atlas diffractometer	1220 independent reflections
Radiation source: X-ray tube	781 reflections with I > 3σ(I)
Mirror monochromator	R_int = 0.092
Detector resolution: 5.1333 pixels mm^-1	θ_max = 26.4°, θ_min = 3.8°
ω scans	h = −9→8
Absorption correction: multi-scan CrysAlisPro, Agilent Technologies, Version 1.171.37.34 (release 22-05-2014 CrysAlis171 .NET) (compiled May 22 2014,16:03:01) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm.	k = −22→22
T_min = 0.279, T_max = 1.0	l = −7→7
10459 measured reflections

Refinement top

Refinement on F	2 constraints
R[F² > 2σ(F²)] = 0.030	Weighting scheme based on measured s.u.'s w = 1/(σ²(F) + 0.0001F²)
wR(F²) = 0.039	(Δ/σ)_max = 0.021
S = 1.32	Δρ_max = 3.99 e Å⁻³
1220 reflections	Δρ_min = −3.31 e Å⁻³
54 parameters	Extinction correction: B-C type 1 Gaussian isotropic (Becker & Coppens, 1974)
0 restraints	Extinction coefficient: 226 (8)

Special details top

Refinement. Occupancy of the Pt5 position is approximated by the Crenel function

Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å²) top

	x	y	z	U_iso*/U_eq	Occ. (<1)
Pt1	0.25	0.5	0.33957 (13)	0.0043 (2)
Pt2	0	0.5	0	0.0049 (2)
Pt3	0.25	0.38865 (3)	−0.00543 (9)	0.00493 (18)
Pt4	0.25	0.25139 (3)	0.25001 (9)	0.00686 (18)
Pt5	0.49984 (18)	0.29822 (5)	0.0128 (5)	0.0052 (5)	0.3212 (13)
Sr1	0	0.87900 (8)	0	0.0066 (4)
As1	0.25	0.5	0.7485 (3)	0.0024 (5)

Atomic displacement parameters (Å²) top

	U¹¹	U²²	U³³	U¹²	U¹³	U²³
Pt1	0.0052 (3)	0.0049 (4)	0.0028 (4)	0	0	0
Pt2	0.0007 (4)	0.0089 (4)	0.0051 (4)	0	0.0000 (2)	0
Pt3	0.0071 (3)	0.0020 (3)	0.0057 (3)	0	0	0.00006 (19)
Pt4	0.0121 (3)	0.0042 (3)	0.0044 (3)	0	0	0.0017 (2)
Pt5	0.0028 (4)	0.0037 (5)	0.0090 (12)	0.0001 (5)	0.0001 (3)	−0.0023 (9)
Sr1	0.0024 (6)	0.0057 (8)	0.0117 (7)	0	−0.0006 (5)	0
As1	0.0011 (8)	0.0035 (10)	0.0026 (9)	0	0	0

Geometric parameters (Å, º) top

	Average	Minimum	Maximum
Pt1—Pt2	2.7757 (10)	2.7738 (10)	2.7776 (10)
Pt1—Pt2ⁱ	2.7757 (10)	2.7738 (10)	2.7776 (10)
Pt1—Pt3	2.8168 (7)	2.8156 (7)	2.8180 (7)
Pt1—Pt3ⁱ	2.8168 (7)	2.8156 (7)	2.8180 (7)
Pt1—Sr1ⁱⁱ	3.098 (2)	3.048 (3)	3.151 (3)
Pt1—Sr1ⁱⁱⁱ	3.098 (2)	3.048 (3)	3.151 (3)
Pt1—Sr1^iv	3.098 (2)	3.048 (3)	3.151 (3)
Pt1—Sr1^v	3.098 (2)	3.048 (3)	3.151 (3)
Pt1—As1^vi	3.368 (2)	3.368 (2)	3.368 (2)
Pt1—As1	2.330 (2)	2.330 (2)	2.330 (2)
Pt2—Pt3	2.8343 (13)	2.8157 (14)	2.8588 (14)
Pt2—Pt3ⁱ	2.8343 (13)	2.8157 (14)	2.8588 (14)
Pt2—Pt3^vii	2.8343 (13)	2.8157 (14)	2.8588 (14)
Pt2—Pt3^viii	2.8343 (13)	2.8157 (14)	2.8588 (14)
Pt2—Sr1^ix	3.5941 (14)	3.3809 (18)	3.8062 (18)
Pt2—Sr1ⁱⁱ	3.5930 (14)	3.3809 (18)	3.8062 (18)
Pt2—Sr1^x	3.5930 (14)	3.3809 (18)	3.8062 (18)
Pt2—Sr1^iv	3.5941 (14)	3.3809 (18)	3.8062 (18)
Pt2—As1^vi	2.4526 (15)	2.4505 (15)	2.4548 (15)
Pt2—As1^xi	2.4526 (15)	2.4505 (15)	2.4548 (15)
Pt3—Pt4	2.8818 (7)	2.8798 (7)	2.8838 (7)
Pt3—Pt4^xii	2.8945 (7)	2.8929 (7)	2.8961 (7)
Pt3—Pt5	2.599 (4)	2.419 (5)	2.713 (5)
Pt3—Pt5^xiii	2.597 (4)	2.416 (5)	2.717 (5)
Pt3—Pt5^xiv	2.596 (4)	2.416 (5)	2.717 (5)
Pt3—Pt5^xv	2.600 (4)	2.419 (5)	2.713 (5)
Pt3—Sr1^ix	3.4556 (17)	3.386 (3)	3.528 (3)
Pt3—Sr1ⁱⁱ	3.5054 (17)	3.433 (3)	3.581 (3)
Pt3—Sr1^xvi	3.4548 (17)	3.386 (3)	3.528 (3)
Pt3—Sr1^v	3.5063 (17)	3.433 (3)	3.581 (3)
Pt3—As1^vi	2.4570 (12)	2.4556 (12)	2.4584 (12)
Pt4—Pt4^xii	2.8550 (7)	2.8490 (8)	2.8608 (8)
Pt4—Pt4^xvii	2.8549 (7)	2.8491 (8)	2.8608 (8)
Pt4—Pt5	2.674 (5)	2.597 (8)	2.792 (8)
Pt4—Pt5^xvii	2.619 (6)	2.571 (7)	2.650 (7)
Pt4—Pt5^xiii	2.576 (6)	2.539 (7)	2.601 (7)
Pt4—Pt5^xviii	2.675 (5)	2.585 (8)	2.820 (8)
Pt4—Pt5^xix	2.675 (5)	2.585 (8)	2.820 (8)
Pt4—Pt5^xiv	2.576 (6)	2.539 (7)	2.601 (7)
Pt4—Pt5^xx	2.620 (6)	2.571 (7)	2.650 (7)
Pt4—Pt5^xv	2.675 (5)	2.597 (8)	2.792 (8)
Pt4—Sr1ⁱⁱ	3.368 (2)	3.273 (3)	3.463 (3)
Pt4—Sr1ⁱ	3.404 (2)	3.324 (3)	3.483 (3)
Pt4—Sr1^xxi	3.404 (2)	3.324 (3)	3.483 (3)
Pt4—Sr1^v	3.370 (2)	3.273 (3)	3.463 (3)
Pt5—Pt5^xix	3.339 (15)	3.315 (15)	3.354 (15)
Pt5—Pt5^xxii	3.231 (12)	3.058 (14)	3.392 (14)
Pt5—Pt5^xx	3.223 (12)	3.062 (14)	3.395 (14)
Pt5—Sr1ⁱ	3.205 (6)	3.107 (8)	3.390 (8)
Pt5—Sr1^xvi	3.213 (8)	2.987 (12)	3.309 (12)
Pt5—Sr1^v	3.129 (8)	3.070 (13)	3.230 (13)
Sr1—As1^xxiii	3.280 (2)	3.210 (3)	3.355 (3)
Sr1—As1^xxiv	3.282 (2)	3.210 (3)	3.355 (3)

Pt2—Pt1—Pt2ⁱ	91.63 (2)	91.55 (2)	91.71 (2)
Pt2—Pt1—Pt3	60.90 (2)	60.42 (2)	61.44 (3)
Pt2—Pt1—Pt3ⁱ	60.90 (2)	60.42 (2)	61.44 (3)
Pt2—Pt1—Sr1ⁱⁱ	75.226 (13)	70.680 (18)	79.717 (17)
Pt2—Pt1—Sr1ⁱⁱⁱ	131.70 (3)	130.77 (3)	132.61 (3)
Pt2—Pt1—Sr1^iv	75.243 (13)	70.680 (18)	79.717 (17)
Pt2—Pt1—Sr1^v	131.71 (3)	130.77 (3)	132.61 (3)
Pt2—Pt1—As1^vi	45.814 (11)	45.776 (11)	45.853 (11)
Pt2—Pt1—As1	134.186 (11)	134.147 (11)	134.224 (11)
Pt2ⁱ—Pt1—Pt3	60.90 (2)	60.42 (2)	61.44 (3)
Pt2ⁱ—Pt1—Pt3ⁱ	60.90 (2)	60.42 (2)	61.44 (3)
Pt2ⁱ—Pt1—Sr1ⁱⁱ	131.70 (3)	130.77 (3)	132.61 (3)
Pt2ⁱ—Pt1—Sr1ⁱⁱⁱ	75.226 (13)	70.680 (18)	79.717 (17)
Pt2ⁱ—Pt1—Sr1^iv	131.71 (3)	130.77 (3)	132.61 (3)
Pt2ⁱ—Pt1—Sr1^v	75.243 (13)	70.680 (18)	79.717 (17)
Pt2ⁱ—Pt1—As1^vi	45.814 (11)	45.776 (11)	45.853 (11)
Pt2ⁱ—Pt1—As1	134.186 (11)	134.147 (11)	134.224 (11)
Pt3—Pt1—Pt3ⁱ	91.50 (3)	91.45 (3)	91.55 (3)
Pt3—Pt1—Sr1ⁱⁱ	72.52 (3)	71.54 (3)	73.51 (3)
Pt3—Pt1—Sr1ⁱⁱⁱ	135.43 (3)	131.25 (2)	139.61 (2)
Pt3—Pt1—Sr1^iv	135.45 (3)	131.25 (2)	139.61 (2)
Pt3—Pt1—Sr1^v	72.53 (3)	71.54 (3)	73.51 (3)
Pt3—Pt1—As1^vi	45.749 (15)	45.725 (15)	45.773 (15)
Pt3—Pt1—As1	134.251 (15)	134.227 (15)	134.275 (15)
Pt3ⁱ—Pt1—Sr1ⁱⁱ	135.43 (3)	131.25 (2)	139.61 (2)
Pt3ⁱ—Pt1—Sr1ⁱⁱⁱ	72.52 (3)	71.54 (3)	73.51 (3)
Pt3ⁱ—Pt1—Sr1^iv	72.53 (3)	71.54 (3)	73.51 (3)
Pt3ⁱ—Pt1—Sr1^v	135.45 (3)	131.25 (2)	139.61 (2)
Pt3ⁱ—Pt1—As1^vi	45.749 (15)	45.725 (15)	45.773 (15)
Pt3ⁱ—Pt1—As1	134.251 (15)	134.227 (15)	134.275 (15)
Sr1ⁱⁱ—Pt1—Sr1ⁱⁱⁱ	145.72 (3)	140.03 (4)	151.46 (4)
Sr1ⁱⁱ—Pt1—Sr1^iv	90.15 (4)	90.07 (4)	90.23 (5)
Sr1ⁱⁱ—Pt1—Sr1^v	79.98 (4)	79.89 (3)	80.07 (6)
Sr1ⁱⁱ—Pt1—As1^vi	107.14 (2)	104.27 (4)	109.98 (4)
Sr1ⁱⁱ—Pt1—As1	72.86 (2)	70.02 (4)	75.73 (4)
Sr1ⁱⁱⁱ—Pt1—Sr1^iv	79.98 (4)	79.89 (3)	80.07 (6)
Sr1ⁱⁱⁱ—Pt1—Sr1^v	90.15 (4)	90.07 (4)	90.23 (5)
Sr1ⁱⁱⁱ—Pt1—As1^vi	107.14 (2)	104.27 (4)	109.98 (4)
Sr1ⁱⁱⁱ—Pt1—As1	72.86 (2)	70.02 (4)	75.73 (4)
Sr1^iv—Pt1—Sr1^v	145.69 (3)	140.03 (4)	151.46 (4)
Sr1^iv—Pt1—As1^vi	107.16 (2)	104.27 (4)	109.98 (4)
Sr1^iv—Pt1—As1	72.84 (2)	70.02 (4)	75.73 (4)
Sr1^v—Pt1—As1^vi	107.16 (2)	104.27 (4)	109.98 (4)
Sr1^v—Pt1—As1	72.84 (2)	70.02 (4)	75.73 (4)
As1^vi—Pt1—As1	180.0 (5)	180.0 (5)	180.0 (5)
Pt1—Pt2—Pt1^vii	176.20 (4)	173.97 (4)	180.0 (5)
Pt1—Pt2—Pt3	60.268 (14)	59.974 (16)	60.500 (15)
Pt1—Pt2—Pt3ⁱ	60.267 (14)	59.974 (16)	60.500 (15)
Pt1—Pt2—Pt3^vii	119.63 (2)	114.89 (3)	124.21 (3)
Pt1—Pt2—Pt3^viii	119.63 (2)	114.89 (3)	124.21 (3)
Pt1—Pt2—Sr1^ix	123.55 (2)	121.21 (3)	125.86 (3)
Pt1—Pt2—Sr1ⁱⁱ	56.441 (17)	54.359 (17)	58.53 (2)
Pt1—Pt2—Sr1^x	123.55 (2)	121.21 (3)	125.86 (3)
Pt1—Pt2—Sr1^iv	56.439 (17)	54.359 (17)	58.53 (2)
Pt1—Pt2—As1^vi	79.94 (4)	79.86 (4)	80.01 (4)
Pt1—Pt2—As1^xi	99.88 (4)	99.77 (4)	99.99 (4)
Pt1^vii—Pt2—Pt3	119.63 (2)	114.89 (3)	124.21 (3)
Pt1^vii—Pt2—Pt3ⁱ	119.63 (2)	114.89 (3)	124.21 (3)
Pt1^vii—Pt2—Pt3^vii	60.267 (14)	59.974 (16)	60.500 (15)
Pt1^vii—Pt2—Pt3^viii	60.268 (14)	59.974 (16)	60.500 (15)
Pt1^vii—Pt2—Sr1^ix	56.439 (17)	54.359 (17)	58.53 (2)
Pt1^vii—Pt2—Sr1ⁱⁱ	123.55 (2)	121.21 (3)	125.86 (3)
Pt1^vii—Pt2—Sr1^x	56.441 (17)	54.359 (17)	58.53 (2)
Pt1^vii—Pt2—Sr1^iv	123.55 (2)	121.21 (3)	125.86 (3)
Pt1^vii—Pt2—As1^vi	99.88 (4)	99.77 (4)	99.99 (4)
Pt1^vii—Pt2—As1^xi	79.94 (4)	79.86 (4)	80.01 (4)
Pt3—Pt2—Pt3ⁱ	90.77 (2)	90.743 (19)	90.80 (3)
Pt3—Pt2—Pt3^vii	89.23 (3)	81.73 (3)	96.79 (4)
Pt3—Pt2—Pt3^viii	175.25 (4)	172.47 (4)	180.0 (5)
Pt3—Pt2—Sr1^ix	63.75 (2)	61.84 (3)	65.72 (3)
Pt3—Pt2—Sr1ⁱⁱ	64.85 (2)	62.94 (3)	66.82 (3)
Pt3—Pt2—Sr1^x	115.14 (2)	113.468 (18)	116.73 (2)
Pt3—Pt2—Sr1^iv	116.24 (2)	114.552 (18)	117.84 (2)
Pt3—Pt2—As1^vi	54.81 (2)	54.48 (2)	55.09 (2)
Pt3—Pt2—As1^xi	125.09 (3)	119.41 (4)	130.64 (4)
Pt3ⁱ—Pt2—Pt3^vii	175.25 (4)	172.47 (4)	180.0 (5)
Pt3ⁱ—Pt2—Pt3^viii	89.23 (3)	81.73 (3)	96.79 (4)
Pt3ⁱ—Pt2—Sr1^ix	115.14 (2)	113.468 (18)	116.73 (2)
Pt3ⁱ—Pt2—Sr1ⁱⁱ	116.24 (2)	114.552 (18)	117.84 (2)
Pt3ⁱ—Pt2—Sr1^x	63.75 (2)	61.84 (3)	65.72 (3)
Pt3ⁱ—Pt2—Sr1^iv	64.85 (2)	62.94 (3)	66.82 (3)
Pt3ⁱ—Pt2—As1^vi	54.81 (2)	54.48 (2)	55.09 (2)
Pt3ⁱ—Pt2—As1^xi	125.09 (3)	119.41 (4)	130.64 (4)
Pt3^vii—Pt2—Pt3^viii	90.77 (2)	90.743 (19)	90.80 (3)
Pt3^vii—Pt2—Sr1^ix	64.85 (2)	62.94 (3)	66.82 (3)
Pt3^vii—Pt2—Sr1ⁱⁱ	63.75 (2)	61.84 (3)	65.72 (3)
Pt3^vii—Pt2—Sr1^x	116.24 (2)	114.552 (18)	117.84 (2)
Pt3^vii—Pt2—Sr1^iv	115.14 (2)	113.468 (18)	116.73 (2)
Pt3^vii—Pt2—As1^vi	125.09 (3)	119.41 (4)	130.64 (4)
Pt3^vii—Pt2—As1^xi	54.81 (2)	54.48 (2)	55.09 (2)
Pt3^viii—Pt2—Sr1^ix	116.24 (2)	114.552 (18)	117.84 (2)
Pt3^viii—Pt2—Sr1ⁱⁱ	115.14 (2)	113.468 (18)	116.73 (2)
Pt3^viii—Pt2—Sr1^x	64.85 (2)	62.94 (3)	66.82 (3)
Pt3^viii—Pt2—Sr1^iv	63.75 (2)	61.84 (3)	65.72 (3)
Pt3^viii—Pt2—As1^vi	125.09 (3)	119.41 (4)	130.64 (4)
Pt3^viii—Pt2—As1^xi	54.81 (2)	54.48 (2)	55.09 (2)
Sr1^ix—Pt2—Sr1ⁱⁱ	104.89 (4)	104.42 (4)	105.39 (5)
Sr1^ix—Pt2—Sr1^x	75.11 (4)	75.09 (4)	75.13 (4)
Sr1^ix—Pt2—Sr1^iv	179.70 (9)	179.51 (4)	180.0 (5)
Sr1^ix—Pt2—As1^vi	62.39 (4)	60.15 (5)	64.64 (6)
Sr1^ix—Pt2—As1^xi	117.60 (4)	115.14 (6)	120.03 (6)
Sr1ⁱⁱ—Pt2—Sr1^x	179.70 (9)	179.51 (5)	180.0 (5)
Sr1ⁱⁱ—Pt2—Sr1^iv	75.11 (4)	75.09 (4)	75.13 (4)
Sr1ⁱⁱ—Pt2—As1^vi	117.60 (4)	115.14 (6)	120.03 (6)
Sr1ⁱⁱ—Pt2—As1^xi	62.39 (4)	60.15 (5)	64.64 (6)
Sr1^x—Pt2—Sr1^iv	104.89 (4)	104.42 (4)	105.39 (5)
Sr1^x—Pt2—As1^vi	62.39 (4)	60.15 (5)	64.64 (6)
Sr1^x—Pt2—As1^xi	117.60 (4)	115.14 (6)	120.03 (6)
Sr1^iv—Pt2—As1^vi	117.60 (4)	115.14 (6)	120.03 (6)
Sr1^iv—Pt2—As1^xi	62.39 (4)	60.15 (5)	64.64 (6)
As1^vi—Pt2—As1^xi	175.70 (4)	173.18 (5)	180.0 (5)
Pt1—Pt3—Pt2	58.835 (17)	58.582 (15)	59.079 (16)
Pt1—Pt3—Pt2ⁱ	58.835 (17)	58.582 (15)	59.079 (16)
Pt1—Pt3—Pt4	105.37 (2)	105.31 (2)	105.43 (2)
Pt1—Pt3—Pt4^xii	164.43 (3)	164.33 (3)	164.53 (3)
Pt1—Pt3—Pt5	114.4 (3)	113.2 (3)	116.5 (3)
Pt1—Pt3—Pt5^xiii	117.2 (3)	112.4 (3)	119.3 (3)
Pt1—Pt3—Pt5^xiv	117.2 (3)	112.4 (3)	119.3 (3)
Pt1—Pt3—Pt5^xv	114.4 (3)	113.2 (3)	116.5 (3)
Pt1—Pt3—Sr1^ix	127.21 (4)	123.94 (4)	130.27 (4)
Pt1—Pt3—Sr1ⁱⁱ	57.44 (3)	57.33 (4)	57.56 (3)
Pt1—Pt3—Sr1^xvi	127.19 (4)	123.94 (4)	130.27 (4)
Pt1—Pt3—Sr1^v	57.44 (3)	57.33 (4)	57.56 (3)
Pt1—Pt3—As1^vi	79.05 (4)	79.00 (4)	79.10 (4)
Pt2—Pt3—Pt2ⁱ	89.21 (2)	89.19 (2)	89.24 (3)
Pt2—Pt3—Pt4	127.46 (5)	124.20 (5)	130.71 (5)
Pt2—Pt3—Pt4^xii	129.00 (5)	126.37 (5)	131.55 (5)
Pt2—Pt3—Pt5	171.81 (16)	170.20 (7)	173.4 (2)
Pt2—Pt3—Pt5^xiii	172.55 (10)	169.53 (13)	174.56 (9)
Pt2—Pt3—Pt5^xiv	83.65 (6)	81.04 (5)	85.48 (6)
Pt2—Pt3—Pt5^xv	83.50 (6)	81.09 (5)	85.35 (6)
Pt2—Pt3—Sr1^ix	68.88 (3)	65.21 (3)	72.40 (3)
Pt2—Pt3—Sr1ⁱⁱ	68.10 (3)	64.51 (3)	71.56 (3)
Pt2—Pt3—Sr1^xvi	116.60 (3)	116.01 (3)	117.02 (3)
Pt2—Pt3—Sr1^v	115.06 (3)	114.42 (3)	115.54 (3)
Pt2—Pt3—As1^vi	54.67 (2)	54.36 (2)	54.97 (2)
Pt2ⁱ—Pt3—Pt4	127.51 (5)	124.20 (5)	130.71 (5)
Pt2ⁱ—Pt3—Pt4^xii	128.96 (5)	126.37 (5)	131.55 (5)
Pt2ⁱ—Pt3—Pt5	83.53 (6)	81.09 (5)	85.35 (6)
Pt2ⁱ—Pt3—Pt5^xiii	83.61 (6)	81.04 (5)	85.48 (6)
Pt2ⁱ—Pt3—Pt5^xiv	172.58 (10)	169.53 (13)	174.56 (9)
Pt2ⁱ—Pt3—Pt5^xv	171.80 (16)	170.20 (7)	173.4 (2)
Pt2ⁱ—Pt3—Sr1^ix	116.60 (3)	116.01 (3)	117.02 (3)
Pt2ⁱ—Pt3—Sr1ⁱⁱ	115.06 (3)	114.42 (3)	115.54 (3)
Pt2ⁱ—Pt3—Sr1^xvi	68.87 (3)	65.21 (3)	72.40 (3)
Pt2ⁱ—Pt3—Sr1^v	68.11 (3)	64.51 (3)	71.56 (3)
Pt2ⁱ—Pt3—As1^vi	54.67 (2)	54.36 (2)	54.97 (2)
Pt4—Pt3—Pt4^xii	59.241 (19)	59.131 (18)	59.349 (19)
Pt4—Pt3—Pt5	58.1 (2)	56.95 (19)	59.8 (2)
Pt4—Pt3—Pt5^xiii	55.8 (2)	54.92 (19)	56.6 (2)
Pt4—Pt3—Pt5^xiv	55.8 (2)	54.92 (19)	56.6 (2)
Pt4—Pt3—Pt5^xv	58.1 (2)	56.95 (19)	59.8 (2)
Pt4—Pt3—Sr1^ix	111.62 (4)	109.52 (5)	113.72 (5)
Pt4—Pt3—Sr1ⁱⁱ	62.76 (4)	60.91 (4)	64.75 (4)
Pt4—Pt3—Sr1^xvi	111.66 (4)	109.52 (5)	113.72 (5)
Pt4—Pt3—Sr1^v	62.78 (4)	60.91 (4)	64.75 (4)
Pt4—Pt3—As1^vi	174.96 (5)	174.41 (5)	175.54 (4)
Pt4^xii—Pt3—Pt5	56.6 (2)	55.83 (19)	57.1 (2)
Pt4^xii—Pt3—Pt5^xiii	57.9 (2)	56.63 (19)	60.2 (2)
Pt4^xii—Pt3—Pt5^xiv	57.9 (2)	56.63 (19)	60.2 (2)
Pt4^xii—Pt3—Pt5^xv	56.6 (2)	55.83 (19)	57.1 (2)
Pt4^xii—Pt3—Sr1^ix	64.13 (4)	62.28 (4)	66.11 (4)
Pt4^xii—Pt3—Sr1ⁱⁱ	110.65 (4)	109.02 (5)	112.23 (5)
Pt4^xii—Pt3—Sr1^xvi	64.12 (4)	62.28 (4)	66.11 (4)
Pt4^xii—Pt3—Sr1^v	110.62 (4)	109.02 (5)	112.23 (5)
Pt4^xii—Pt3—As1^vi	116.40 (4)	116.34 (4)	116.45 (4)
Pt5—Pt3—Pt5^xiv	102.16 (13)	101.64 (14)	102.93 (11)
Pt5—Pt3—Sr1^ix	115.74 (19)	110.5 (3)	118.8 (2)
Pt5—Pt3—Sr1ⁱⁱ	112.02 (18)	110.12 (14)	114.3 (3)
Pt5—Pt3—Sr1^xvi	63.03 (19)	57.3 (3)	65.33 (14)
Pt5—Pt3—Sr1^v	59.07 (19)	57.54 (14)	61.6 (3)
Pt5—Pt3—As1^vi	122.12 (16)	117.6 (2)	124.04 (14)
Pt5^xiii—Pt3—Pt5^xv	102.18 (13)	101.64 (14)	102.93 (11)
Pt5^xiii—Pt3—Sr1^ix	113.71 (18)	111.76 (14)	115.8 (3)
Pt5^xiii—Pt3—Sr1^xvi	59.96 (19)	58.40 (14)	62.3 (3)
Pt5^xiii—Pt3—Sr1^v	62.21 (19)	56.6 (3)	64.58 (14)
Pt5^xiii—Pt3—As1^vi	119.91 (16)	119.05 (14)	121.1 (2)
Pt5^xiv—Pt3—Sr1^ix	59.93 (19)	58.40 (14)	62.3 (3)
Pt5^xiv—Pt3—Sr1ⁱⁱ	62.28 (19)	56.6 (3)	64.58 (14)
Pt5^xiv—Pt3—Sr1^xvi	113.67 (18)	111.76 (14)	115.8 (3)
Pt5^xiv—Pt3—As1^vi	119.89 (16)	119.05 (14)	121.1 (2)
Pt5^xv—Pt3—Sr1^ix	62.96 (19)	57.3 (3)	65.33 (14)
Pt5^xv—Pt3—Sr1ⁱⁱ	59.10 (19)	57.54 (14)	61.6 (3)
Pt5^xv—Pt3—Sr1^xvi	115.68 (19)	110.5 (3)	118.8 (2)
Pt5^xv—Pt3—Sr1^v	112.06 (18)	110.12 (14)	114.3 (3)
Pt5^xv—Pt3—As1^vi	122.06 (16)	117.6 (2)	124.04 (14)
Sr1^ix—Pt3—Sr1ⁱⁱ	109.92 (4)	103.80 (5)	115.94 (5)
Sr1^ix—Pt3—Sr1^xvi	70.36 (3)	70.298 (10)	70.42 (5)
Sr1^ix—Pt3—Sr1^v	172.87 (5)	171.19 (5)	175.07 (5)
Sr1^ix—Pt3—As1^vi	64.87 (4)	64.35 (4)	65.36 (4)
Sr1ⁱⁱ—Pt3—Sr1^xvi	172.88 (5)	171.19 (5)	175.07 (5)
Sr1ⁱⁱ—Pt3—Sr1^v	69.19 (3)	69.134 (10)	69.26 (5)
Sr1ⁱⁱ—Pt3—As1^vi	120.57 (5)	117.68 (5)	123.28 (4)
Sr1^xvi—Pt3—Sr1^v	109.92 (4)	103.80 (5)	115.94 (5)
Sr1^xvi—Pt3—As1^vi	64.86 (4)	64.35 (4)	65.36 (4)
Sr1^v—Pt3—As1^vi	120.58 (5)	117.68 (5)	123.28 (4)
Pt3—Pt4—Pt3^xvii	176.31 (5)	174.71 (4)	178.43 (3)
Pt3—Pt4—Pt4^xii	60.601 (18)	60.522 (18)	60.681 (18)
Pt3—Pt4—Pt4^xvii	121.25 (2)	121.08 (2)	121.43 (2)
Pt3—Pt4—Pt5	55.60 (10)	52.10 (10)	57.11 (9)
Pt3—Pt4—Pt5^xvii	125.32 (10)	118.48 (12)	132.80 (7)
Pt3—Pt4—Pt5^xiii	56.49 (9)	52.38 (8)	59.33 (11)
Pt3—Pt4—Pt5^xviii	122.40 (11)	119.24 (10)	129.59 (11)
Pt3—Pt4—Pt5^xix	122.40 (11)	119.24 (10)	129.59 (11)
Pt3—Pt4—Pt5^xiv	56.47 (9)	52.38 (8)	59.33 (11)
Pt3—Pt4—Pt5^xx	125.11 (10)	118.48 (12)	132.80 (7)
Pt3—Pt4—Pt5^xv	55.61 (10)	52.10 (10)	57.11 (9)
Pt3—Pt4—Sr1ⁱⁱ	67.71 (3)	66.01 (3)	69.46 (3)
Pt3—Pt4—Sr1ⁱ	112.67 (4)	111.00 (3)	114.38 (3)
Pt3—Pt4—Sr1^xxi	112.68 (4)	111.00 (3)	114.38 (3)
Pt3—Pt4—Sr1^v	67.71 (3)	66.01 (3)	69.46 (3)
Pt3^xvii—Pt4—Pt4^xii	117.68 (2)	117.52 (2)	117.84 (2)
Pt3^xvii—Pt4—Pt4^xvii	60.159 (18)	60.090 (18)	60.227 (18)
Pt3^xvii—Pt4—Pt5	120.36 (11)	117.72 (11)	126.90 (11)
Pt3^xvii—Pt4—Pt5^xvii	55.96 (8)	52.05 (7)	58.59 (10)
Pt3^xvii—Pt4—Pt5^xiii	124.73 (9)	118.04 (12)	131.52 (7)
Pt3^xvii—Pt4—Pt5^xviii	55.41 (9)	52.00 (9)	56.80 (10)
Pt3^xvii—Pt4—Pt5^xix	55.41 (9)	52.00 (9)	56.80 (10)
Pt3^xvii—Pt4—Pt5^xiv	124.79 (9)	118.04 (12)	131.52 (7)
Pt3^xvii—Pt4—Pt5^xx	56.04 (8)	52.05 (7)	58.59 (10)
Pt3^xvii—Pt4—Pt5^xv	120.35 (11)	117.72 (11)	126.90 (11)
Pt3^xvii—Pt4—Sr1ⁱⁱ	113.37 (4)	111.25 (4)	115.54 (4)
Pt3^xvii—Pt4—Sr1ⁱ	65.95 (3)	64.13 (3)	67.84 (3)
Pt3^xvii—Pt4—Sr1^xxi	65.98 (3)	64.13 (3)	67.84 (3)
Pt3^xvii—Pt4—Sr1^v	113.33 (4)	111.25 (4)	115.54 (4)
Pt4^xii—Pt4—Pt4^xvii	175.51 (6)	173.61 (6)	177.98 (2)
Pt4^xii—Pt4—Pt5	56.4 (3)	55.5 (3)	57.3 (3)
Pt4^xii—Pt4—Pt5^xvii	122.0 (3)	114.4 (3)	127.1 (3)
Pt4^xii—Pt4—Pt5^xiii	58.7 (3)	56.8 (3)	62.3 (3)
Pt4^xii—Pt4—Pt5^xviii	120.4 (3)	118.5 (3)	124.3 (3)
Pt4^xii—Pt4—Pt5^xix	120.4 (3)	118.5 (3)	124.3 (3)
Pt4^xii—Pt4—Pt5^xiv	58.6 (3)	56.8 (3)	62.3 (3)
Pt4^xii—Pt4—Pt5^xx	121.7 (3)	114.4 (3)	127.1 (3)
Pt4^xii—Pt4—Pt5^xv	56.4 (3)	55.5 (3)	57.3 (3)
Pt4^xii—Pt4—Sr1ⁱⁱ	115.72 (3)	111.45 (3)	119.81 (3)
Pt4^xii—Pt4—Sr1ⁱ	64.43 (3)	63.49 (2)	65.54 (2)
Pt4^xii—Pt4—Sr1^xxi	64.43 (3)	63.49 (2)	65.54 (2)
Pt4^xii—Pt4—Sr1^v	115.66 (3)	111.45 (3)	119.81 (3)
Pt4^xvii—Pt4—Pt5	120.3 (3)	118.2 (3)	124.7 (3)
Pt4^xvii—Pt4—Pt5^xvii	58.3 (3)	56.8 (3)	61.1 (3)
Pt4^xvii—Pt4—Pt5^xiii	124.1 (3)	115.5 (3)	129.4 (3)
Pt4^xvii—Pt4—Pt5^xviii	55.4 (3)	54.2 (3)	56.3 (3)
Pt4^xvii—Pt4—Pt5^xix	55.4 (3)	54.2 (3)	56.3 (3)
Pt4^xvii—Pt4—Pt5^xiv	124.2 (3)	115.5 (3)	129.4 (3)
Pt4^xvii—Pt4—Pt5^xx	58.4 (3)	56.8 (3)	61.1 (3)
Pt4^xvii—Pt4—Pt5^xv	120.3 (3)	118.2 (3)	124.7 (3)
Pt4^xvii—Pt4—Sr1ⁱⁱ	65.69 (3)	65.31 (3)	66.33 (2)
Pt4^xvii—Pt4—Sr1ⁱ	113.87 (3)	109.32 (3)	118.31 (3)
Pt4^xvii—Pt4—Sr1^xxi	113.92 (3)	109.32 (3)	118.31 (3)
Pt4^xvii—Pt4—Sr1^v	65.70 (3)	65.31 (3)	66.33 (2)
Pt5—Pt4—Pt5^xvii	170.33 (13)	170.20 (13)	170.46 (12)
Pt5—Pt4—Pt5^xviii	178.60 (13)	177.93 (13)	179.28 (13)
Pt5—Pt4—Pt5^xix	74.2 (3)	73.8 (3)	74.4 (3)
Pt5—Pt4—Pt5^xiv	99.8 (2)	98.5 (3)	100.4 (2)
Pt5—Pt4—Pt5^xx	75.7 (3)	71.3 (3)	80.6 (3)
Pt5—Pt4—Sr1ⁱⁱ	115.94 (13)	112.53 (12)	119.27 (9)
Pt5—Pt4—Sr1ⁱ	61.83 (13)	58.11 (7)	67.86 (12)
Pt5—Pt4—Sr1^xxi	115.24 (16)	111.8 (2)	118.60 (19)
Pt5—Pt4—Sr1^v	59.87 (17)	58.54 (15)	61.6 (2)
Pt5^xvii—Pt4—Pt5^xiii	174.7 (3)	171.0 (4)	179.1 (3)
Pt5^xvii—Pt4—Pt5^xix	98.9 (3)	97.5 (3)	99.6 (3)
Pt5^xvii—Pt4—Pt5^xv	76.0 (3)	71.3 (3)	80.6 (3)
Pt5^xvii—Pt4—Sr1ⁱⁱ	62.96 (13)	59.59 (9)	69.02 (12)
Pt5^xvii—Pt4—Sr1ⁱ	116.83 (13)	113.05 (11)	118.61 (14)
Pt5^xvii—Pt4—Sr1^xxi	63.65 (17)	57.4 (2)	66.39 (19)
Pt5^xvii—Pt4—Sr1^v	117.79 (17)	116.35 (14)	119.59 (17)
Pt5^xiii—Pt4—Pt5^xviii	171.69 (17)	171.57 (17)	171.81 (17)
Pt5^xiii—Pt4—Pt5^xix	77.0 (3)	72.1 (3)	81.7 (3)
Pt5^xiii—Pt4—Pt5^xv	99.8 (3)	98.5 (3)	100.4 (3)
Pt5^xiii—Pt4—Sr1ⁱⁱ	118.63 (13)	114.74 (11)	120.44 (14)
Pt5^xiii—Pt4—Sr1ⁱ	63.02 (14)	59.68 (9)	68.72 (12)
Pt5^xiii—Pt4—Sr1^xxi	117.23 (17)	115.77 (15)	119.06 (18)
Pt5^xiii—Pt4—Sr1^v	64.90 (17)	58.5 (2)	67.58 (14)
Pt5^xviii—Pt4—Pt5^xiv	77.0 (3)	72.1 (3)	81.7 (3)
Pt5^xviii—Pt4—Pt5^xx	98.9 (2)	97.5 (3)	99.6 (2)
Pt5^xviii—Pt4—Pt5^xv	74.2 (3)	73.8 (3)	74.4 (3)
Pt5^xviii—Pt4—Sr1ⁱⁱ	62.53 (13)	58.23 (7)	69.01 (12)
Pt5^xviii—Pt4—Sr1ⁱ	114.51 (13)	111.06 (12)	117.64 (9)
Pt5^xviii—Pt4—Sr1^xxi	59.62 (17)	58.33 (15)	61.46 (19)
Pt5^xviii—Pt4—Sr1^v	115.94 (17)	112.4 (2)	119.27 (19)
Pt5^xix—Pt4—Pt5^xiv	171.69 (17)	171.57 (17)	171.81 (16)
Pt5^xix—Pt4—Pt5^xv	178.60 (13)	177.93 (12)	179.28 (14)
Pt5^xix—Pt4—Sr1ⁱⁱ	115.94 (17)	112.4 (2)	119.27 (19)
Pt5^xix—Pt4—Sr1ⁱ	59.62 (17)	58.33 (15)	61.46 (19)
Pt5^xix—Pt4—Sr1^xxi	114.51 (13)	111.06 (12)	117.64 (9)
Pt5^xix—Pt4—Sr1^v	62.53 (13)	58.23 (7)	69.01 (12)
Pt5^xiv—Pt4—Pt5^xx	174.5 (3)	171.0 (3)	179.1 (3)
Pt5^xiv—Pt4—Sr1ⁱⁱ	64.98 (17)	58.5 (2)	67.58 (14)
Pt5^xiv—Pt4—Sr1ⁱ	117.21 (17)	115.77 (15)	119.06 (18)
Pt5^xiv—Pt4—Sr1^xxi	63.04 (14)	59.68 (9)	68.72 (12)
Pt5^xiv—Pt4—Sr1^v	118.64 (14)	114.74 (11)	120.44 (14)
Pt5^xx—Pt4—Pt5^xv	170.33 (14)	170.20 (14)	170.46 (14)
Pt5^xx—Pt4—Sr1ⁱⁱ	117.80 (17)	116.35 (14)	119.59 (17)
Pt5^xx—Pt4—Sr1ⁱ	63.46 (17)	57.4 (2)	66.39 (19)
Pt5^xx—Pt4—Sr1^xxi	116.83 (13)	113.05 (11)	118.61 (14)
Pt5^xx—Pt4—Sr1^v	62.86 (13)	59.59 (9)	69.02 (12)
Pt5^xv—Pt4—Sr1ⁱⁱ	59.90 (17)	58.54 (15)	61.6 (2)
Pt5^xv—Pt4—Sr1ⁱ	115.20 (16)	111.8 (2)	118.60 (19)
Pt5^xv—Pt4—Sr1^xxi	61.80 (13)	58.11 (7)	67.86 (12)
Pt5^xv—Pt4—Sr1^v	115.96 (13)	112.53 (12)	119.27 (9)
Sr1ⁱⁱ—Pt4—Sr1ⁱ	174.98 (5)	171.92 (3)	179.61 (6)
Sr1ⁱⁱ—Pt4—Sr1^xxi	108.07 (5)	100.72 (4)	115.62 (4)
Sr1ⁱⁱ—Pt4—Sr1^v	72.42 (4)	72.26 (3)	72.59 (5)
Sr1ⁱ—Pt4—Sr1^xxi	71.58 (4)	71.44 (3)	71.72 (5)
Sr1ⁱ—Pt4—Sr1^v	107.97 (5)	100.72 (4)	115.62 (4)
Sr1^xxi—Pt4—Sr1^v	174.97 (5)	171.92 (4)	179.61 (6)
Pt3—Pt5—Pt3^xiii	101.8 (2)	100.4 (2)	104.63 (19)
Pt3—Pt5—Pt4	66.32 (8)	63.09 (12)	69.99 (9)
Pt3—Pt5—Pt4^xii	67.40 (9)	65.55 (10)	70.82 (12)
Pt3—Pt5—Pt4^xiii	139.1 (3)	135.2 (3)	146.6 (5)
Pt3—Pt5—Pt4^xxv	148.2 (3)	140.3 (5)	151.2 (3)
Pt3—Pt5—Pt5^xix	107.8 (3)	106.0 (4)	110.1 (2)
Pt3—Pt5—Pt5^xxii	110.2 (3)	107.8 (2)	112.1 (4)
Pt3—Pt5—Pt5^xx	113.1 (2)	112.2 (3)	114.12 (18)
Pt3—Pt5—Sr1ⁱ	128.97 (12)	127.58 (11)	129.62 (12)
Pt3—Pt5—Sr1^xvi	70.82 (17)	68.94 (15)	72.8 (2)
Pt3—Pt5—Sr1^v	75.46 (18)	70.7 (2)	78.6 (2)
Pt3^xiii—Pt5—Pt4	146.4 (3)	138.4 (5)	149.4 (4)
Pt3^xiii—Pt5—Pt4^xii	141.3 (3)	137.5 (3)	148.6 (5)
Pt3^xiii—Pt5—Pt4^xiii	67.76 (9)	65.75 (9)	70.98 (12)
Pt3^xiii—Pt5—Pt4^xxv	66.73 (8)	63.01 (12)	70.65 (10)
Pt3^xiii—Pt5—Pt5^xix	106.5 (3)	104.7 (4)	108.8 (2)
Pt3^xiii—Pt5—Pt5^xxii	111.4 (3)	109.0 (2)	113.3 (4)
Pt3^xiii—Pt5—Pt5^xx	111.8 (2)	110.9 (3)	112.92 (18)
Pt3^xiii—Pt5—Sr1ⁱ	128.97 (12)	127.61 (11)	129.67 (12)
Pt3^xiii—Pt5—Sr1^xvi	72.04 (17)	70.14 (15)	74.1 (2)
Pt3^xiii—Pt5—Sr1^v	74.15 (17)	69.5 (2)	77.2 (2)
Pt4—Pt5—Pt4^xii	65.33 (7)	63.33 (5)	67.07 (7)
Pt4—Pt5—Pt4^xiii	141.4 (2)	133.2 (2)	146.52 (13)
Pt4—Pt5—Pt4^xxv	106.0 (3)	99.2 (3)	110.1 (2)
Pt4—Pt5—Pt5^xix	53.13 (18)	51.7 (2)	54.78 (15)
Pt4—Pt5—Pt5^xxii	106.51 (17)	104.72 (18)	108.31 (17)
Pt4—Pt5—Pt5^xx	52.37 (13)	50.34 (16)	54.42 (12)
Pt4—Pt5—Sr1ⁱ	70.90 (14)	66.92 (11)	72.62 (14)
Pt4—Pt5—Sr1^xvi	126.30 (15)	124.44 (13)	128.49 (19)
Pt4—Pt5—Sr1^v	72.47 (19)	68.9 (3)	74.29 (14)
Pt4^xii—Pt5—Pt4^xiii	95.7 (3)	87.7 (3)	108.7 (4)
Pt4^xii—Pt5—Pt4^xxv	139.6 (2)	131.0 (2)	144.76 (13)
Pt4^xii—Pt5—Pt5^xix	108.03 (19)	106.3 (2)	110.15 (18)
Pt4^xii—Pt5—Pt5^xxii	51.85 (17)	49.10 (13)	54.4 (2)
Pt4^xii—Pt5—Pt5^xx	107.0 (2)	105.87 (19)	108.4 (2)
Pt4^xii—Pt5—Sr1ⁱ	70.44 (14)	65.89 (11)	73.60 (10)
Pt4^xii—Pt5—Sr1^xvi	69.45 (19)	67.26 (13)	74.9 (3)
Pt4^xii—Pt5—Sr1^v	131.89 (15)	125.6 (2)	135.26 (18)
Pt4^xiii—Pt5—Pt4^xxv	65.96 (7)	63.50 (6)	67.62 (7)
Pt4^xiii—Pt5—Pt5^xix	108.88 (19)	107.1 (2)	111.06 (19)
Pt4^xiii—Pt5—Pt5^xxii	51.77 (18)	48.95 (13)	54.4 (2)
Pt4^xiii—Pt5—Pt5^xx	107.9 (2)	106.69 (19)	109.3 (2)
Pt4^xiii—Pt5—Sr1ⁱ	71.26 (14)	66.83 (12)	74.43 (10)
Pt4^xiii—Pt5—Sr1^xvi	68.50 (19)	66.27 (13)	74.0 (3)
Pt4^xiii—Pt5—Sr1^v	132.02 (15)	125.6 (2)	135.19 (18)
Pt4^xxv—Pt5—Pt5^xix	52.68 (17)	51.5 (2)	54.13 (14)
Pt4^xxv—Pt5—Pt5^xxii	105.82 (17)	104.10 (18)	107.54 (17)
Pt4^xxv—Pt5—Pt5^xx	51.35 (13)	49.27 (16)	53.47 (12)
Pt4^xxv—Pt5—Sr1ⁱ	69.70 (14)	65.54 (11)	71.48 (13)
Pt4^xxv—Pt5—Sr1^xvi	126.92 (15)	125.10 (13)	129.3 (2)
Pt4^xxv—Pt5—Sr1^v	72.95 (19)	69.6 (3)	74.74 (14)
Pt5^xix—Pt5—Pt5^xxii	117.8 (2)	117.7 (2)	118.1 (3)
Pt5^xix—Pt5—Sr1ⁱ	58.74 (18)	57.77 (19)	60.10 (18)
Pt5^xix—Pt5—Sr1^xvi	178.9 (3)	177.9 (3)	179.91 (19)
Pt5^xix—Pt5—Sr1^v	57.2 (2)	57.0 (3)	57.7 (2)
Pt5^xxii—Pt5—Sr1ⁱ	58.97 (17)	57.69 (17)	60.05 (18)
Pt5^xxii—Pt5—Sr1^xvi	63.1 (3)	61.62 (19)	64.3 (3)
Pt5^xxii—Pt5—Sr1^v	175.1 (3)	174.6 (3)	175.9 (3)
Pt5^xx—Pt5—Sr1ⁱ	56.33 (17)	56.04 (17)	56.7 (2)
Pt5^xx—Pt5—Sr1^xvi	172.0 (3)	170.8 (3)	173.3 (3)
Pt5^xx—Pt5—Sr1^v	58.90 (19)	57.0 (2)	60.7 (2)
Sr1ⁱ—Pt5—Sr1^xvi	118.5 (3)	114.1 (3)	124.4 (4)
Sr1ⁱ—Pt5—Sr1^v	116.4 (3)	113.6 (3)	118.8 (2)
Sr1^xvi—Pt5—Sr1^v	125.14 (19)	120.78 (10)	132.20 (17)
Pt1^xxiii—Sr1—Pt1^xxiv	89.85 (4)	89.18 (6)	90.68 (6)
Pt1^xxiii—Sr1—Pt2^xxiii	48.30 (2)	45.88 (3)	50.83 (3)
Pt1^xxiii—Sr1—Pt2^xxvi	78.63 (4)	75.86 (4)	81.32 (5)
Pt1^xxiii—Sr1—Pt3^xxiii	50.03 (3)	48.97 (4)	51.10 (4)
Pt1^xxiii—Sr1—Pt3^xxvi	80.48 (4)	79.73 (4)	81.26 (3)
Pt1^xxiii—Sr1—Pt3^xxvii	95.29 (4)	90.73 (5)	99.98 (5)
Pt1^xxiii—Sr1—Pt3^xxiv	124.82 (5)	121.06 (5)	128.37 (5)
Pt1^xxiii—Sr1—Pt4^xxiii	88.91 (5)	86.77 (2)	91.24 (2)
Pt1^xxiii—Sr1—Pt4ⁱ	103.80 (6)	101.22 (4)	106.56 (3)
Pt1^xxiii—Sr1—Pt4^xxiv	171.69 (5)	165.76 (8)	177.96 (7)
Pt1^xxiii—Sr1—Pt4^viii	137.90 (4)	131.83 (6)	144.12 (6)
Pt1^xxiii—Sr1—Pt5ⁱ	133.90 (15)	133.51 (14)	134.30 (16)
Pt1^xxiii—Sr1—Pt5^viii	136.18 (13)	135.58 (12)	136.92 (11)
Pt1^xxiii—Sr1—Pt5^xxviii	94.87 (11)	89.64 (9)	99.14 (14)
Pt1^xxiii—Sr1—Pt5^xxix	125.91 (9)	121.62 (10)	128.59 (10)
Pt1^xxiii—Sr1—Pt5^xxx	93.72 (11)	88.89 (10)	96.56 (11)
Pt1^xxiii—Sr1—Pt5^xxxi	127.32 (10)	122.68 (8)	130.65 (13)
Pt1^xxiii—Sr1—As1^xxiii	42.70 (4)	42.26 (4)	43.12 (4)
Pt1^xxiii—Sr1—As1^xxiv	77.78 (4)	75.97 (3)	79.59 (4)
Pt1^xxiv—Sr1—Pt2^xxiii	78.58 (4)	75.86 (4)	81.32 (5)
Pt1^xxiv—Sr1—Pt2^xxvi	48.35 (2)	45.88 (3)	50.83 (3)
Pt1^xxiv—Sr1—Pt3^xxiii	124.74 (5)	121.06 (5)	128.37 (5)
Pt1^xxiv—Sr1—Pt3^xxvi	95.39 (4)	90.73 (5)	99.98 (5)
Pt1^xxiv—Sr1—Pt3^xxvii	80.47 (4)	79.73 (4)	81.26 (3)
Pt1^xxiv—Sr1—Pt3^xxiv	50.05 (3)	48.97 (4)	51.10 (4)
Pt1^xxiv—Sr1—Pt4^xxiii	171.57 (5)	165.76 (8)	177.96 (7)
Pt1^xxiv—Sr1—Pt4ⁱ	138.02 (4)	131.83 (6)	144.12 (6)
Pt1^xxiv—Sr1—Pt4^xxiv	88.92 (5)	86.77 (2)	91.24 (2)
Pt1^xxiv—Sr1—Pt4^viii	103.83 (6)	101.22 (4)	106.56 (3)
Pt1^xxiv—Sr1—Pt5ⁱ	136.17 (13)	135.58 (12)	136.92 (11)
Pt1^xxiv—Sr1—Pt5^viii	133.90 (15)	133.51 (14)	134.30 (16)
Pt1^xxiv—Sr1—Pt5^xxviii	127.21 (10)	122.68 (8)	130.65 (13)
Pt1^xxiv—Sr1—Pt5^xxix	93.72 (11)	88.89 (10)	96.56 (11)
Pt1^xxiv—Sr1—Pt5^xxx	125.91 (9)	121.62 (10)	128.59 (10)
Pt1^xxiv—Sr1—Pt5^xxxi	95.00 (11)	89.64 (9)	99.14 (14)
Pt1^xxiv—Sr1—As1^xxiii	77.81 (4)	75.97 (3)	79.59 (4)
Pt1^xxiv—Sr1—As1^xxiv	42.69 (4)	42.26 (4)	43.12 (4)
Pt2^xxiii—Sr1—Pt2^xxvi	104.89 (5)	104.42 (6)	105.34 (6)
Pt2^xxiii—Sr1—Pt3^xxiii	47.03 (2)	45.40 (3)	48.77 (3)
Pt2^xxiii—Sr1—Pt3^xxvi	127.98 (6)	125.96 (7)	129.97 (7)
Pt2^xxiii—Sr1—Pt3^xxvii	47.36 (2)	45.65 (3)	49.18 (3)
Pt2^xxiii—Sr1—Pt3^xxiv	128.35 (6)	126.37 (7)	130.30 (7)
Pt2^xxiii—Sr1—Pt4^xxiii	94.75 (3)	92.64 (5)	96.92 (5)
Pt2^xxiii—Sr1—Pt4ⁱ	139.06 (5)	135.02 (7)	143.25 (7)
Pt2^xxiii—Sr1—Pt4^xxiv	138.94 (6)	135.04 (6)	143.00 (6)
Pt2^xxiii—Sr1—Pt4^viii	95.21 (3)	93.15 (5)	97.31 (5)
Pt2^xxiii—Sr1—Pt5ⁱ	126.7 (3)	124.1 (3)	127.9 (3)
Pt2^xxiii—Sr1—Pt5^viii	128.4 (3)	127.1 (3)	130.6 (3)
Pt2^xxiii—Sr1—Pt5^xxviii	65.14 (13)	61.56 (11)	68.40 (16)
Pt2^xxiii—Sr1—Pt5^xxix	170.01 (15)	166.77 (13)	171.55 (16)
Pt2^xxiii—Sr1—Pt5^xxx	64.74 (14)	61.63 (12)	66.22 (14)
Pt2^xxiii—Sr1—Pt5^xxxi	169.81 (14)	166.02 (13)	173.30 (17)
Pt2^xxiii—Sr1—As1^xxiii	86.23 (5)	83.77 (5)	88.69 (5)
Pt2^xxiii—Sr1—As1^xxiv	41.48 (3)	39.47 (3)	43.61 (4)
Pt2^xxvi—Sr1—Pt3^xxiii	128.39 (6)	126.37 (7)	130.30 (7)
Pt2^xxvi—Sr1—Pt3^xxvi	47.39 (2)	45.65 (3)	49.18 (3)
Pt2^xxvi—Sr1—Pt3^xxvii	128.02 (6)	125.96 (7)	129.97 (7)
Pt2^xxvi—Sr1—Pt3^xxiv	47.07 (2)	45.40 (3)	48.77 (3)
Pt2^xxvi—Sr1—Pt4^xxiii	139.01 (6)	135.04 (6)	143.00 (6)
Pt2^xxvi—Sr1—Pt4ⁱ	95.25 (3)	93.15 (5)	97.31 (5)
Pt2^xxvi—Sr1—Pt4^xxiv	94.79 (3)	92.64 (5)	96.92 (5)
Pt2^xxvi—Sr1—Pt4^viii	139.13 (5)	135.02 (7)	143.25 (7)
Pt2^xxvi—Sr1—Pt5ⁱ	128.3 (3)	127.1 (3)	130.6 (3)
Pt2^xxvi—Sr1—Pt5^viii	126.6 (3)	124.1 (3)	127.9 (3)
Pt2^xxvi—Sr1—Pt5^xxviii	169.70 (14)	166.02 (13)	173.30 (17)
Pt2^xxvi—Sr1—Pt5^xxix	64.74 (14)	61.63 (12)	66.22 (14)
Pt2^xxvi—Sr1—Pt5^xxx	170.01 (15)	166.77 (13)	171.55 (16)
Pt2^xxvi—Sr1—Pt5^xxxi	65.24 (14)	61.56 (11)	68.40 (16)
Pt2^xxvi—Sr1—As1^xxiii	41.52 (3)	39.47 (3)	43.61 (4)
Pt2^xxvi—Sr1—As1^xxiv	86.28 (5)	83.77 (5)	88.69 (5)
Pt3^xxiii—Sr1—Pt3^xxvi	109.92 (5)	108.90 (2)	111.06 (2)
Pt3^xxiii—Sr1—Pt3^xxvii	69.71 (3)	63.71 (3)	75.95 (4)
Pt3^xxiii—Sr1—Pt3^xxiv	172.93 (6)	171.68 (8)	175.19 (7)
Pt3^xxiii—Sr1—Pt4^xxiii	49.51 (3)	48.52 (2)	50.65 (2)
Pt3^xxiii—Sr1—Pt4ⁱ	92.69 (5)	90.45 (4)	95.12 (4)
Pt3^xxiii—Sr1—Pt4^xxiv	135.62 (5)	132.49 (5)	138.90 (5)
Pt3^xxiii—Sr1—Pt4^viii	91.20 (4)	85.04 (4)	97.52 (4)
Pt3^xxiii—Sr1—Pt5ⁱ	92.1 (2)	90.5 (2)	93.0 (2)
Pt3^xxiii—Sr1—Pt5^viii	93.8 (2)	92.9 (2)	96.0 (2)
Pt3^xxiii—Sr1—Pt5^xxviii	45.66 (8)	41.43 (7)	49.38 (10)
Pt3^xxiii—Sr1—Pt5^xxix	138.62 (9)	137.92 (8)	140.13 (10)
Pt3^xxiii—Sr1—Pt5^xxx	45.52 (9)	41.56 (8)	47.67 (8)
Pt3^xxiii—Sr1—Pt5^xxxi	139.77 (10)	138.88 (13)	140.09 (8)
Pt3^xxiii—Sr1—As1^xxiii	88.65 (5)	87.99 (4)	89.44 (4)
Pt3^xxiii—Sr1—As1^xxiv	87.45 (4)	83.07 (5)	91.97 (5)
Pt3^xxvi—Sr1—Pt3^xxvii	172.81 (7)	171.53 (8)	175.12 (7)
Pt3^xxvi—Sr1—Pt3^xxiv	69.83 (3)	63.71 (3)	75.95 (4)
Pt3^xxvi—Sr1—Pt4^xxiii	92.30 (5)	90.06 (3)	94.69 (4)
Pt3^xxvi—Sr1—Pt4ⁱ	49.91 (3)	49.12 (2)	50.83 (2)
Pt3^xxvi—Sr1—Pt4^xxiv	91.74 (4)	85.61 (4)	97.82 (4)
Pt3^xxvi—Sr1—Pt4^viii	135.35 (5)	132.39 (5)	138.33 (5)
Pt3^xxvi—Sr1—Pt5ⁱ	93.8 (2)	92.9 (2)	96.0 (2)
Pt3^xxvi—Sr1—Pt5^viii	92.1 (2)	90.6 (2)	93.1 (2)
Pt3^xxvi—Sr1—Pt5^xxviii	139.40 (9)	138.59 (13)	139.69 (8)
Pt3^xxvi—Sr1—Pt5^xxix	45.97 (8)	41.98 (8)	48.18 (8)
Pt3^xxvi—Sr1—Pt5^xxx	138.20 (9)	137.50 (8)	139.75 (10)
Pt3^xxvi—Sr1—Pt5^xxxi	46.24 (8)	41.88 (7)	49.84 (10)
Pt3^xxvi—Sr1—As1^xxiii	42.71 (3)	41.75 (4)	43.65 (4)
Pt3^xxvi—Sr1—As1^xxiv	131.79 (6)	128.67 (5)	134.69 (5)
Pt3^xxvii—Sr1—Pt3^xxiv	109.92 (5)	108.90 (2)	111.06 (2)
Pt3^xxvii—Sr1—Pt4^xxiii	91.63 (4)	85.61 (4)	97.82 (4)
Pt3^xxvii—Sr1—Pt4ⁱ	135.30 (5)	132.39 (5)	138.33 (5)
Pt3^xxvii—Sr1—Pt4^xxiv	92.27 (5)	90.06 (3)	94.69 (4)
Pt3^xxvii—Sr1—Pt4^viii	49.90 (3)	49.12 (2)	50.83 (2)
Pt3^xxvii—Sr1—Pt5ⁱ	92.2 (2)	90.6 (2)	93.1 (2)
Pt3^xxvii—Sr1—Pt5^viii	93.8 (2)	92.9 (2)	96.0 (2)
Pt3^xxvii—Sr1—Pt5^xxviii	46.13 (8)	41.88 (7)	49.84 (10)
Pt3^xxvii—Sr1—Pt5^xxix	138.20 (9)	137.50 (8)	139.75 (10)
Pt3^xxvii—Sr1—Pt5^xxx	45.97 (8)	41.98 (8)	48.18 (8)
Pt3^xxvii—Sr1—Pt5^xxxi	139.38 (10)	138.59 (13)	139.69 (8)
Pt3^xxvii—Sr1—As1^xxiii	131.73 (6)	128.67 (5)	134.69 (5)
Pt3^xxvii—Sr1—As1^xxiv	42.69 (3)	41.75 (4)	43.65 (4)
Pt3^xxiv—Sr1—Pt4^xxiii	135.67 (5)	132.49 (5)	138.90 (5)
Pt3^xxiv—Sr1—Pt4ⁱ	91.32 (4)	85.04 (4)	97.52 (4)
Pt3^xxiv—Sr1—Pt4^xxiv	49.52 (3)	48.52 (2)	50.65 (2)
Pt3^xxiv—Sr1—Pt4^viii	92.72 (5)	90.45 (4)	95.12 (4)
Pt3^xxiv—Sr1—Pt5ⁱ	93.8 (2)	92.9 (2)	96.0 (2)
Pt3^xxiv—Sr1—Pt5^viii	92.1 (2)	90.5 (2)	93.0 (2)
Pt3^xxiv—Sr1—Pt5^xxviii	139.79 (9)	138.88 (13)	140.09 (8)
Pt3^xxiv—Sr1—Pt5^xxix	45.52 (9)	41.56 (8)	47.67 (8)
Pt3^xxiv—Sr1—Pt5^xxx	138.62 (9)	137.92 (8)	140.13 (10)
Pt3^xxiv—Sr1—Pt5^xxxi	45.77 (8)	41.43 (7)	49.38 (10)
Pt3^xxiv—Sr1—As1^xxiii	87.53 (4)	83.07 (5)	91.97 (5)
Pt3^xxiv—Sr1—As1^xxiv	88.65 (5)	87.99 (4)	89.44 (4)
Pt4^xxiii—Sr1—Pt4ⁱ	49.87 (3)	48.45 (3)	51.16 (3)
Pt4^xxiii—Sr1—Pt4^xxiv	93.12 (5)	88.81 (6)	97.57 (6)
Pt4^xxiii—Sr1—Pt4^viii	71.85 (4)	64.34 (4)	79.33 (4)
Pt4^xxiii—Sr1—Pt5ⁱ	46.63 (17)	45.14 (17)	47.50 (18)
Pt4^xxiii—Sr1—Pt5^viii	47.71 (15)	45.38 (15)	50.52 (16)
Pt4^xxiii—Sr1—Pt5^xxviii	46.52 (9)	45.59 (8)	47.54 (9)
Pt4^xxiii—Sr1—Pt5^xxix	93.50 (12)	92.47 (12)	94.83 (12)
Pt4^xxiii—Sr1—Pt5^xxx	47.70 (8)	46.35 (8)	49.51 (8)
Pt4^xxiii—Sr1—Pt5^xxxi	94.35 (12)	92.84 (14)	95.40 (10)
Pt4^xxiii—Sr1—As1^xxiii	106.44 (5)	103.48 (3)	109.56 (3)
Pt4^xxiii—Sr1—As1^xxiv	129.28 (5)	123.70 (6)	135.05 (7)
Pt4ⁱ—Sr1—Pt4^xxiv	71.95 (4)	64.34 (4)	79.33 (4)
Pt4ⁱ—Sr1—Pt4^viii	91.88 (5)	88.14 (6)	95.82 (6)
Pt4ⁱ—Sr1—Pt5ⁱ	47.28 (15)	45.22 (15)	49.74 (17)
Pt4ⁱ—Sr1—Pt5^viii	45.69 (18)	44.41 (17)	46.49 (18)
Pt4ⁱ—Sr1—Pt5^xxviii	93.97 (12)	92.41 (14)	94.98 (10)
Pt4ⁱ—Sr1—Pt5^xxix	47.49 (8)	46.01 (8)	49.64 (8)
Pt4ⁱ—Sr1—Pt5^xxx	93.07 (12)	92.04 (12)	94.40 (12)
Pt4ⁱ—Sr1—Pt5^xxxi	46.90 (9)	45.79 (8)	47.82 (9)
Pt4ⁱ—Sr1—As1^xxiii	85.88 (4)	84.19 (3)	87.67 (3)
Pt4ⁱ—Sr1—As1^xxiv	175.14 (6)	173.28 (8)	179.69 (6)
Pt4^xxiv—Sr1—Pt4^viii	49.88 (3)	48.45 (3)	51.16 (3)
Pt4^xxiv—Sr1—Pt5ⁱ	47.67 (15)	45.38 (15)	50.52 (16)
Pt4^xxiv—Sr1—Pt5^viii	46.63 (17)	45.14 (17)	47.50 (18)
Pt4^xxiv—Sr1—Pt5^xxviii	94.40 (12)	92.84 (14)	95.40 (10)
Pt4^xxiv—Sr1—Pt5^xxix	47.70 (8)	46.35 (8)	49.51 (8)
Pt4^xxiv—Sr1—Pt5^xxx	93.50 (12)	92.47 (12)	94.83 (12)
Pt4^xxiv—Sr1—Pt5^xxxi	46.55 (9)	45.59 (8)	47.54 (9)
Pt4^xxiv—Sr1—As1^xxiii	129.39 (5)	123.70 (6)	135.05 (7)
Pt4^xxiv—Sr1—As1^xxiv	106.41 (5)	103.48 (3)	109.56 (3)
Pt4^viii—Sr1—Pt5ⁱ	45.70 (18)	44.41 (17)	46.49 (18)
Pt4^viii—Sr1—Pt5^viii	47.30 (15)	45.22 (15)	49.74 (17)
Pt4^viii—Sr1—Pt5^xxviii	46.87 (9)	45.79 (8)	47.82 (9)
Pt4^viii—Sr1—Pt5^xxix	93.07 (12)	92.04 (12)	94.40 (12)
Pt4^viii—Sr1—Pt5^xxx	47.49 (8)	46.01 (8)	49.64 (8)
Pt4^viii—Sr1—Pt5^xxxi	93.92 (12)	92.41 (14)	94.98 (10)
Pt4^viii—Sr1—As1^xxiii	175.14 (6)	173.28 (8)	179.69 (6)
Pt4^viii—Sr1—As1^xxiv	85.86 (4)	84.19 (3)	87.67 (3)
Pt5ⁱ—Sr1—Pt5^xxix	64.0 (3)	62.8 (2)	64.6 (3)
Pt5ⁱ—Sr1—Pt5^xxx	62.2 (2)	59.2 (3)	65.3 (2)
Pt5ⁱ—Sr1—Pt5^xxxi	60.5 (2)	58.97 (19)	61.8 (2)
Pt5ⁱ—Sr1—As1^xxiii	133.39 (12)	132.68 (11)	134.41 (14)
Pt5ⁱ—Sr1—As1^xxiv	130.51 (12)	129.87 (16)	131.04 (11)
Pt5^viii—Sr1—Pt5^xxviii	60.6 (2)	58.97 (19)	61.8 (2)
Pt5^viii—Sr1—Pt5^xxix	62.2 (2)	59.2 (3)	65.3 (2)
Pt5^viii—Sr1—Pt5^xxx	64.0 (3)	62.8 (2)	64.6 (3)
Pt5^viii—Sr1—As1^xxiii	130.50 (12)	129.87 (16)	131.04 (11)
Pt5^viii—Sr1—As1^xxiv	133.40 (12)	132.68 (11)	134.41 (14)
Pt5^xxviii—Sr1—Pt5^xxxi	129.50 (18)	129.47 (18)	129.55 (18)
Pt5^xxviii—Sr1—As1^xxiii	134.77 (9)	130.76 (8)	137.74 (13)
Pt5^xxviii—Sr1—As1^xxiv	86.70 (11)	81.60 (9)	90.97 (14)
Pt5^xxix—Sr1—Pt5^xxx	125.05 (19)	122.5 (2)	127.64 (18)
Pt5^xxix—Sr1—As1^xxiii	85.80 (11)	81.11 (10)	88.42 (11)
Pt5^xxix—Sr1—As1^xxiv	133.54 (8)	129.73 (10)	135.89 (10)
Pt5^xxx—Sr1—As1^xxiii	133.54 (8)	129.73 (10)	135.89 (10)
Pt5^xxx—Sr1—As1^xxiv	85.80 (11)	81.11 (10)	88.42 (11)
Pt5^xxxi—Sr1—As1^xxiii	86.83 (11)	81.60 (9)	90.97 (14)
Pt5^xxxi—Sr1—As1^xxiv	134.86 (9)	130.76 (8)	137.74 (13)
As1^xxiii—Sr1—As1^xxiv	96.10 (5)	95.43 (6)	96.92 (6)
Pt1—As1—Pt1^xxxii	180.0 (5)	180.0 (5)	180.0 (5)
Pt1—As1—Pt2^xxxii	125.75 (4)	125.72 (4)	125.79 (4)
Pt1—As1—Pt2^xxxiii	125.75 (4)	125.72 (4)	125.79 (4)
Pt1—As1—Pt3^xxxii	124.80 (4)	124.77 (4)	124.82 (4)
Pt1—As1—Pt3^xxxiii	124.80 (4)	124.77 (4)	124.82 (4)
Pt1—As1—Sr1ⁱⁱ	64.44 (3)	61.93 (3)	67.03 (3)
Pt1—As1—Sr1ⁱⁱⁱ	64.44 (3)	61.93 (3)	67.03 (3)
Pt1—As1—Sr1^iv	64.46 (3)	61.93 (3)	67.03 (3)
Pt1—As1—Sr1^v	64.46 (3)	61.93 (3)	67.03 (3)
Pt1^xxxii—As1—Pt2^xxxii	54.25 (4)	54.21 (4)	54.28 (4)
Pt1^xxxii—As1—Pt2^xxxiii	54.25 (4)	54.21 (4)	54.28 (4)
Pt1^xxxii—As1—Pt3^xxxii	55.20 (4)	55.18 (4)	55.23 (4)
Pt1^xxxii—As1—Pt3^xxxiii	55.20 (4)	55.18 (4)	55.23 (4)
Pt1^xxxii—As1—Sr1ⁱⁱ	115.56 (3)	112.97 (3)	118.07 (3)
Pt1^xxxii—As1—Sr1ⁱⁱⁱ	115.56 (3)	112.97 (3)	118.07 (3)
Pt1^xxxii—As1—Sr1^iv	115.54 (3)	112.97 (3)	118.07 (3)
Pt1^xxxii—As1—Sr1^v	115.54 (3)	112.97 (3)	118.07 (3)
Pt2^xxxii—As1—Pt2^xxxiii	108.49 (7)	108.42 (7)	108.57 (7)
Pt2^xxxii—As1—Pt3^xxxii	70.53 (4)	69.94 (4)	71.16 (5)
Pt2^xxxii—As1—Pt3^xxxiii	70.52 (4)	69.94 (4)	71.16 (5)
Pt2^xxxii—As1—Sr1ⁱⁱ	76.130 (12)	71.797 (18)	80.336 (18)
Pt2^xxxii—As1—Sr1ⁱⁱⁱ	138.03 (3)	135.79 (4)	140.25 (4)
Pt2^xxxii—As1—Sr1^iv	76.091 (12)	71.797 (18)	80.336 (18)
Pt2^xxxii—As1—Sr1^v	138.06 (3)	135.79 (4)	140.25 (4)
Pt2^xxxiii—As1—Pt3^xxxii	70.52 (4)	69.94 (4)	71.16 (5)
Pt2^xxxiii—As1—Pt3^xxxiii	70.53 (4)	69.94 (4)	71.16 (5)
Pt2^xxxiii—As1—Sr1ⁱⁱ	138.03 (3)	135.79 (4)	140.25 (4)
Pt2^xxxiii—As1—Sr1ⁱⁱⁱ	76.130 (12)	71.797 (18)	80.336 (18)
Pt2^xxxiii—As1—Sr1^iv	138.06 (3)	135.79 (4)	140.25 (4)
Pt2^xxxiii—As1—Sr1^v	76.091 (12)	71.797 (18)	80.336 (18)
Pt3^xxxii—As1—Pt3^xxxiii	110.41 (7)	110.36 (7)	110.45 (7)
Pt3^xxxii—As1—Sr1ⁱⁱ	72.44 (3)	71.98 (3)	72.90 (3)
Pt3^xxxii—As1—Sr1ⁱⁱⁱ	142.62 (3)	138.86 (3)	146.28 (3)
Pt3^xxxii—As1—Sr1^iv	142.59 (3)	138.86 (3)	146.28 (3)
Pt3^xxxii—As1—Sr1^v	72.44 (3)	71.98 (3)	72.90 (3)
Pt3^xxxiii—As1—Sr1ⁱⁱ	142.62 (3)	138.86 (3)	146.28 (3)
Pt3^xxxiii—As1—Sr1ⁱⁱⁱ	72.44 (3)	71.98 (3)	72.90 (3)
Pt3^xxxiii—As1—Sr1^iv	72.44 (3)	71.98 (3)	72.90 (3)
Pt3^xxxiii—As1—Sr1^v	142.59 (3)	138.86 (3)	146.28 (3)
Sr1ⁱⁱ—As1—Sr1ⁱⁱⁱ	128.89 (7)	123.86 (7)	134.06 (7)
Sr1ⁱⁱ—As1—Sr1^iv	83.90 (5)	83.83 (5)	83.98 (5)
Sr1ⁱⁱ—As1—Sr1^v	74.71 (4)	74.63 (4)	74.79 (6)
Sr1ⁱⁱⁱ—As1—Sr1^iv	74.71 (4)	74.63 (4)	74.79 (6)
Sr1ⁱⁱⁱ—As1—Sr1^v	83.90 (5)	83.83 (5)	83.98 (5)
Sr1^iv—As1—Sr1^v	128.93 (7)	123.86 (7)	134.06 (7)

Symmetry codes: (i) −x₁+1/2, −x₂+3/2, x₃+1/2, x₄; (ii) x₁, x₂−1/2, x₃+1/2, x₄; (iii) −x₁+1/2, −x₂+1, x₃, x₄; (iv) −x₁, −x₂+1, −x₃, −x₄; (v) x₁+1/2, x₂−1/2, −x₃+1/2, −x₄; (vi) x₁, x₂, x₃−1, x₄; (vii) −x₁, x₂, −x₃, −x₄+1/2; (viii) x₁−1/2, −x₂+3/2, −x₃+1/2, −x₄+1/2; (ix) x₁, x₂−1/2, x₃−1/2, x₄; (x) −x₁, −x₂+1, −x₃−1, −x₄; (xi) −x₁, x₂, −x₃+1, −x₄+1/2; (xii) −x₁+1/2, −x₂, x₃−1, x₄; (xiii) −x₁+1, x₂, −x₃, −x₄+1/2; (xiv) x₁−1/2, x₂, −x₃, −x₄; (xv) −x₁+1/2, x₂, x₃, x₄+1/2; (xvi) x₁+1/2, x₂−1/2, −x₃−1/2, −x₄; (xvii) −x₁+1/2, −x₂, x₃, x₄; (xviii) x₁−1/2, −x₂, −x₃, −x₄+1/2; (xix) −x₁+1, −x₂, −x₃, −x₄; (xx) x₁, −x₂, x₃, x₄+1/2; (xxi) −x₁, −x₂+3/2, −x₃+1/2, −x₄; (xxii) x₁, −x₂, x₃−1, x₄+1/2; (xxiii) x₁, x₂+1/2, x₃−1/2, x₄; (xxiv) −x₁, x₂+1/2, −x₃+1/2, −x₄+1/2; (xxv) x₁+1/2, −x₂, −x₃, −x₄+1/2; (xxvi) x₁, x₂+1/2, x₃+1/2, x₄; (xxvii) −x₁, x₂+1/2, −x₃−1/2, −x₄+1/2; (xxviii) x₁−1/2, x₂+1/2, −x₃−1/2, −x₄; (xxix) x₁−1/2, x₂+1/2, −x₃+1/2, −x₄; (xxx) −x₁+1/2, x₂+1/2, x₃−1/2, x₄+1/2; (xxxi) −x₁+1/2, x₂+1/2, x₃+1/2, x₄+1/2; (xxxii) x₁, x₂, x₃+1, x₄; (xxxiii) −x₁+1/2, −x₂+3/2, x₃+3/2, x₄.

(II) top

Crystal data top

AsPt_7.285Sr₂	F(000) = 2709
M_r = 1671.3	D_x = 13.537 Mg m⁻³
Orthorhombic, Amma(00γ)ss0†	Mo Kα radiation, λ = 0.71073 Å
q = 0.603800c*	Cell parameters from 3790 reflections
a = 7.9509 Å	θ = 3.8–26.4°
b = 18.1042 Å	µ = 140.54 mm⁻¹
c = 5.6972 Å	T = 293 K
V = 820.08 (8) Å³	Plate, metallic dark black
Z = 4	0.01 × 0.01 × 0.002 mm

Data collection top

SuperNova, Dual, Cu at zero, Atlas diffractometer	1220 independent reflections
Radiation source: X-ray tube	781 reflections with I > 3σ(I)
Mirror monochromator	R_int = 0.092
Detector resolution: 5.1333 pixels mm^-1	θ_max = 26.4°, θ_min = 3.8°
ω scans	h = −9→8
Absorption correction: multi-scan CrysAlisPro, Agilent Technologies, Version 1.171.37.34 (release 22-05-2014 CrysAlis171 .NET) (compiled May 22 2014,16:03:01) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm.	k = −22→22
T_min = 0.279, T_max = 1.0	l = −7→7
10459 measured reflections

Refinement top

Refinement on F	3 constraints
R[F² > 2σ(F²)] = 0.030	Weighting scheme based on measured s.u.'s w = 1/(σ²(F) + 0.0001F²)
wR(F²) = 0.040	(Δ/σ)_max = 0.042
S = 1.32	Δρ_max = 4.58 e Å⁻³
1220 reflections	Δρ_min = −3.29 e Å⁻³
54 parameters	Extinction correction: B-C type 1 Gaussian isotropic (Becker & Coppens, 1974)
0 restraints	Extinction coefficient: 226 (8)

Special details top

Refinement. Occupancy of the Pt5 position is approximated by the harmonic function, which has been constrained by ocos1 = 0

Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å²) top

	x	y	z	U_iso*/U_eq	Occ. (<1)
Pt1	0.25	0.5	0.33956 (13)	0.0043 (2)
Pt2	0	0.5	0	0.0047 (2)
Pt3	0.25	0.38864 (3)	−0.00543 (9)	0.00486 (18)
Pt4	0.25	0.25139 (3)	0.25001 (9)	0.00684 (18)
Pt5	0.4996 (12)	0.29942 (7)	0.0010 (16)	0.0054 (8)	0.3212 (13)
Sr1	0	0.87896 (8)	0	0.0067 (4)
As1	0.25	0.5	0.7485 (3)	0.0023 (5)

Atomic displacement parameters (Å²) top

	U¹¹	U²²	U³³	U¹²	U¹³	U²³
Pt1	0.0052 (3)	0.0050 (4)	0.0028 (4)	0	0	0
Pt2	0.0007 (4)	0.0083 (4)	0.0051 (4)	0	0.0000 (2)	0
Pt3	0.0071 (3)	0.0018 (3)	0.0057 (3)	0	0	0.00006 (19)
Pt4	0.0120 (3)	0.0042 (3)	0.0043 (3)	0	0	0.0016 (2)
Pt5	0.0028 (4)	0.003 (2)	0.0102 (12)	0.000 (2)	0.0000 (3)	0.0025 (19)
Sr1	0.0024 (6)	0.0063 (8)	0.0115 (7)	0	−0.0006 (5)	0
As1	0.0011 (8)	0.0034 (10)	0.0025 (9)	0	0	0

Geometric parameters (Å, º) top

	Average	Minimum	Maximum
Pt1—Pt2	2.7756 (5)	2.7737 (5)	2.7776 (5)
Pt1—Pt2ⁱ	2.7756 (5)	2.7737 (5)	2.7776 (5)
Pt1—Pt3	2.8169 (7)	2.8157 (7)	2.8181 (7)
Pt1—Pt3ⁱ	2.8169 (7)	2.8157 (7)	2.8181 (7)
Pt1—Sr1ⁱⁱ	3.0982 (18)	3.048 (2)	3.151 (2)
Pt1—Sr1ⁱⁱⁱ	3.0982 (18)	3.048 (2)	3.151 (2)
Pt1—Sr1^iv	3.0989 (18)	3.048 (2)	3.151 (2)
Pt1—Sr1^v	3.0989 (18)	3.048 (2)	3.151 (2)
Pt1—As1^vi	3.367 (2)	3.367 (2)	3.367 (2)
Pt1—As1	2.330 (2)	2.330 (2)	2.330 (2)
Pt2—Pt3	2.8344 (10)	2.8158 (11)	2.8591 (11)
Pt2—Pt3ⁱ	2.8345 (10)	2.8158 (11)	2.8591 (11)
Pt2—Pt3^vii	2.8345 (10)	2.8158 (11)	2.8591 (11)
Pt2—Pt3^viii	2.8344 (10)	2.8158 (11)	2.8591 (11)
Pt2—Sr1^ix	3.5946 (14)	3.3810 (18)	3.8071 (18)
Pt2—Sr1ⁱⁱ	3.5935 (14)	3.3810 (18)	3.8071 (18)
Pt2—Sr1^x	3.5935 (14)	3.3810 (18)	3.8071 (18)
Pt2—Sr1^iv	3.5946 (14)	3.3810 (18)	3.8071 (18)
Pt2—As1^vi	2.4525 (11)	2.4503 (11)	2.4547 (11)
Pt2—As1^xi	2.4525 (11)	2.4503 (11)	2.4547 (11)
Pt3—Pt4	2.8816 (7)	2.8795 (7)	2.8836 (7)
Pt3—Pt4^xii	2.8943 (7)	2.8927 (7)	2.8959 (7)
Pt3—Pt5	2.563 (12)	2.404 (18)	2.717 (18)
Pt3—Pt5^xiii	2.566 (12)	2.412 (18)	2.718 (18)
Pt3—Pt5^xiv	2.567 (12)	2.412 (18)	2.718 (18)
Pt3—Pt5^xv	2.562 (12)	2.404 (18)	2.717 (18)
Pt3—Sr1^ix	3.4557 (16)	3.386 (3)	3.528 (3)
Pt3—Sr1ⁱⁱ	3.5054 (16)	3.433 (3)	3.581 (3)
Pt3—Sr1^xvi	3.4548 (16)	3.386 (3)	3.528 (3)
Pt3—Sr1^v	3.5063 (16)	3.433 (3)	3.581 (3)
Pt3—As1^vi	2.4570 (12)	2.4557 (12)	2.4585 (12)
Pt4—Pt4^xii	2.8550 (7)	2.8490 (8)	2.8608 (8)
Pt4—Pt4^xvii	2.8549 (7)	2.8491 (8)	2.8608 (8)
Pt4—Pt5	2.598 (17)	2.51 (3)	2.68 (3)
Pt4—Pt5^xvii	2.619 (18)	2.49 (3)	2.75 (3)
Pt4—Pt5^xiii	2.608 (17)	2.48 (3)	2.73 (3)
Pt4—Pt5^xviii	2.618 (17)	2.51 (3)	2.72 (3)
Pt4—Pt5^xix	2.620 (17)	2.51 (3)	2.72 (3)
Pt4—Pt5^xiv	2.607 (17)	2.48 (3)	2.73 (3)
Pt4—Pt5^xx	2.621 (18)	2.49 (3)	2.75 (3)
Pt4—Pt5^xv	2.598 (17)	2.51 (3)	2.68 (3)
Pt4—Sr1ⁱⁱ	3.368 (2)	3.273 (3)	3.463 (3)
Pt4—Sr1ⁱ	3.404 (2)	3.324 (3)	3.483 (3)
Pt4—Sr1^xxi	3.403 (2)	3.324 (3)	3.483 (3)
Pt4—Sr1^v	3.369 (2)	3.273 (3)	3.463 (3)
Pt5—Pt5^xiii	0.12 (3)	0.04 (6)	0.17 (6)
Pt5—Pt5^xxii	3.37 (4)	3.23 (4)	3.51 (4)
Pt5—Pt5^xix	3.35 (4)	3.04 (4)	3.67 (4)
Pt5—Pt5^xxiii	3.37 (4)	3.13 (4)	3.60 (4)
Pt5—Pt5^xx	3.36 (4)	3.13 (4)	3.60 (4)
Pt5—Sr1ⁱ	3.228 (14)	3.09 (3)	3.37 (3)
Pt5—Sr1^xvi	3.20 (2)	3.03 (4)	3.36 (4)
Pt5—Sr1^v	3.19 (2)	3.05 (4)	3.33 (4)
Sr1—As1^xxiv	3.2809 (19)	3.210 (3)	3.355 (3)
Sr1—As1^xxv	3.2823 (19)	3.210 (3)	3.355 (3)

Pt2—Pt1—Pt2ⁱ	91.63 (2)	91.55 (2)	91.71 (2)
Pt2—Pt1—Pt3	60.90 (2)	60.42 (2)	61.45 (3)
Pt2—Pt1—Pt3ⁱ	60.90 (2)	60.42 (2)	61.45 (3)
Pt2—Pt1—Sr1ⁱⁱ	75.229 (12)	70.676 (18)	79.726 (17)
Pt2—Pt1—Sr1ⁱⁱⁱ	131.69 (3)	130.76 (3)	132.61 (3)
Pt2—Pt1—Sr1^iv	75.246 (12)	70.676 (18)	79.726 (17)
Pt2—Pt1—Sr1^v	131.70 (3)	130.76 (3)	132.61 (3)
Pt2—Pt1—As1^vi	45.815 (11)	45.777 (11)	45.854 (11)
Pt2—Pt1—As1	134.185 (11)	134.146 (11)	134.223 (11)
Pt2ⁱ—Pt1—Pt3	60.90 (2)	60.42 (2)	61.45 (3)
Pt2ⁱ—Pt1—Pt3ⁱ	60.90 (2)	60.42 (2)	61.45 (3)
Pt2ⁱ—Pt1—Sr1ⁱⁱ	131.69 (3)	130.76 (3)	132.61 (3)
Pt2ⁱ—Pt1—Sr1ⁱⁱⁱ	75.229 (12)	70.676 (18)	79.726 (17)
Pt2ⁱ—Pt1—Sr1^iv	131.70 (3)	130.76 (3)	132.61 (3)
Pt2ⁱ—Pt1—Sr1^v	75.246 (12)	70.676 (18)	79.726 (17)
Pt2ⁱ—Pt1—As1^vi	45.815 (11)	45.777 (11)	45.854 (11)
Pt2ⁱ—Pt1—As1	134.185 (11)	134.146 (11)	134.223 (11)
Pt3—Pt1—Pt3ⁱ	91.51 (3)	91.46 (3)	91.56 (3)
Pt3—Pt1—Sr1ⁱⁱ	72.50 (3)	71.52 (3)	73.51 (3)
Pt3—Pt1—Sr1ⁱⁱⁱ	135.44 (3)	131.26 (2)	139.62 (2)
Pt3—Pt1—Sr1^iv	135.46 (3)	131.26 (2)	139.62 (2)
Pt3—Pt1—Sr1^v	72.52 (3)	71.52 (3)	73.51 (3)
Pt3—Pt1—As1^vi	45.754 (15)	45.730 (15)	45.778 (15)
Pt3—Pt1—As1	134.246 (15)	134.222 (15)	134.270 (15)
Pt3ⁱ—Pt1—Sr1ⁱⁱ	135.44 (3)	131.26 (2)	139.62 (2)
Pt3ⁱ—Pt1—Sr1ⁱⁱⁱ	72.50 (3)	71.52 (3)	73.51 (3)
Pt3ⁱ—Pt1—Sr1^iv	72.52 (3)	71.52 (3)	73.51 (3)
Pt3ⁱ—Pt1—Sr1^v	135.46 (3)	131.26 (2)	139.62 (2)
Pt3ⁱ—Pt1—As1^vi	45.754 (15)	45.729 (15)	45.778 (15)
Pt3ⁱ—Pt1—As1	134.246 (15)	134.222 (15)	134.270 (15)
Sr1ⁱⁱ—Pt1—Sr1ⁱⁱⁱ	145.72 (3)	140.02 (4)	151.48 (5)
Sr1ⁱⁱ—Pt1—Sr1^iv	90.17 (4)	90.09 (4)	90.25 (5)
Sr1ⁱⁱ—Pt1—Sr1^v	79.96 (4)	79.87 (3)	80.05 (6)
Sr1ⁱⁱ—Pt1—As1^vi	107.14 (2)	104.26 (4)	109.99 (4)
Sr1ⁱⁱ—Pt1—As1	72.86 (2)	70.01 (4)	75.74 (4)
Sr1ⁱⁱⁱ—Pt1—Sr1^iv	79.96 (4)	79.87 (3)	80.05 (6)
Sr1ⁱⁱⁱ—Pt1—Sr1^v	90.17 (4)	90.09 (4)	90.25 (5)
Sr1ⁱⁱⁱ—Pt1—As1^vi	107.14 (2)	104.26 (4)	109.99 (4)
Sr1ⁱⁱⁱ—Pt1—As1	72.86 (2)	70.01 (4)	75.74 (4)
Sr1^iv—Pt1—Sr1^v	145.69 (3)	140.02 (4)	151.48 (5)
Sr1^iv—Pt1—As1^vi	107.15 (2)	104.26 (4)	109.99 (4)
Sr1^iv—Pt1—As1	72.85 (2)	70.01 (4)	75.74 (4)
Sr1^v—Pt1—As1^vi	107.15 (2)	104.26 (4)	109.99 (4)
Sr1^v—Pt1—As1	72.85 (2)	70.01 (4)	75.74 (4)
As1^vi—Pt1—As1	180.0 (5)	180.0 (5)	180.0 (5)
Pt1—Pt2—Pt1^vii	176.20 (4)	173.97 (4)	180.0 (5)
Pt1—Pt2—Pt3	60.269 (14)	59.974 (16)	60.503 (15)
Pt1—Pt2—Pt3ⁱ	60.269 (14)	59.974 (16)	60.503 (15)
Pt1—Pt2—Pt3^vii	119.63 (2)	114.88 (3)	124.22 (3)
Pt1—Pt2—Pt3^viii	119.63 (2)	114.88 (3)	124.22 (3)
Pt1—Pt2—Sr1^ix	123.55 (2)	121.20 (3)	125.86 (3)
Pt1—Pt2—Sr1ⁱⁱ	56.447 (17)	54.363 (17)	58.54 (2)
Pt1—Pt2—Sr1^x	123.54 (2)	121.20 (3)	125.86 (3)
Pt1—Pt2—Sr1^iv	56.445 (17)	54.363 (17)	58.54 (2)
Pt1—Pt2—As1^vi	79.93 (4)	79.86 (4)	80.01 (4)
Pt1—Pt2—As1^xi	99.89 (4)	99.78 (4)	99.99 (4)
Pt1^vii—Pt2—Pt3	119.63 (2)	114.88 (3)	124.22 (3)
Pt1^vii—Pt2—Pt3ⁱ	119.63 (2)	114.88 (3)	124.22 (3)
Pt1^vii—Pt2—Pt3^vii	60.269 (14)	59.974 (16)	60.503 (15)
Pt1^vii—Pt2—Pt3^viii	60.269 (14)	59.974 (16)	60.503 (15)
Pt1^vii—Pt2—Sr1^ix	56.445 (17)	54.363 (17)	58.54 (2)
Pt1^vii—Pt2—Sr1ⁱⁱ	123.54 (2)	121.20 (3)	125.86 (3)
Pt1^vii—Pt2—Sr1^x	56.447 (17)	54.363 (17)	58.54 (2)
Pt1^vii—Pt2—Sr1^iv	123.55 (2)	121.20 (3)	125.86 (3)
Pt1^vii—Pt2—As1^vi	99.89 (4)	99.78 (4)	99.99 (4)
Pt1^vii—Pt2—As1^xi	79.93 (4)	79.86 (4)	80.01 (4)
Pt3—Pt2—Pt3ⁱ	90.78 (2)	90.750 (18)	90.81 (3)
Pt3—Pt2—Pt3^vii	89.22 (3)	81.72 (3)	96.78 (4)
Pt3—Pt2—Pt3^viii	175.25 (4)	172.47 (4)	180.0 (5)
Pt3—Pt2—Sr1^ix	63.74 (2)	61.83 (3)	65.71 (3)
Pt3—Pt2—Sr1ⁱⁱ	64.84 (2)	62.93 (3)	66.81 (3)
Pt3—Pt2—Sr1^x	115.15 (2)	113.472 (18)	116.74 (2)
Pt3—Pt2—Sr1^iv	116.24 (2)	114.559 (18)	117.85 (2)
Pt3—Pt2—As1^vi	54.81 (2)	54.47 (2)	55.09 (2)
Pt3—Pt2—As1^xi	125.09 (3)	119.40 (4)	130.64 (4)
Pt3ⁱ—Pt2—Pt3^vii	175.25 (4)	172.47 (4)	180.0 (5)
Pt3ⁱ—Pt2—Pt3^viii	89.22 (3)	81.72 (3)	96.78 (4)
Pt3ⁱ—Pt2—Sr1^ix	115.14 (2)	113.472 (18)	116.74 (2)
Pt3ⁱ—Pt2—Sr1ⁱⁱ	116.25 (2)	114.559 (18)	117.85 (2)
Pt3ⁱ—Pt2—Sr1^x	63.74 (2)	61.83 (3)	65.71 (3)
Pt3ⁱ—Pt2—Sr1^iv	64.84 (2)	62.93 (3)	66.81 (3)
Pt3ⁱ—Pt2—As1^vi	54.81 (2)	54.47 (2)	55.09 (2)
Pt3ⁱ—Pt2—As1^xi	125.09 (3)	119.40 (4)	130.64 (4)
Pt3^vii—Pt2—Pt3^viii	90.78 (2)	90.750 (18)	90.81 (3)
Pt3^vii—Pt2—Sr1^ix	64.84 (2)	62.93 (3)	66.81 (3)
Pt3^vii—Pt2—Sr1ⁱⁱ	63.74 (2)	61.83 (3)	65.71 (3)
Pt3^vii—Pt2—Sr1^x	116.25 (2)	114.559 (18)	117.85 (2)
Pt3^vii—Pt2—Sr1^iv	115.14 (2)	113.472 (18)	116.74 (2)
Pt3^vii—Pt2—As1^vi	125.09 (3)	119.40 (4)	130.64 (4)
Pt3^vii—Pt2—As1^xi	54.81 (2)	54.47 (2)	55.09 (2)
Pt3^viii—Pt2—Sr1^ix	116.24 (2)	114.559 (18)	117.85 (2)
Pt3^viii—Pt2—Sr1ⁱⁱ	115.15 (2)	113.472 (18)	116.74 (2)
Pt3^viii—Pt2—Sr1^x	64.84 (2)	62.93 (3)	66.81 (3)
Pt3^viii—Pt2—Sr1^iv	63.74 (2)	61.83 (3)	65.71 (3)
Pt3^viii—Pt2—As1^vi	125.09 (3)	119.40 (4)	130.64 (4)
Pt3^viii—Pt2—As1^xi	54.81 (2)	54.47 (2)	55.09 (2)
Sr1^ix—Pt2—Sr1ⁱⁱ	104.87 (4)	104.40 (4)	105.37 (5)
Sr1^ix—Pt2—Sr1^x	75.13 (4)	75.11 (4)	75.15 (4)
Sr1^ix—Pt2—Sr1^iv	179.70 (9)	179.51 (5)	180.0 (5)
Sr1^ix—Pt2—As1^vi	62.39 (4)	60.15 (5)	64.65 (6)
Sr1^ix—Pt2—As1^xi	117.59 (4)	115.13 (6)	120.03 (6)
Sr1ⁱⁱ—Pt2—Sr1^x	179.70 (9)	179.51 (5)	180.0 (5)
Sr1ⁱⁱ—Pt2—Sr1^iv	75.13 (4)	75.11 (4)	75.15 (4)
Sr1ⁱⁱ—Pt2—As1^vi	117.59 (4)	115.13 (6)	120.03 (6)
Sr1ⁱⁱ—Pt2—As1^xi	62.40 (4)	60.15 (5)	64.65 (6)
Sr1^x—Pt2—Sr1^iv	104.87 (4)	104.40 (4)	105.37 (5)
Sr1^x—Pt2—As1^vi	62.40 (4)	60.15 (5)	64.65 (6)
Sr1^x—Pt2—As1^xi	117.59 (4)	115.13 (6)	120.03 (6)
Sr1^iv—Pt2—As1^vi	117.59 (4)	115.13 (6)	120.03 (6)
Sr1^iv—Pt2—As1^xi	62.39 (4)	60.15 (5)	64.65 (6)
As1^vi—Pt2—As1^xi	175.69 (4)	173.17 (5)	180.0 (5)
Pt1—Pt3—Pt2	58.831 (17)	58.576 (15)	59.076 (16)
Pt1—Pt3—Pt2ⁱ	58.830 (17)	58.576 (15)	59.076 (16)
Pt1—Pt3—Pt4	105.38 (2)	105.32 (2)	105.44 (2)
Pt1—Pt3—Pt4^xii	164.43 (3)	164.34 (3)	164.54 (3)
Pt1—Pt3—Pt5	116.2 (8)	113.1 (7)	119.5 (8)
Pt1—Pt3—Pt5^xiii	116.3 (8)	112.3 (8)	120.5 (8)
Pt1—Pt3—Pt5^xiv	116.4 (8)	112.3 (8)	120.5 (8)
Pt1—Pt3—Pt5^xv	116.3 (8)	113.1 (7)	119.5 (8)
Pt1—Pt3—Sr1^ix	127.21 (4)	123.94 (4)	130.28 (4)
Pt1—Pt3—Sr1ⁱⁱ	57.45 (3)	57.35 (4)	57.57 (3)
Pt1—Pt3—Sr1^xvi	127.20 (4)	123.94 (4)	130.28 (4)
Pt1—Pt3—Sr1^v	57.45 (3)	57.35 (4)	57.57 (3)
Pt1—Pt3—As1^vi	79.04 (4)	78.99 (4)	79.08 (4)
Pt2—Pt3—Pt2ⁱ	89.21 (2)	89.18 (2)	89.24 (3)
Pt2—Pt3—Pt4	127.46 (5)	124.20 (5)	130.71 (5)
Pt2—Pt3—Pt4^xii	129.00 (5)	126.37 (5)	131.56 (5)
Pt2—Pt3—Pt5	173.0 (4)	169.55 (17)	177.6 (4)
Pt2—Pt3—Pt5^xiii	173.0 (4)	169.2 (3)	177.93 (19)
Pt2—Pt3—Pt5^xiv	84.45 (14)	80.22 (13)	88.72 (15)
Pt2—Pt3—Pt5^xv	84.50 (14)	80.35 (13)	88.73 (15)
Pt2—Pt3—Sr1^ix	68.89 (3)	65.21 (3)	72.41 (3)
Pt2—Pt3—Sr1ⁱⁱ	68.10 (3)	64.51 (3)	71.57 (3)
Pt2—Pt3—Sr1^xvi	116.61 (3)	116.01 (3)	117.03 (3)
Pt2—Pt3—Sr1^v	115.07 (3)	114.43 (3)	115.54 (3)
Pt2—Pt3—As1^vi	54.66 (2)	54.35 (2)	54.97 (2)
Pt2ⁱ—Pt3—Pt4	127.51 (5)	124.20 (5)	130.71 (5)
Pt2ⁱ—Pt3—Pt4^xii	128.96 (5)	126.37 (5)	131.56 (5)
Pt2ⁱ—Pt3—Pt5	84.53 (14)	80.35 (13)	88.73 (15)
Pt2ⁱ—Pt3—Pt5^xiii	84.42 (14)	80.22 (13)	88.72 (15)
Pt2ⁱ—Pt3—Pt5^xiv	173.1 (4)	169.2 (3)	177.93 (19)
Pt2ⁱ—Pt3—Pt5^xv	173.0 (4)	169.55 (17)	177.6 (4)
Pt2ⁱ—Pt3—Sr1^ix	116.61 (3)	116.01 (3)	117.03 (3)
Pt2ⁱ—Pt3—Sr1ⁱⁱ	115.07 (3)	114.43 (3)	115.54 (3)
Pt2ⁱ—Pt3—Sr1^xvi	68.88 (3)	65.21 (3)	72.41 (3)
Pt2ⁱ—Pt3—Sr1^v	68.12 (3)	64.51 (3)	71.57 (3)
Pt2ⁱ—Pt3—As1^vi	54.66 (2)	54.35 (2)	54.97 (2)
Pt4—Pt3—Pt4^xii	59.246 (18)	59.136 (18)	59.354 (18)
Pt4—Pt3—Pt5	56.6 (6)	55.6 (6)	57.4 (6)
Pt4—Pt3—Pt5^xiii	56.8 (6)	54.6 (7)	59.1 (6)
Pt4—Pt3—Pt5^xiv	56.8 (6)	54.6 (7)	59.1 (6)
Pt4—Pt3—Pt5^xv	56.6 (6)	55.6 (6)	57.4 (6)
Pt4—Pt3—Sr1^ix	111.61 (4)	109.52 (5)	113.71 (5)
Pt4—Pt3—Sr1ⁱⁱ	62.75 (4)	60.90 (4)	64.74 (4)
Pt4—Pt3—Sr1^xvi	111.65 (4)	109.52 (5)	113.71 (5)
Pt4—Pt3—Sr1^v	62.77 (4)	60.90 (4)	64.74 (4)
Pt4—Pt3—As1^vi	174.97 (5)	174.42 (5)	175.55 (4)
Pt4^xii—Pt3—Pt5	56.9 (6)	54.7 (7)	59.2 (5)
Pt4^xii—Pt3—Pt5^xiii	56.9 (6)	55.1 (6)	58.5 (6)
Pt4^xii—Pt3—Pt5^xiv	56.9 (6)	55.1 (6)	58.5 (6)
Pt4^xii—Pt3—Pt5^xv	57.0 (6)	54.7 (7)	59.2 (5)
Pt4^xii—Pt3—Sr1^ix	64.12 (4)	62.26 (4)	66.10 (4)
Pt4^xii—Pt3—Sr1ⁱⁱ	110.64 (4)	109.01 (5)	112.22 (5)
Pt4^xii—Pt3—Sr1^xvi	64.11 (4)	62.26 (4)	66.10 (4)
Pt4^xii—Pt3—Sr1^v	110.61 (4)	109.01 (5)	112.22 (5)
Pt4^xii—Pt3—As1^vi	116.40 (4)	116.35 (4)	116.46 (4)
Pt5—Pt3—Pt5^xiii	2.2 (7)	1.0 (15)	3.1 (5)
Pt5—Pt3—Pt5^xiv	101.9 (3)	99.1 (5)	105.0 (5)
Pt5—Pt3—Pt5^xv	101.8 (3)	101.7 (2)	102.0 (5)
Pt5—Pt3—Sr1^ix	115.2 (5)	112.9 (4)	117.4 (4)
Pt5—Pt3—Sr1ⁱⁱ	113.4 (5)	109.6 (4)	117.5 (4)
Pt5—Pt3—Sr1^xvi	62.1 (6)	58.0 (3)	66.3 (3)
Pt5—Pt3—Sr1^v	61.1 (6)	57.4 (5)	65.2 (6)
Pt5—Pt3—As1^vi	121.7 (5)	117.7 (4)	125.8 (4)
Pt5^xiii—Pt3—Pt5^xiv	102.0 (3)	101.8 (2)	102.2 (5)
Pt5^xiii—Pt3—Pt5^xv	101.9 (3)	99.1 (5)	105.0 (5)
Pt5^xiii—Pt3—Sr1^ix	115.1 (5)	111.2 (4)	119.2 (4)
Pt5^xiii—Pt3—Sr1ⁱⁱ	113.6 (5)	111.3 (4)	115.9 (4)
Pt5^xiii—Pt3—Sr1^xvi	62.0 (6)	58.1 (6)	66.0 (6)
Pt5^xiii—Pt3—Sr1^v	61.2 (6)	57.1 (3)	65.5 (3)
Pt5^xiii—Pt3—As1^vi	121.5 (5)	118.4 (6)	124.8 (6)
Pt5^xiv—Pt3—Pt5^xv	2.2 (7)	1.0 (15)	3.1 (5)
Pt5^xiv—Pt3—Sr1^ix	61.9 (6)	58.1 (6)	66.0 (6)
Pt5^xiv—Pt3—Sr1ⁱⁱ	61.3 (6)	57.1 (3)	65.5 (3)
Pt5^xiv—Pt3—Sr1^xvi	115.1 (5)	111.2 (4)	119.2 (4)
Pt5^xiv—Pt3—Sr1^v	113.6 (5)	111.3 (4)	115.9 (4)
Pt5^xiv—Pt3—As1^vi	121.5 (5)	118.4 (6)	124.8 (6)
Pt5^xv—Pt3—Sr1^ix	62.1 (6)	58.0 (3)	66.3 (3)
Pt5^xv—Pt3—Sr1ⁱⁱ	61.2 (6)	57.4 (5)	65.2 (6)
Pt5^xv—Pt3—Sr1^xvi	115.2 (5)	112.9 (4)	117.4 (4)
Pt5^xv—Pt3—Sr1^v	113.5 (5)	109.6 (4)	117.5 (4)
Pt5^xv—Pt3—As1^vi	121.7 (5)	117.7 (4)	125.8 (4)
Sr1^ix—Pt3—Sr1ⁱⁱ	109.92 (4)	103.80 (5)	115.95 (5)
Sr1^ix—Pt3—Sr1^xvi	70.36 (3)	70.297 (10)	70.42 (5)
Sr1^ix—Pt3—Sr1^v	172.85 (5)	171.17 (5)	175.04 (5)
Sr1^ix—Pt3—As1^vi	64.88 (4)	64.36 (4)	65.37 (4)
Sr1ⁱⁱ—Pt3—Sr1^xvi	172.87 (5)	171.17 (5)	175.04 (5)
Sr1ⁱⁱ—Pt3—Sr1^v	69.19 (3)	69.133 (9)	69.26 (5)
Sr1ⁱⁱ—Pt3—As1^vi	120.58 (5)	117.68 (5)	123.28 (4)
Sr1^xvi—Pt3—Sr1^v	109.92 (4)	103.80 (5)	115.95 (5)
Sr1^xvi—Pt3—As1^vi	64.88 (4)	64.36 (4)	65.37 (4)
Sr1^v—Pt3—As1^vi	120.59 (5)	117.68 (5)	123.28 (4)
Pt3—Pt4—Pt3^xvii	176.31 (5)	174.71 (4)	178.43 (3)
Pt3—Pt4—Pt4^xii	60.599 (18)	60.520 (18)	60.679 (18)
Pt3—Pt4—Pt4^xvii	121.26 (2)	121.08 (2)	121.43 (2)
Pt3—Pt4—Pt5	55.4 (3)	52.3 (2)	58.4 (3)
Pt3—Pt4—Pt5^xvii	125.6 (3)	119.1 (3)	132.2 (2)
Pt3—Pt4—Pt5^xiii	55.4 (3)	52.5 (3)	58.4 (3)
Pt3—Pt4—Pt5^xviii	125.4 (3)	117.8 (3)	133.06 (19)
Pt3—Pt4—Pt5^xix	125.3 (3)	117.8 (3)	133.06 (19)
Pt3—Pt4—Pt5^xiv	55.5 (3)	52.5 (3)	58.4 (3)
Pt3—Pt4—Pt5^xx	125.4 (3)	119.1 (3)	132.2 (2)
Pt3—Pt4—Pt5^xv	55.4 (3)	52.3 (2)	58.4 (3)
Pt3—Pt4—Sr1ⁱⁱ	67.73 (3)	66.01 (3)	69.48 (3)
Pt3—Pt4—Sr1ⁱ	112.66 (4)	111.00 (3)	114.37 (3)
Pt3—Pt4—Sr1^xxi	112.67 (4)	111.00 (3)	114.37 (3)
Pt3—Pt4—Sr1^v	67.72 (3)	66.01 (3)	69.48 (3)
Pt3^xvii—Pt4—Pt4^xii	117.68 (2)	117.53 (2)	117.84 (2)
Pt3^xvii—Pt4—Pt4^xvii	60.156 (17)	60.087 (17)	60.224 (17)
Pt3^xvii—Pt4—Pt5	123.9 (2)	116.4 (3)	131.47 (17)
Pt3^xvii—Pt4—Pt5^xvii	55.0 (2)	52.3 (2)	57.8 (2)
Pt3^xvii—Pt4—Pt5^xiii	123.9 (2)	118.1 (3)	129.9 (2)
Pt3^xvii—Pt4—Pt5^xviii	55.2 (2)	52.2 (2)	58.0 (3)
Pt3^xvii—Pt4—Pt5^xix	55.2 (2)	52.2 (2)	58.0 (3)
Pt3^xvii—Pt4—Pt5^xiv	123.9 (2)	118.1 (3)	129.9 (2)
Pt3^xvii—Pt4—Pt5^xx	55.1 (2)	52.3 (2)	57.8 (2)
Pt3^xvii—Pt4—Pt5^xv	124.0 (2)	116.4 (3)	131.47 (17)
Pt3^xvii—Pt4—Sr1ⁱⁱ	113.36 (4)	111.25 (4)	115.53 (4)
Pt3^xvii—Pt4—Sr1ⁱ	65.96 (3)	64.13 (3)	67.85 (3)
Pt3^xvii—Pt4—Sr1^xxi	65.99 (3)	64.13 (3)	67.85 (3)
Pt3^xvii—Pt4—Sr1^v	113.32 (4)	111.25 (4)	115.53 (4)
Pt4^xii—Pt4—Pt4^xvii	175.51 (6)	173.60 (6)	177.98 (2)
Pt4^xii—Pt4—Pt5	57.2 (8)	54.8 (9)	59.7 (8)
Pt4^xii—Pt4—Pt5^xvii	122.7 (8)	116.8 (8)	128.7 (8)
Pt4^xii—Pt4—Pt5^xiii	57.0 (8)	55.6 (8)	58.5 (8)
Pt4^xii—Pt4—Pt5^xviii	122.4 (8)	115.8 (8)	128.8 (8)
Pt4^xii—Pt4—Pt5^xix	122.3 (8)	115.8 (8)	128.8 (8)
Pt4^xii—Pt4—Pt5^xiv	57.0 (8)	55.6 (8)	58.5 (8)
Pt4^xii—Pt4—Pt5^xx	122.6 (8)	116.8 (8)	128.7 (8)
Pt4^xii—Pt4—Pt5^xv	57.2 (8)	54.8 (9)	59.7 (8)
Pt4^xii—Pt4—Sr1ⁱⁱ	115.73 (3)	111.45 (3)	119.82 (3)
Pt4^xii—Pt4—Sr1ⁱ	64.42 (3)	63.48 (2)	65.53 (2)
Pt4^xii—Pt4—Sr1^xxi	64.42 (3)	63.48 (2)	65.53 (2)
Pt4^xii—Pt4—Sr1^v	115.67 (3)	111.45 (3)	119.82 (3)
Pt4^xvii—Pt4—Pt5	123.5 (8)	116.2 (8)	130.8 (8)
Pt4^xvii—Pt4—Pt5^xvii	56.4 (8)	55.6 (9)	57.4 (8)
Pt4^xvii—Pt4—Pt5^xiii	123.7 (8)	116.9 (8)	130.7 (8)
Pt4^xvii—Pt4—Pt5^xviii	56.6 (8)	54.7 (9)	58.7 (8)
Pt4^xvii—Pt4—Pt5^xix	56.7 (8)	54.7 (9)	58.7 (8)
Pt4^xvii—Pt4—Pt5^xiv	123.8 (8)	116.9 (8)	130.7 (8)
Pt4^xvii—Pt4—Pt5^xx	56.4 (8)	55.6 (9)	57.4 (8)
Pt4^xvii—Pt4—Pt5^xv	123.6 (8)	116.2 (8)	130.8 (8)
Pt4^xvii—Pt4—Sr1ⁱⁱ	65.69 (3)	65.31 (3)	66.33 (2)
Pt4^xvii—Pt4—Sr1ⁱ	113.87 (3)	109.31 (3)	118.32 (3)
Pt4^xvii—Pt4—Sr1^xxi	113.92 (3)	109.31 (3)	118.32 (3)
Pt4^xvii—Pt4—Sr1^v	65.70 (3)	65.31 (3)	66.33 (2)
Pt5—Pt4—Pt5^xvii	172.9 (8)	169.0 (7)	177.9 (6)
Pt5—Pt4—Pt5^xiii	2.5 (6)	0.8 (11)	3.7 (6)
Pt5—Pt4—Pt5^xviii	172.4 (7)	167.7 (6)	179.1 (10)
Pt5—Pt4—Pt5^xix	80.3 (8)	69.0 (8)	92.2 (7)
Pt5—Pt4—Pt5^xiv	99.8 (8)	98.0 (7)	101.4 (7)
Pt5—Pt4—Pt5^xx	80.6 (8)	70.7 (8)	91.1 (7)
Pt5—Pt4—Pt5^xv	100.0 (8)	99.8 (8)	100.1 (7)
Pt5—Pt4—Sr1ⁱⁱ	116.7 (3)	114.59 (18)	118.8 (2)
Pt5—Pt4—Sr1ⁱ	63.5 (3)	58.5 (2)	68.7 (3)
Pt5—Pt4—Sr1^xxi	116.6 (5)	114.5 (4)	118.2 (4)
Pt5—Pt4—Sr1^v	63.1 (5)	58.2 (5)	68.3 (5)
Pt5^xvii—Pt4—Pt5^xiii	174.3 (8)	170.8 (8)	179.0 (7)
Pt5^xvii—Pt4—Pt5^xviii	2.4 (6)	0.6 (10)	3.5 (6)
Pt5^xvii—Pt4—Pt5^xix	98.9 (8)	97.2 (7)	100.7 (8)
Pt5^xvii—Pt4—Pt5^xiv	80.8 (8)	72.4 (8)	89.7 (8)
Pt5^xvii—Pt4—Pt5^xx	98.8 (8)	98.4 (8)	99.1 (7)
Pt5^xvii—Pt4—Pt5^xv	80.7 (8)	70.7 (9)	91.1 (8)
Pt5^xvii—Pt4—Sr1ⁱⁱ	64.0 (3)	58.60 (18)	69.8 (3)
Pt5^xvii—Pt4—Sr1ⁱ	115.1 (3)	111.3 (4)	119.5 (4)
Pt5^xvii—Pt4—Sr1^xxi	62.7 (5)	57.0 (4)	68.6 (4)
Pt5^xvii—Pt4—Sr1^v	117.2 (5)	114.8 (6)	119.7 (6)
Pt5^xiii—Pt4—Pt5^xviii	172.9 (7)	169.6 (7)	178.1 (7)
Pt5^xiii—Pt4—Pt5^xix	80.5 (8)	70.7 (8)	90.8 (8)
Pt5^xiii—Pt4—Pt5^xiv	99.8 (8)	99.5 (8)	100.1 (7)
Pt5^xiii—Pt4—Pt5^xx	80.7 (8)	72.4 (8)	89.7 (8)
Pt5^xiii—Pt4—Pt5^xv	99.8 (8)	98.0 (7)	101.4 (8)
Pt5^xiii—Pt4—Sr1ⁱⁱ	116.8 (3)	112.8 (4)	121.4 (4)
Pt5^xiii—Pt4—Sr1ⁱ	63.5 (3)	58.72 (17)	68.6 (2)
Pt5^xiii—Pt4—Sr1^xxi	116.5 (5)	114.3 (6)	119.0 (6)
Pt5^xiii—Pt4—Sr1^v	63.3 (5)	57.3 (4)	69.6 (4)
Pt5^xviii—Pt4—Pt5^xix	99.2 (8)	99.0 (9)	99.5 (7)
Pt5^xviii—Pt4—Pt5^xiv	80.6 (8)	70.7 (8)	90.8 (8)
Pt5^xviii—Pt4—Pt5^xx	98.9 (8)	97.2 (7)	100.7 (7)
Pt5^xviii—Pt4—Pt5^xv	80.5 (8)	69.0 (9)	92.2 (8)
Pt5^xviii—Pt4—Sr1ⁱⁱ	64.0 (3)	58.73 (18)	69.3 (3)
Pt5^xviii—Pt4—Sr1ⁱ	115.1 (3)	112.98 (19)	117.0 (2)
Pt5^xviii—Pt4—Sr1^xxi	62.5 (5)	57.6 (6)	67.5 (6)
Pt5^xviii—Pt4—Sr1^v	117.3 (5)	115.3 (5)	118.9 (4)
Pt5^xix—Pt4—Pt5^xiv	172.9 (8)	169.6 (7)	178.1 (7)
Pt5^xix—Pt4—Pt5^xx	2.4 (6)	0.6 (10)	3.5 (6)
Pt5^xix—Pt4—Pt5^xv	172.4 (7)	167.7 (7)	179.1 (9)
Pt5^xix—Pt4—Sr1ⁱⁱ	117.3 (5)	115.3 (5)	118.9 (4)
Pt5^xix—Pt4—Sr1ⁱ	62.4 (5)	57.6 (6)	67.5 (6)
Pt5^xix—Pt4—Sr1^xxi	115.1 (3)	112.98 (19)	117.0 (2)
Pt5^xix—Pt4—Sr1^v	63.9 (3)	58.73 (18)	69.3 (3)
Pt5^xiv—Pt4—Pt5^xx	174.3 (8)	170.8 (8)	179.0 (7)
Pt5^xiv—Pt4—Pt5^xv	2.5 (6)	0.8 (11)	3.7 (6)
Pt5^xiv—Pt4—Sr1ⁱⁱ	63.4 (5)	57.3 (4)	69.6 (4)
Pt5^xiv—Pt4—Sr1ⁱ	116.5 (5)	114.3 (6)	119.0 (6)
Pt5^xiv—Pt4—Sr1^xxi	63.5 (3)	58.72 (17)	68.6 (2)
Pt5^xiv—Pt4—Sr1^v	116.9 (3)	112.8 (4)	121.4 (4)
Pt5^xx—Pt4—Pt5^xv	172.9 (7)	169.0 (8)	177.9 (6)
Pt5^xx—Pt4—Sr1ⁱⁱ	117.1 (5)	114.8 (6)	119.7 (6)
Pt5^xx—Pt4—Sr1ⁱ	62.7 (5)	57.0 (4)	68.6 (4)
Pt5^xx—Pt4—Sr1^xxi	115.2 (3)	111.3 (4)	119.5 (4)
Pt5^xx—Pt4—Sr1^v	63.9 (3)	58.60 (18)	69.8 (3)
Pt5^xv—Pt4—Sr1ⁱⁱ	63.2 (5)	58.2 (5)	68.3 (5)
Pt5^xv—Pt4—Sr1ⁱ	116.7 (5)	114.5 (4)	118.2 (4)
Pt5^xv—Pt4—Sr1^xxi	63.6 (3)	58.5 (2)	68.7 (3)
Pt5^xv—Pt4—Sr1^v	116.7 (3)	114.59 (18)	118.8 (2)
Sr1ⁱⁱ—Pt4—Sr1ⁱ	174.98 (5)	171.91 (3)	179.61 (6)
Sr1ⁱⁱ—Pt4—Sr1^xxi	108.06 (5)	100.71 (4)	115.60 (4)
Sr1ⁱⁱ—Pt4—Sr1^v	72.44 (4)	72.27 (3)	72.61 (5)
Sr1ⁱ—Pt4—Sr1^xxi	71.59 (4)	71.45 (3)	71.73 (5)
Sr1ⁱ—Pt4—Sr1^v	107.96 (5)	100.71 (4)	115.60 (4)
Sr1^xxi—Pt4—Sr1^v	174.97 (5)	171.91 (4)	179.61 (6)
Pt3—Pt5—Pt3^xiii	101.7 (5)	98.6 (8)	104.6 (9)
Pt3—Pt5—Pt4	68.0 (3)	64.5 (3)	71.6 (5)
Pt3—Pt5—Pt4^xii	68.0 (3)	64.0 (4)	72.4 (5)
Pt3—Pt5—Pt4^xiii	142.7 (10)	134.4 (6)	151.3 (6)
Pt3—Pt5—Pt4^xxvi	144.8 (10)	139.5 (5)	149.3 (7)
Pt3—Pt5—Pt5^xiii	91 (10)	51 (4)	130 (5)
Pt3—Pt5—Pt5^xxii	108.9 (7)	106.2 (4)	111.7 (4)
Pt3—Pt5—Pt5^xix	110.4 (7)	107.1 (4)	113.7 (4)
Pt3—Pt5—Pt5^xxiii	108.8 (7)	105.1 (4)	112.6 (5)
Pt3—Pt5—Pt5^xx	110.3 (7)	107.4 (4)	112.9 (4)
Pt3—Pt5—Sr1ⁱ	129.1 (4)	127.7 (5)	130.5 (5)
Pt3—Pt5—Sr1^xvi	72.8 (5)	68.3 (4)	77.6 (4)
Pt3—Pt5—Sr1^v	74.1 (5)	72.3 (4)	76.2 (4)
Pt3^xiii—Pt5—Pt4	142.8 (10)	137.3 (5)	147.4 (7)
Pt3^xiii—Pt5—Pt4^xii	144.7 (10)	136.6 (6)	153.1 (6)
Pt3^xiii—Pt5—Pt4^xiii	67.8 (3)	64.1 (4)	71.8 (5)
Pt3^xiii—Pt5—Pt4^xxvi	67.9 (3)	64.4 (4)	71.8 (5)
Pt3^xiii—Pt5—Pt5^xiii	86 (10)	47 (4)	126 (5)
Pt3^xiii—Pt5—Pt5^xxii	110.0 (7)	107.3 (4)	112.7 (4)
Pt3^xiii—Pt5—Pt5^xix	109.0 (7)	105.6 (4)	112.3 (4)
Pt3^xiii—Pt5—Pt5^xxiii	110.0 (7)	106.3 (5)	113.8 (5)
Pt3^xiii—Pt5—Pt5^xx	109.0 (7)	106.0 (5)	111.7 (5)
Pt3^xiii—Pt5—Sr1ⁱ	129.0 (4)	127.4 (5)	130.5 (5)
Pt3^xiii—Pt5—Sr1^xvi	74.0 (5)	69.4 (4)	78.9 (4)
Pt3^xiii—Pt5—Sr1^v	72.8 (5)	71.0 (4)	74.8 (4)
Pt4—Pt5—Pt4^xii	66.4 (3)	63.3 (2)	69.6 (2)
Pt4—Pt5—Pt4^xiii	140.3 (6)	133.7 (5)	146.9 (3)
Pt4—Pt5—Pt4^xxvi	99.7 (8)	87.4 (6)	111.6 (6)
Pt4—Pt5—Pt5^xiii	93 (14)	52 (18)	130 (12)
Pt4—Pt5—Pt5^xxii	106.6 (6)	104.8 (6)	108.4 (7)
Pt4—Pt5—Pt5^xix	50.1 (4)	43.8 (3)	56.2 (4)
Pt4—Pt5—Pt5^xxiii	106.4 (6)	105.1 (5)	107.9 (5)
Pt4—Pt5—Pt5^xx	50.1 (4)	43.7 (3)	56.1 (4)
Pt4—Pt5—Sr1ⁱ	70.5 (4)	67.0 (3)	73.9 (3)
Pt4—Pt5—Sr1^xvi	129.8 (5)	123.9 (4)	135.8 (4)
Pt4—Pt5—Sr1^v	70.3 (6)	66.4 (3)	74.1 (3)
Pt4^xii—Pt5—Pt4^xiii	99.0 (8)	90.1 (7)	107.8 (7)
Pt4^xii—Pt5—Pt4^xxvi	138.3 (6)	131.5 (4)	145.1 (3)
Pt4^xii—Pt5—Pt5^xiii	90 (14)	58 (11)	140 (20)
Pt4^xii—Pt5—Pt5^xxii	49.5 (4)	45.0 (4)	53.7 (4)
Pt4^xii—Pt5—Pt5^xix	106.1 (6)	101.1 (6)	111.0 (7)
Pt4^xii—Pt5—Pt5^xxiii	49.3 (4)	44.9 (4)	53.6 (4)
Pt4^xii—Pt5—Pt5^xx	106.1 (6)	100.7 (6)	111.7 (7)
Pt4^xii—Pt5—Sr1ⁱ	69.4 (4)	65.9 (2)	72.6 (3)
Pt4^xii—Pt5—Sr1^xvi	70.7 (6)	66.8 (2)	74.6 (2)
Pt4^xii—Pt5—Sr1^v	130.3 (5)	126.1 (4)	135.0 (5)
Pt4^xiii—Pt5—Pt4^xxvi	66.3 (3)	63.0 (2)	69.7 (2)
Pt4^xiii—Pt5—Pt5^xiii	85 (14)	48 (12)	127 (18)
Pt4^xiii—Pt5—Pt5^xxii	49.8 (4)	45.2 (4)	54.1 (4)
Pt4^xiii—Pt5—Pt5^xix	106.7 (6)	101.5 (6)	111.8 (7)
Pt4^xiii—Pt5—Pt5^xxiii	49.8 (4)	45.3 (4)	54.2 (4)
Pt4^xiii—Pt5—Pt5^xx	106.9 (6)	101.2 (6)	112.6 (7)
Pt4^xiii—Pt5—Sr1ⁱ	70.4 (4)	67.2 (2)	73.3 (3)
Pt4^xiii—Pt5—Sr1^xvi	70.0 (6)	65.8 (2)	74.1 (2)
Pt4^xiii—Pt5—Sr1^v	129.8 (5)	125.3 (4)	134.7 (4)
Pt4^xxvi—Pt5—Pt5^xiii	88 (14)	40 (20)	121 (11)
Pt4^xxvi—Pt5—Pt5^xxii	105.7 (6)	104.1 (6)	107.3 (7)
Pt4^xxvi—Pt5—Pt5^xix	49.6 (4)	43.5 (4)	55.4 (4)
Pt4^xxvi—Pt5—Pt5^xxiii	105.7 (6)	104.6 (5)	107.0 (5)
Pt4^xxvi—Pt5—Pt5^xx	49.7 (4)	43.6 (4)	55.5 (4)
Pt4^xxvi—Pt5—Sr1ⁱ	69.4 (4)	65.8 (2)	72.9 (3)
Pt4^xxvi—Pt5—Sr1^xvi	129.9 (5)	124.4 (4)	135.6 (5)
Pt4^xxvi—Pt5—Sr1^v	71.0 (6)	67.2 (4)	74.6 (3)
Pt5^xiii—Pt5—Pt5^xxii	86 (16)	5(17)	172 (17)
Pt5^xiii—Pt5—Pt5^xix	94 (16)	10 (30)	174 (14)
Pt5^xiii—Pt5—Pt5^xxiii	85 (16)	6(14)	170 (30)
Pt5^xiii—Pt5—Pt5^xx	93 (16)	8(17)	175 (18)
Pt5^xiii—Pt5—Sr1ⁱ	91 (16)	2(4)	178 (5)
Pt5^xiii—Pt5—Sr1^xvi	85 (16)	5(11)	170 (30)
Pt5^xiii—Pt5—Sr1^v	93 (16)	10 (30)	175 (11)
Pt5^xxii—Pt5—Pt5^xix	115.8 (7)	114.5 (8)	117.2 (8)
Pt5^xxii—Pt5—Pt5^xxiii	1.6 (5)	0.1 (3)	2.5 (5)
Pt5^xxii—Pt5—Pt5^xx	115.9 (7)	112.9 (8)	118.8 (8)
Pt5^xxii—Pt5—Sr1ⁱ	57.9 (5)	56.7 (5)	59.0 (4)
Pt5^xxii—Pt5—Sr1^xvi	58.8 (6)	56.0 (8)	61.7 (9)
Pt5^xxii—Pt5—Sr1^v	174.9 (8)	171.9 (7)	178.0 (7)
Pt5^xix—Pt5—Pt5^xxiii	115.7 (7)	112.1 (6)	119.5 (6)
Pt5^xix—Pt5—Pt5^xx	1.6 (5)	0.1 (3)	2.6 (5)
Pt5^xix—Pt5—Sr1ⁱ	57.9 (5)	56.2 (4)	59.8 (5)
Pt5^xix—Pt5—Sr1^xvi	174.6 (8)	170.8 (7)	178.5 (8)
Pt5^xix—Pt5—Sr1^v	59.1 (6)	57.3 (6)	60.9 (7)
Pt5^xxiii—Pt5—Pt5^xx	115.8 (7)	112.0 (9)	119.6 (9)
Pt5^xxiii—Pt5—Sr1ⁱ	57.8 (5)	55.7 (4)	59.9 (4)
Pt5^xxiii—Pt5—Sr1^xvi	58.9 (6)	58.0 (5)	59.9 (6)
Pt5^xxiii—Pt5—Sr1^v	174.8 (8)	169.4 (7)	180.0 (5)
Pt5^xx—Pt5—Sr1ⁱ	58.0 (5)	56.0 (4)	60.1 (5)
Pt5^xx—Pt5—Sr1^xvi	174.7 (8)	171.4 (8)	177.9 (8)
Pt5^xx—Pt5—Sr1^v	59.0 (6)	55.4 (8)	62.9 (9)
Sr1ⁱ—Pt5—Sr1^xvi	116.7 (7)	114.6 (8)	118.7 (10)
Sr1ⁱ—Pt5—Sr1^v	117.1 (7)	113.5 (8)	120.7 (10)
Sr1^xvi—Pt5—Sr1^v	126.3 (4)	120.6 (2)	131.9 (2)
Pt1^xxiv—Sr1—Pt1^xxv	89.83 (5)	89.17 (6)	90.65 (6)
Pt1^xxiv—Sr1—Pt2^xxiv	48.29 (3)	45.87 (3)	50.83 (3)
Pt1^xxiv—Sr1—Pt2^xxvii	78.62 (4)	75.85 (4)	81.31 (5)
Pt1^xxiv—Sr1—Pt3^xxiv	50.03 (3)	48.96 (4)	51.11 (4)
Pt1^xxiv—Sr1—Pt3^xxvii	80.47 (4)	79.73 (4)	81.26 (3)
Pt1^xxiv—Sr1—Pt3^xxviii	95.28 (4)	90.71 (5)	99.97 (5)
Pt1^xxiv—Sr1—Pt3^xxv	124.80 (5)	121.04 (5)	128.36 (5)
Pt1^xxiv—Sr1—Pt4^xxiv	88.91 (5)	86.77 (2)	91.24 (2)
Pt1^xxiv—Sr1—Pt4ⁱ	103.80 (6)	101.21 (4)	106.57 (3)
Pt1^xxiv—Sr1—Pt4^xxv	171.68 (5)	165.75 (8)	177.97 (7)
Pt1^xxiv—Sr1—Pt4^viii	137.89 (4)	131.82 (6)	144.14 (6)
Pt1^xxiv—Sr1—Pt5ⁱ	135.0 (4)	133.9 (4)	136.1 (3)
Pt1^xxiv—Sr1—Pt5^viii	135.0 (4)	134.1 (4)	135.9 (4)
Pt1^xxiv—Sr1—Pt5^xxix	93.2 (3)	88.6 (3)	97.8 (3)
Pt1^xxiv—Sr1—Pt5^xxx	125.7 (3)	121.5 (3)	129.8 (3)
Pt1^xxiv—Sr1—Pt5^xxxi	93.2 (3)	88.6 (3)	98.0 (3)
Pt1^xxiv—Sr1—Pt5^xxxii	125.6 (3)	121.3 (3)	129.6 (3)
Pt1^xxiv—Sr1—As1^xxiv	42.69 (4)	42.26 (4)	43.11 (4)
Pt1^xxiv—Sr1—As1^xxv	77.76 (4)	75.95 (3)	79.57 (4)
Pt1^xxv—Sr1—Pt2^xxiv	78.57 (4)	75.85 (4)	81.31 (5)
Pt1^xxv—Sr1—Pt2^xxvii	48.34 (3)	45.87 (3)	50.83 (3)
Pt1^xxv—Sr1—Pt3^xxiv	124.73 (5)	121.04 (5)	128.36 (5)
Pt1^xxv—Sr1—Pt3^xxvii	95.38 (4)	90.71 (5)	99.97 (5)
Pt1^xxv—Sr1—Pt3^xxviii	80.47 (4)	79.73 (4)	81.26 (3)
Pt1^xxv—Sr1—Pt3^xxv	50.05 (3)	48.96 (4)	51.11 (4)
Pt1^xxv—Sr1—Pt4^xxiv	171.56 (5)	165.75 (8)	177.97 (7)
Pt1^xxv—Sr1—Pt4ⁱ	138.02 (4)	131.82 (6)	144.14 (6)
Pt1^xxv—Sr1—Pt4^xxv	88.92 (5)	86.77 (2)	91.24 (2)
Pt1^xxv—Sr1—Pt4^viii	103.83 (6)	101.21 (4)	106.57 (3)
Pt1^xxv—Sr1—Pt5ⁱ	135.0 (4)	134.1 (4)	135.9 (4)
Pt1^xxv—Sr1—Pt5^viii	135.0 (4)	133.9 (4)	136.1 (3)
Pt1^xxv—Sr1—Pt5^xxix	125.5 (3)	121.3 (3)	129.6 (3)
Pt1^xxv—Sr1—Pt5^xxx	93.3 (3)	88.6 (3)	98.0 (3)
Pt1^xxv—Sr1—Pt5^xxxi	125.7 (3)	121.5 (3)	129.8 (3)
Pt1^xxv—Sr1—Pt5^xxxii	93.3 (3)	88.6 (3)	97.8 (3)
Pt1^xxv—Sr1—As1^xxiv	77.79 (4)	75.95 (3)	79.57 (4)
Pt1^xxv—Sr1—As1^xxv	42.69 (4)	42.26 (4)	43.11 (4)
Pt2^xxiv—Sr1—Pt2^xxvii	104.87 (5)	104.39 (6)	105.33 (6)
Pt2^xxiv—Sr1—Pt3^xxiv	47.03 (2)	45.39 (3)	48.78 (3)
Pt2^xxiv—Sr1—Pt3^xxvii	127.97 (6)	125.95 (7)	129.95 (7)
Pt2^xxiv—Sr1—Pt3^xxviii	47.36 (2)	45.65 (3)	49.18 (3)
Pt2^xxiv—Sr1—Pt3^xxv	128.34 (6)	126.36 (7)	130.28 (7)
Pt2^xxiv—Sr1—Pt4^xxiv	94.75 (3)	92.63 (5)	96.92 (5)
Pt2^xxiv—Sr1—Pt4ⁱ	139.06 (5)	135.02 (7)	143.26 (8)
Pt2^xxiv—Sr1—Pt4^xxv	138.95 (6)	135.04 (6)	143.01 (6)
Pt2^xxiv—Sr1—Pt4^viii	95.21 (3)	93.14 (5)	97.32 (5)
Pt2^xxiv—Sr1—Pt5ⁱ	127.7 (8)	127.4 (8)	127.9 (8)
Pt2^xxiv—Sr1—Pt5^viii	127.5 (8)	126.8 (8)	128.2 (8)
Pt2^xxiv—Sr1—Pt5^xxix	64.3 (4)	62.0 (3)	66.6 (4)
Pt2^xxiv—Sr1—Pt5^xxx	169.4 (4)	166.1 (3)	172.7 (4)
Pt2^xxiv—Sr1—Pt5^xxxi	64.5 (4)	61.6 (3)	67.5 (4)
Pt2^xxiv—Sr1—Pt5^xxxii	169.2 (4)	167.0 (3)	171.5 (4)
Pt2^xxiv—Sr1—As1^xxiv	86.22 (5)	83.75 (5)	88.68 (5)
Pt2^xxiv—Sr1—As1^xxv	41.47 (3)	39.45 (3)	43.61 (4)
Pt2^xxvii—Sr1—Pt3^xxiv	128.38 (6)	126.36 (7)	130.28 (7)
Pt2^xxvii—Sr1—Pt3^xxvii	47.39 (2)	45.65 (3)	49.18 (3)
Pt2^xxvii—Sr1—Pt3^xxviii	128.00 (6)	125.95 (7)	129.95 (7)
Pt2^xxvii—Sr1—Pt3^xxv	47.06 (2)	45.39 (3)	48.78 (3)
Pt2^xxvii—Sr1—Pt4^xxiv	139.01 (6)	135.04 (6)	143.01 (6)
Pt2^xxvii—Sr1—Pt4ⁱ	95.25 (3)	93.14 (5)	97.32 (5)
Pt2^xxvii—Sr1—Pt4^xxv	94.79 (3)	92.63 (5)	96.92 (5)
Pt2^xxvii—Sr1—Pt4^viii	139.14 (6)	135.02 (7)	143.26 (8)
Pt2^xxvii—Sr1—Pt5ⁱ	127.5 (8)	126.8 (8)	128.2 (8)
Pt2^xxvii—Sr1—Pt5^viii	127.7 (8)	127.4 (8)	127.9 (8)
Pt2^xxvii—Sr1—Pt5^xxix	169.2 (4)	167.0 (3)	171.5 (4)
Pt2^xxvii—Sr1—Pt5^xxx	64.5 (4)	61.6 (3)	67.5 (4)
Pt2^xxvii—Sr1—Pt5^xxxi	169.3 (4)	166.1 (3)	172.7 (4)
Pt2^xxvii—Sr1—Pt5^xxxii	64.4 (4)	62.0 (3)	66.6 (4)
Pt2^xxvii—Sr1—As1^xxiv	41.51 (3)	39.45 (3)	43.61 (4)
Pt2^xxvii—Sr1—As1^xxv	86.26 (5)	83.75 (5)	88.68 (5)
Pt3^xxiv—Sr1—Pt3^xxvii	109.91 (5)	108.89 (2)	111.06 (2)
Pt3^xxiv—Sr1—Pt3^xxviii	69.71 (3)	63.70 (3)	75.96 (4)
Pt3^xxiv—Sr1—Pt3^xxv	172.91 (7)	171.67 (8)	175.16 (7)
Pt3^xxiv—Sr1—Pt4^xxiv	49.51 (3)	48.52 (2)	50.65 (2)
Pt3^xxiv—Sr1—Pt4ⁱ	92.70 (5)	90.45 (4)	95.13 (4)
Pt3^xxiv—Sr1—Pt4^xxv	135.64 (5)	132.50 (5)	138.92 (5)
Pt3^xxiv—Sr1—Pt4^viii	91.21 (4)	85.04 (4)	97.54 (4)
Pt3^xxiv—Sr1—Pt5ⁱ	92.9 (7)	92.1 (7)	93.8 (7)
Pt3^xxiv—Sr1—Pt5^viii	92.8 (7)	92.7 (7)	93.0 (7)
Pt3^xxiv—Sr1—Pt5^xxix	44.7 (3)	41.1 (2)	48.4 (3)
Pt3^xxiv—Sr1—Pt5^xxx	139.0 (2)	137.2 (2)	141.0 (2)
Pt3^xxiv—Sr1—Pt5^xxxi	44.7 (3)	40.7 (2)	48.8 (3)
Pt3^xxiv—Sr1—Pt5^xxxii	139.0 (2)	137.8 (2)	139.9 (3)
Pt3^xxiv—Sr1—As1^xxiv	88.65 (5)	87.99 (4)	89.43 (4)
Pt3^xxiv—Sr1—As1^xxv	87.44 (4)	83.05 (5)	91.97 (5)
Pt3^xxvii—Sr1—Pt3^xxviii	172.79 (7)	171.51 (8)	175.09 (7)
Pt3^xxvii—Sr1—Pt3^xxv	69.83 (3)	63.70 (3)	75.96 (4)
Pt3^xxvii—Sr1—Pt4^xxiv	92.30 (5)	90.06 (3)	94.70 (4)
Pt3^xxvii—Sr1—Pt4ⁱ	49.91 (3)	49.11 (2)	50.83 (2)
Pt3^xxvii—Sr1—Pt4^xxv	91.74 (4)	85.61 (4)	97.83 (4)
Pt3^xxvii—Sr1—Pt4^viii	135.37 (5)	132.41 (5)	138.34 (5)
Pt3^xxvii—Sr1—Pt5ⁱ	92.8 (7)	92.6 (7)	93.0 (7)
Pt3^xxvii—Sr1—Pt5^viii	93.0 (7)	92.2 (6)	93.9 (7)
Pt3^xxvii—Sr1—Pt5^xxix	138.6 (2)	137.4 (2)	139.7 (3)
Pt3^xxvii—Sr1—Pt5^xxx	45.3 (3)	41.3 (2)	49.3 (3)
Pt3^xxvii—Sr1—Pt5^xxxi	138.5 (2)	136.7 (2)	140.5 (2)
Pt3^xxvii—Sr1—Pt5^xxxii	45.1 (3)	41.4 (2)	48.8 (3)
Pt3^xxvii—Sr1—As1^xxiv	42.70 (3)	41.74 (4)	43.65 (4)
Pt3^xxvii—Sr1—As1^xxv	131.77 (6)	128.65 (6)	134.68 (5)
Pt3^xxviii—Sr1—Pt3^xxv	109.92 (5)	108.89 (2)	111.06 (2)
Pt3^xxviii—Sr1—Pt4^xxiv	91.63 (4)	85.61 (4)	97.83 (4)
Pt3^xxviii—Sr1—Pt4ⁱ	135.32 (5)	132.41 (5)	138.34 (5)
Pt3^xxviii—Sr1—Pt4^xxv	92.28 (5)	90.06 (3)	94.70 (4)
Pt3^xxviii—Sr1—Pt4^viii	49.90 (3)	49.11 (2)	50.83 (2)
Pt3^xxviii—Sr1—Pt5ⁱ	93.0 (7)	92.2 (6)	93.9 (7)
Pt3^xxviii—Sr1—Pt5^viii	92.8 (7)	92.6 (7)	93.0 (7)
Pt3^xxviii—Sr1—Pt5^xxix	45.0 (3)	41.4 (2)	48.8 (3)
Pt3^xxviii—Sr1—Pt5^xxx	138.5 (2)	136.7 (2)	140.5 (2)
Pt3^xxviii—Sr1—Pt5^xxxi	45.2 (3)	41.3 (2)	49.3 (3)
Pt3^xxviii—Sr1—Pt5^xxxii	138.6 (2)	137.4 (2)	139.7 (3)
Pt3^xxviii—Sr1—As1^xxiv	131.71 (6)	128.65 (6)	134.68 (5)
Pt3^xxviii—Sr1—As1^xxv	42.69 (3)	41.74 (4)	43.65 (4)
Pt3^xxv—Sr1—Pt4^xxiv	135.69 (5)	132.50 (5)	138.92 (5)
Pt3^xxv—Sr1—Pt4ⁱ	91.33 (4)	85.04 (4)	97.54 (4)
Pt3^xxv—Sr1—Pt4^xxv	49.52 (3)	48.52 (2)	50.65 (2)
Pt3^xxv—Sr1—Pt4^viii	92.73 (5)	90.45 (4)	95.13 (4)
Pt3^xxv—Sr1—Pt5ⁱ	92.8 (7)	92.7 (7)	93.0 (7)
Pt3^xxv—Sr1—Pt5^viii	92.9 (7)	92.1 (7)	93.8 (7)
Pt3^xxv—Sr1—Pt5^xxix	139.0 (2)	137.8 (2)	139.9 (3)
Pt3^xxv—Sr1—Pt5^xxx	44.8 (3)	40.7 (2)	48.8 (3)
Pt3^xxv—Sr1—Pt5^xxxi	139.0 (2)	137.2 (2)	141.0 (2)
Pt3^xxv—Sr1—Pt5^xxxii	44.7 (3)	41.1 (2)	48.4 (3)
Pt3^xxv—Sr1—As1^xxiv	87.53 (4)	83.05 (5)	91.97 (5)
Pt3^xxv—Sr1—As1^xxv	88.65 (5)	87.99 (4)	89.43 (4)
Pt4^xxiv—Sr1—Pt4ⁱ	49.88 (3)	48.45 (3)	51.17 (3)
Pt4^xxiv—Sr1—Pt4^xxv	93.14 (5)	88.84 (6)	97.58 (6)
Pt4^xxiv—Sr1—Pt4^viii	71.86 (4)	64.35 (4)	79.34 (4)
Pt4^xxiv—Sr1—Pt5ⁱ	46.7 (5)	44.2 (5)	49.1 (5)
Pt4^xxiv—Sr1—Pt5^viii	46.7 (5)	44.7 (5)	48.5 (5)
Pt4^xxiv—Sr1—Pt5^xxix	46.6 (3)	43.9 (2)	49.3 (3)
Pt4^xxiv—Sr1—Pt5^xxx	93.9 (3)	91.8 (3)	96.1 (3)
Pt4^xxiv—Sr1—Pt5^xxxi	46.5 (3)	44.3 (2)	48.7 (3)
Pt4^xxiv—Sr1—Pt5^xxxii	93.9 (3)	93.2 (3)	94.4 (3)
Pt4^xxiv—Sr1—As1^xxiv	106.44 (5)	103.48 (3)	109.56 (3)
Pt4^xxiv—Sr1—As1^xxv	129.27 (5)	123.68 (6)	135.06 (7)
Pt4ⁱ—Sr1—Pt4^xxv	71.97 (4)	64.35 (4)	79.34 (4)
Pt4ⁱ—Sr1—Pt4^viii	91.90 (5)	88.17 (6)	95.83 (6)
Pt4ⁱ—Sr1—Pt5ⁱ	46.0 (5)	44.2 (5)	47.6 (5)
Pt4ⁱ—Sr1—Pt5^viii	46.2 (5)	43.9 (5)	48.3 (5)
Pt4ⁱ—Sr1—Pt5^xxix	93.5 (3)	92.9 (3)	94.0 (3)
Pt4ⁱ—Sr1—Pt5^xxx	46.7 (3)	44.1 (2)	49.1 (3)
Pt4ⁱ—Sr1—Pt5^xxxi	93.4 (3)	91.3 (3)	95.6 (3)
Pt4ⁱ—Sr1—Pt5^xxxii	46.6 (3)	43.8 (2)	49.3 (3)
Pt4ⁱ—Sr1—As1^xxiv	85.88 (4)	84.19 (3)	87.67 (3)
Pt4ⁱ—Sr1—As1^xxv	175.14 (6)	173.28 (9)	179.68 (6)
Pt4^xxv—Sr1—Pt4^viii	49.89 (3)	48.45 (3)	51.17 (3)
Pt4^xxv—Sr1—Pt5ⁱ	46.7 (5)	44.7 (5)	48.5 (5)
Pt4^xxv—Sr1—Pt5^viii	46.7 (5)	44.2 (5)	49.1 (5)
Pt4^xxv—Sr1—Pt5^xxix	93.9 (3)	93.2 (3)	94.4 (3)
Pt4^xxv—Sr1—Pt5^xxx	46.5 (3)	44.3 (2)	48.7 (3)
Pt4^xxv—Sr1—Pt5^xxxi	93.8 (3)	91.8 (3)	96.1 (3)
Pt4^xxv—Sr1—Pt5^xxxii	46.6 (3)	43.9 (2)	49.3 (3)
Pt4^xxv—Sr1—As1^xxiv	129.38 (5)	123.68 (6)	135.06 (7)
Pt4^xxv—Sr1—As1^xxv	106.41 (5)	103.48 (3)	109.56 (3)
Pt4^viii—Sr1—Pt5ⁱ	46.2 (5)	43.9 (5)	48.3 (5)
Pt4^viii—Sr1—Pt5^viii	46.0 (5)	44.2 (5)	47.6 (5)
Pt4^viii—Sr1—Pt5^xxix	46.6 (3)	43.8 (2)	49.3 (3)
Pt4^viii—Sr1—Pt5^xxx	93.4 (3)	91.3 (3)	95.6 (3)
Pt4^viii—Sr1—Pt5^xxxi	46.6 (3)	44.1 (2)	49.1 (3)
Pt4^viii—Sr1—Pt5^xxxii	93.5 (3)	92.9 (3)	94.0 (3)
Pt4^viii—Sr1—As1^xxiv	175.14 (6)	173.28 (9)	179.68 (6)
Pt4^viii—Sr1—As1^xxv	85.86 (4)	84.19 (3)	87.67 (3)
Pt5ⁱ—Sr1—Pt5^viii	0.6 (9)	0.1 (3)	1.2 (12)
Pt5ⁱ—Sr1—Pt5^xxix	63.3 (6)	60.9 (4)	65.8 (4)
Pt5ⁱ—Sr1—Pt5^xxx	62.9 (6)	59.3 (7)	66.4 (6)
Pt5ⁱ—Sr1—Pt5^xxxi	63.2 (6)	60.3 (6)	65.9 (6)
Pt5ⁱ—Sr1—Pt5^xxxii	63.1 (6)	60.7 (4)	65.4 (4)
Pt5ⁱ—Sr1—As1^xxiv	131.8 (3)	130.65 (18)	133.0 (2)
Pt5ⁱ—Sr1—As1^xxv	132.0 (3)	130.7 (2)	133.3 (2)
Pt5^viii—Sr1—Pt5^xxix	63.1 (6)	60.7 (4)	65.4 (4)
Pt5^viii—Sr1—Pt5^xxx	63.2 (6)	60.3 (6)	65.9 (6)
Pt5^viii—Sr1—Pt5^xxxi	63.0 (6)	59.3 (7)	66.4 (6)
Pt5^viii—Sr1—Pt5^xxxii	63.3 (6)	60.9 (4)	65.8 (4)
Pt5^viii—Sr1—As1^xxiv	132.0 (3)	130.7 (2)	133.3 (2)
Pt5^viii—Sr1—As1^xxv	131.8 (3)	130.65 (18)	133.0 (2)
Pt5^xxix—Sr1—Pt5^xxx	126.3 (5)	123.9 (5)	128.7 (5)
Pt5^xxix—Sr1—Pt5^xxxi	1.8 (5)	0.1 (2)	3.0 (6)
Pt5^xxix—Sr1—Pt5^xxxii	126.4 (5)	126.1 (5)	126.9 (6)
Pt5^xxix—Sr1—As1^xxiv	133.3 (2)	129.6 (2)	136.9 (3)
Pt5^xxix—Sr1—As1^xxv	85.1 (3)	80.8 (3)	89.5 (3)
Pt5^xxx—Sr1—Pt5^xxxi	126.1 (5)	121.0 (6)	131.2 (5)
Pt5^xxx—Sr1—Pt5^xxxii	1.8 (5)	0.1 (3)	3.0 (6)
Pt5^xxx—Sr1—As1^xxiv	85.4 (3)	80.8 (3)	90.0 (3)
Pt5^xxx—Sr1—As1^xxv	133.3 (2)	129.6 (2)	136.9 (3)
Pt5^xxxi—Sr1—Pt5^xxxii	126.3 (5)	123.9 (6)	128.7 (5)
Pt5^xxxi—Sr1—As1^xxiv	133.3 (2)	129.6 (2)	136.9 (3)
Pt5^xxxi—Sr1—As1^xxv	85.3 (3)	80.8 (3)	90.0 (3)
Pt5^xxxii—Sr1—As1^xxiv	85.2 (3)	80.8 (3)	89.5 (3)
Pt5^xxxii—Sr1—As1^xxv	133.3 (2)	129.6 (2)	136.9 (3)
As1^xxiv—Sr1—As1^xxv	96.08 (5)	95.42 (6)	96.89 (6)
Pt1—As1—Pt1^xxxiii	180.0 (5)	180.0 (5)	180.0 (5)
Pt1—As1—Pt2^xxxiii	125.75 (4)	125.71 (4)	125.79 (4)
Pt1—As1—Pt2^xxxiv	125.75 (4)	125.71 (4)	125.79 (4)
Pt1—As1—Pt3^xxxiii	124.79 (4)	124.77 (4)	124.81 (4)
Pt1—As1—Pt3^xxxiv	124.79 (4)	124.77 (4)	124.81 (4)
Pt1—As1—Sr1ⁱⁱ	64.44 (3)	61.93 (3)	67.04 (3)
Pt1—As1—Sr1ⁱⁱⁱ	64.44 (3)	61.93 (3)	67.04 (3)
Pt1—As1—Sr1^iv	64.46 (3)	61.93 (3)	67.04 (3)
Pt1—As1—Sr1^v	64.46 (3)	61.93 (3)	67.04 (3)
Pt1^xxxiii—As1—Pt2^xxxiii	54.25 (4)	54.21 (4)	54.29 (4)
Pt1^xxxiii—As1—Pt2^xxxiv	54.25 (4)	54.21 (4)	54.29 (4)
Pt1^xxxiii—As1—Pt3^xxxiii	55.21 (4)	55.19 (4)	55.23 (4)
Pt1^xxxiii—As1—Pt3^xxxiv	55.21 (4)	55.19 (4)	55.23 (4)
Pt1^xxxiii—As1—Sr1ⁱⁱ	115.56 (3)	112.96 (3)	118.07 (3)
Pt1^xxxiii—As1—Sr1ⁱⁱⁱ	115.56 (3)	112.96 (3)	118.07 (3)
Pt1^xxxiii—As1—Sr1^iv	115.54 (3)	112.96 (3)	118.07 (3)
Pt1^xxxiii—As1—Sr1^v	115.54 (3)	112.96 (3)	118.07 (3)
Pt2^xxxiii—As1—Pt2^xxxiv	108.50 (7)	108.43 (7)	108.58 (7)
Pt2^xxxiii—As1—Pt3^xxxiii	70.53 (4)	69.94 (4)	71.17 (5)
Pt2^xxxiii—As1—Pt3^xxxiv	70.52 (4)	69.94 (4)	71.17 (5)
Pt2^xxxiii—As1—Sr1ⁱⁱ	76.132 (12)	71.790 (18)	80.346 (18)
Pt2^xxxiii—As1—Sr1ⁱⁱⁱ	138.03 (3)	135.77 (4)	140.24 (4)
Pt2^xxxiii—As1—Sr1^iv	76.093 (12)	71.790 (18)	80.346 (18)
Pt2^xxxiii—As1—Sr1^v	138.05 (3)	135.77 (4)	140.24 (4)
Pt2^xxxiv—As1—Pt3^xxxiii	70.52 (4)	69.94 (4)	71.17 (5)
Pt2^xxxiv—As1—Pt3^xxxiv	70.53 (4)	69.94 (4)	71.17 (5)
Pt2^xxxiv—As1—Sr1ⁱⁱ	138.03 (3)	135.77 (4)	140.24 (4)
Pt2^xxxiv—As1—Sr1ⁱⁱⁱ	76.132 (12)	71.790 (18)	80.346 (18)
Pt2^xxxiv—As1—Sr1^iv	138.05 (3)	135.77 (4)	140.24 (4)
Pt2^xxxiv—As1—Sr1^v	76.093 (12)	71.790 (18)	80.346 (18)
Pt3^xxxiii—As1—Pt3^xxxiv	110.42 (7)	110.38 (7)	110.47 (7)
Pt3^xxxiii—As1—Sr1ⁱⁱ	72.43 (3)	71.96 (3)	72.89 (3)
Pt3^xxxiii—As1—Sr1ⁱⁱⁱ	142.63 (3)	138.87 (3)	146.29 (3)
Pt3^xxxiii—As1—Sr1^iv	142.60 (3)	138.87 (3)	146.29 (3)
Pt3^xxxiii—As1—Sr1^v	72.43 (3)	71.96 (3)	72.89 (3)
Pt3^xxxiv—As1—Sr1ⁱⁱ	142.63 (3)	138.87 (3)	146.29 (3)
Pt3^xxxiv—As1—Sr1ⁱⁱⁱ	72.43 (3)	71.96 (3)	72.89 (3)
Pt3^xxxiv—As1—Sr1^iv	72.43 (3)	71.96 (3)	72.89 (3)
Pt3^xxxiv—As1—Sr1^v	142.60 (3)	138.87 (3)	146.29 (3)
Sr1ⁱⁱ—As1—Sr1ⁱⁱⁱ	128.89 (7)	123.85 (7)	134.07 (7)
Sr1ⁱⁱ—As1—Sr1^iv	83.92 (5)	83.84 (5)	84.00 (6)
Sr1ⁱⁱ—As1—Sr1^v	74.69 (4)	74.61 (4)	74.77 (6)
Sr1ⁱⁱⁱ—As1—Sr1^iv	74.69 (4)	74.61 (4)	74.77 (6)
Sr1ⁱⁱⁱ—As1—Sr1^v	83.92 (5)	83.84 (5)	84.00 (6)
Sr1^iv—As1—Sr1^v	128.93 (7)	123.85 (7)	134.07 (7)

Symmetry codes: (i) −x₁+1/2, −x₂+3/2, x₃+1/2, x₄; (ii) x₁, x₂−1/2, x₃+1/2, x₄; (iii) −x₁+1/2, −x₂+1, x₃, x₄; (iv) −x₁, −x₂+1, −x₃, −x₄; (v) x₁+1/2, x₂−1/2, −x₃+1/2, −x₄; (vi) x₁, x₂, x₃−1, x₄; (vii) −x₁, x₂, −x₃, −x₄+1/2; (viii) x₁−1/2, −x₂+3/2, −x₃+1/2, −x₄+1/2; (ix) x₁, x₂−1/2, x₃−1/2, x₄; (x) −x₁, −x₂+1, −x₃−1, −x₄; (xi) −x₁, x₂, −x₃+1, −x₄+1/2; (xii) −x₁+1/2, −x₂, x₃−1, x₄; (xiii) −x₁+1, x₂, −x₃, −x₄+1/2; (xiv) x₁−1/2, x₂, −x₃, −x₄; (xv) −x₁+1/2, x₂, x₃, x₄+1/2; (xvi) x₁+1/2, x₂−1/2, −x₃−1/2, −x₄; (xvii) −x₁+1/2, −x₂, x₃, x₄; (xviii) x₁−1/2, −x₂, −x₃, −x₄+1/2; (xix) −x₁+1, −x₂, −x₃, −x₄; (xx) x₁, −x₂, x₃, x₄+1/2; (xxi) −x₁, −x₂+3/2, −x₃+1/2, −x₄; (xxii) −x₁+1, −x₂, −x₃−1, −x₄; (xxiii) x₁, −x₂, x₃−1, x₄+1/2; (xxiv) x₁, x₂+1/2, x₃−1/2, x₄; (xxv) −x₁, x₂+1/2, −x₃+1/2, −x₄+1/2; (xxvi) x₁+1/2, −x₂, −x₃, −x₄+1/2; (xxvii) x₁, x₂+1/2, x₃+1/2, x₄; (xxviii) −x₁, x₂+1/2, −x₃−1/2, −x₄+1/2; (xxix) x₁−1/2, x₂+1/2, −x₃−1/2, −x₄; (xxx) x₁−1/2, x₂+1/2, −x₃+1/2, −x₄; (xxxi) −x₁+1/2, x₂+1/2, x₃−1/2, x₄+1/2; (xxxii) −x₁+1/2, x₂+1/2, x₃+1/2, x₄+1/2; (xxxiii) x₁, x₂, x₃+1, x₄; (xxxiv) −x₁+1/2, −x₂+3/2, x₃+3/2, x₄.

(III) top

Crystal data top

AsPt_7.285Sr₂	F(000) = 2709
M_r = 1671.3	D_x = 13.537 Mg m⁻³
Orthorhombic, Amma(00γ)ss0†	Mo Kα radiation, λ = 0.71073 Å
q = 0.603800c*	Cell parameters from 3790 reflections
a = 7.9509 Å	θ = 3.8–26.4°
b = 18.1042 Å	µ = 140.54 mm⁻¹
c = 5.6972 Å	T = 293 K
V = 820.08 (8) Å³	Plate, metallic dark black
Z = 4	0.01 × 0.01 × 0.002 mm

Data collection top

SuperNova, Dual, Cu at zero, Atlas diffractometer	1220 independent reflections
Radiation source: X-ray tube	781 reflections with I > 3σ(I)
Mirror monochromator	R_int = 0.092
Detector resolution: 5.1333 pixels mm^-1	θ_max = 26.4°, θ_min = 3.8°
ω scans	h = −9→8
Absorption correction: multi-scan CrysAlisPro, Agilent Technologies, Version 1.171.37.34 (release 22-05-2014 CrysAlis171 .NET) (compiled May 22 2014,16:03:01) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm.	k = −22→22
T_min = 0.279, T_max = 1.0	l = −7→7
10459 measured reflections

Refinement top

Refinement on F	2 constraints
R[F² > 2σ(F²)] = 0.030	Weighting scheme based on measured s.u.'s w = 1/(σ²(F) + 0.0001F²)
wR(F²) = 0.039	(Δ/σ)_max = 0.043
S = 1.32	Δρ_max = 4.57 e Å⁻³
1220 reflections	Δρ_min = −3.30 e Å⁻³
55 parameters	Extinction correction: B-C type 1 Gaussian isotropic (Becker & Coppens, 1974)
0 restraints	Extinction coefficient: 226 (8)

Special details top

Refinement. Occupancy of the Pt5 position is approximated by the harmonic function without any constrains

Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å²) top

	x	y	z	U_iso*/U_eq	Occ. (<1)
Pt1	0.25	0.5	0.33956 (13)	0.0043 (2)
Pt2	0	0.5	0	0.0048 (2)
Pt3	0.25	0.38864 (3)	−0.00543 (9)	0.00488 (18)
Pt4	0.25	0.25139 (3)	0.25001 (9)	0.00685 (18)
Pt5	0.4998 (2)	0.3003 (7)	0.012 (5)	0.0071 (10)	0.3213 (13)
Sr1	0	0.87896 (8)	0	0.0067 (4)
As1	0.25	0.5	0.7485 (3)	0.0024 (5)

Atomic displacement parameters (Å²) top

	U¹¹	U²²	U³³	U¹²	U¹³	U²³
Pt1	0.0052 (3)	0.0050 (4)	0.0028 (4)	0	0	0
Pt2	0.0007 (4)	0.0083 (4)	0.0052 (4)	0	0.0000 (2)	0
Pt3	0.0071 (3)	0.0018 (3)	0.0057 (3)	0	0	0.00006 (19)
Pt4	0.0120 (3)	0.0042 (3)	0.0043 (3)	0	0	0.0016 (2)
Pt5	0.0028 (4)	0.0069 (6)	0.012 (3)	0.0002 (5)	0.0001 (3)	−0.0012 (8)
Sr1	0.0024 (6)	0.0063 (8)	0.0115 (7)	0	−0.0006 (5)	0
As1	0.0011 (8)	0.0034 (10)	0.0026 (9)	0	0	0

Geometric parameters (Å, º) top

	Average	Minimum	Maximum
Pt1—Pt2	2.7756 (5)	2.7737 (5)	2.7776 (5)
Pt1—Pt2ⁱ	2.7756 (5)	2.7737 (5)	2.7776 (5)
Pt1—Pt3	2.8169 (7)	2.8157 (7)	2.8181 (7)
Pt1—Pt3ⁱ	2.8169 (7)	2.8157 (7)	2.8181 (7)
Pt1—Sr1ⁱⁱ	3.0981 (18)	3.048 (2)	3.151 (2)
Pt1—Sr1ⁱⁱⁱ	3.0981 (18)	3.048 (2)	3.151 (2)
Pt1—Sr1^iv	3.0988 (18)	3.048 (2)	3.151 (2)
Pt1—Sr1^v	3.0988 (18)	3.048 (2)	3.151 (2)
Pt1—As1^vi	3.367 (2)	3.367 (2)	3.367 (2)
Pt1—As1	2.330 (2)	2.330 (2)	2.330 (2)
Pt2—Pt3	2.8344 (10)	2.8158 (11)	2.8592 (11)
Pt2—Pt3ⁱ	2.8345 (10)	2.8158 (11)	2.8592 (11)
Pt2—Pt3^vii	2.8345 (10)	2.8158 (11)	2.8592 (11)
Pt2—Pt3^viii	2.8344 (10)	2.8158 (11)	2.8592 (11)
Pt2—Sr1^ix	3.5945 (14)	3.3808 (18)	3.8071 (18)
Pt2—Sr1ⁱⁱ	3.5934 (14)	3.3808 (18)	3.8071 (18)
Pt2—Sr1^x	3.5934 (14)	3.3808 (18)	3.8071 (18)
Pt2—Sr1^iv	3.5945 (14)	3.3808 (18)	3.8071 (18)
Pt2—As1^vi	2.4525 (11)	2.4503 (11)	2.4547 (11)
Pt2—As1^xi	2.4525 (11)	2.4503 (11)	2.4547 (11)
Pt3—Pt4	2.8816 (7)	2.8796 (7)	2.8836 (7)
Pt3—Pt4^xii	2.8943 (7)	2.8927 (7)	2.8959 (7)
Pt3—Pt5	2.573 (10)	2.400 (13)	2.704 (13)
Pt3—Pt5^xiii	2.571 (10)	2.401 (13)	2.704 (13)
Pt3—Pt5^xiv	2.571 (10)	2.401 (13)	2.704 (13)
Pt3—Pt5^xv	2.573 (10)	2.400 (13)	2.704 (13)
Pt3—Sr1^ix	3.4557 (16)	3.385 (3)	3.528 (3)
Pt3—Sr1ⁱⁱ	3.5054 (16)	3.433 (3)	3.581 (3)
Pt3—Sr1^xvi	3.4548 (16)	3.385 (3)	3.528 (3)
Pt3—Sr1^v	3.5063 (16)	3.433 (3)	3.581 (3)
Pt3—As1^vi	2.4570 (12)	2.4556 (12)	2.4584 (12)
Pt4—Pt4^xii	2.8550 (7)	2.8490 (8)	2.8608 (8)
Pt4—Pt4^xvii	2.8549 (7)	2.8491 (8)	2.8608 (8)
Pt4—Pt5	2.602 (19)	2.45 (2)	2.69 (2)
Pt4—Pt5^xvii	2.65 (2)	2.54 (3)	2.79 (3)
Pt4—Pt5^xiii	2.63 (2)	2.52 (3)	2.77 (3)
Pt4—Pt5^xviii	2.613 (18)	2.47 (2)	2.71 (2)
Pt4—Pt5^xix	2.615 (18)	2.47 (2)	2.71 (2)
Pt4—Pt5^xiv	2.63 (2)	2.52 (3)	2.77 (3)
Pt4—Pt5^xx	2.66 (2)	2.54 (3)	2.79 (3)
Pt4—Pt5^xv	2.602 (19)	2.45 (2)	2.69 (2)
Pt4—Sr1ⁱⁱ	3.368 (2)	3.273 (3)	3.463 (3)
Pt4—Sr1ⁱ	3.404 (2)	3.324 (3)	3.483 (3)
Pt4—Sr1^xxi	3.403 (2)	3.324 (3)	3.483 (3)
Pt4—Sr1^v	3.369 (2)	3.273 (3)	3.463 (3)
Pt5—Pt5^xiii	0.14 (4)	0.13 (6)	0.14 (6)
Pt5—Pt5^xxii	3.54 (4)	3.38 (5)	3.62 (5)
Pt5—Pt5^xix	3.18 (5)	3.12 (5)	3.28 (5)
Pt5—Pt5^xxiii	3.35 (5)	3.24 (5)	3.51 (5)
Pt5—Pt5^xx	3.35 (5)	3.24 (5)	3.51 (5)
Pt5—Sr1ⁱ	3.228 (16)	3.12 (2)	3.37 (2)
Pt5—Sr1^xvi	3.24 (3)	3.15 (4)	3.35 (4)
Pt5—Sr1^v	3.11 (3)	3.03 (4)	3.23 (4)
Sr1—As1^xxiv	3.2808 (19)	3.210 (3)	3.355 (3)
Sr1—As1^xxv	3.2822 (19)	3.210 (3)	3.355 (3)

Pt2—Pt1—Pt2ⁱ	91.63 (2)	91.55 (2)	91.71 (2)
Pt2—Pt1—Pt3	60.90 (2)	60.42 (2)	61.45 (3)
Pt2—Pt1—Pt3ⁱ	60.90 (2)	60.42 (2)	61.45 (3)
Pt2—Pt1—Sr1ⁱⁱ	75.229 (12)	70.673 (18)	79.728 (17)
Pt2—Pt1—Sr1ⁱⁱⁱ	131.69 (3)	130.76 (3)	132.61 (3)
Pt2—Pt1—Sr1^iv	75.246 (12)	70.673 (18)	79.728 (17)
Pt2—Pt1—Sr1^v	131.70 (3)	130.76 (3)	132.61 (3)
Pt2—Pt1—As1^vi	45.815 (11)	45.777 (11)	45.854 (11)
Pt2—Pt1—As1	134.185 (11)	134.146 (11)	134.223 (11)
Pt2ⁱ—Pt1—Pt3	60.90 (2)	60.42 (2)	61.45 (3)
Pt2ⁱ—Pt1—Pt3ⁱ	60.90 (2)	60.42 (2)	61.45 (3)
Pt2ⁱ—Pt1—Sr1ⁱⁱ	131.69 (3)	130.76 (3)	132.61 (3)
Pt2ⁱ—Pt1—Sr1ⁱⁱⁱ	75.229 (12)	70.673 (18)	79.728 (17)
Pt2ⁱ—Pt1—Sr1^iv	131.70 (3)	130.76 (3)	132.61 (3)
Pt2ⁱ—Pt1—Sr1^v	75.246 (12)	70.673 (18)	79.728 (17)
Pt2ⁱ—Pt1—As1^vi	45.815 (11)	45.777 (11)	45.854 (11)
Pt2ⁱ—Pt1—As1	134.185 (11)	134.146 (11)	134.223 (11)
Pt3—Pt1—Pt3ⁱ	91.51 (3)	91.46 (3)	91.55 (3)
Pt3—Pt1—Sr1ⁱⁱ	72.51 (3)	71.52 (3)	73.51 (3)
Pt3—Pt1—Sr1ⁱⁱⁱ	135.44 (3)	131.25 (2)	139.62 (2)
Pt3—Pt1—Sr1^iv	135.45 (3)	131.25 (2)	139.62 (2)
Pt3—Pt1—Sr1^v	72.52 (3)	71.52 (3)	73.51 (3)
Pt3—Pt1—As1^vi	45.753 (15)	45.729 (15)	45.777 (15)
Pt3—Pt1—As1	134.247 (15)	134.223 (15)	134.271 (15)
Pt3ⁱ—Pt1—Sr1ⁱⁱ	135.44 (3)	131.25 (2)	139.62 (2)
Pt3ⁱ—Pt1—Sr1ⁱⁱⁱ	72.51 (3)	71.52 (3)	73.51 (3)
Pt3ⁱ—Pt1—Sr1^iv	72.52 (3)	71.52 (3)	73.51 (3)
Pt3ⁱ—Pt1—Sr1^v	135.45 (3)	131.25 (2)	139.62 (2)
Pt3ⁱ—Pt1—As1^vi	45.753 (15)	45.729 (15)	45.777 (15)
Pt3ⁱ—Pt1—As1	134.247 (15)	134.223 (15)	134.271 (15)
Sr1ⁱⁱ—Pt1—Sr1ⁱⁱⁱ	145.72 (3)	140.02 (4)	151.48 (4)
Sr1ⁱⁱ—Pt1—Sr1^iv	90.17 (4)	90.09 (4)	90.25 (5)
Sr1ⁱⁱ—Pt1—Sr1^v	79.96 (4)	79.88 (3)	80.05 (6)
Sr1ⁱⁱ—Pt1—As1^vi	107.14 (2)	104.26 (4)	109.99 (4)
Sr1ⁱⁱ—Pt1—As1	72.86 (2)	70.01 (4)	75.74 (4)
Sr1ⁱⁱⁱ—Pt1—Sr1^iv	79.96 (4)	79.88 (3)	80.05 (6)
Sr1ⁱⁱⁱ—Pt1—Sr1^v	90.17 (4)	90.09 (4)	90.25 (5)
Sr1ⁱⁱⁱ—Pt1—As1^vi	107.14 (2)	104.26 (4)	109.99 (4)
Sr1ⁱⁱⁱ—Pt1—As1	72.86 (2)	70.01 (4)	75.74 (4)
Sr1^iv—Pt1—Sr1^v	145.69 (3)	140.02 (4)	151.48 (4)
Sr1^iv—Pt1—As1^vi	107.15 (2)	104.26 (4)	109.99 (4)
Sr1^iv—Pt1—As1	72.85 (2)	70.01 (4)	75.74 (4)
Sr1^v—Pt1—As1^vi	107.15 (2)	104.26 (4)	109.99 (4)
Sr1^v—Pt1—As1	72.85 (2)	70.01 (4)	75.74 (4)
As1^vi—Pt1—As1	180.0 (5)	180.0 (5)	180.0 (5)
Pt1—Pt2—Pt1^vii	176.20 (4)	173.96 (4)	180.0 (5)
Pt1—Pt2—Pt3	60.269 (14)	59.974 (16)	60.503 (15)
Pt1—Pt2—Pt3ⁱ	60.269 (14)	59.974 (16)	60.503 (15)
Pt1—Pt2—Pt3^vii	119.63 (2)	114.88 (3)	124.22 (3)
Pt1—Pt2—Pt3^viii	119.63 (2)	114.88 (3)	124.22 (3)
Pt1—Pt2—Sr1^ix	123.55 (2)	121.21 (3)	125.86 (3)
Pt1—Pt2—Sr1ⁱⁱ	56.446 (17)	54.361 (17)	58.54 (2)
Pt1—Pt2—Sr1^x	123.55 (2)	121.21 (3)	125.86 (3)
Pt1—Pt2—Sr1^iv	56.444 (17)	54.361 (17)	58.54 (2)
Pt1—Pt2—As1^vi	79.93 (4)	79.86 (4)	80.01 (4)
Pt1—Pt2—As1^xi	99.88 (4)	99.78 (4)	99.99 (4)
Pt1^vii—Pt2—Pt3	119.63 (2)	114.88 (3)	124.22 (3)
Pt1^vii—Pt2—Pt3ⁱ	119.63 (2)	114.88 (3)	124.22 (3)
Pt1^vii—Pt2—Pt3^vii	60.269 (14)	59.974 (16)	60.503 (15)
Pt1^vii—Pt2—Pt3^viii	60.269 (14)	59.974 (16)	60.503 (15)
Pt1^vii—Pt2—Sr1^ix	56.444 (17)	54.361 (17)	58.54 (2)
Pt1^vii—Pt2—Sr1ⁱⁱ	123.55 (2)	121.21 (3)	125.86 (3)
Pt1^vii—Pt2—Sr1^x	56.446 (17)	54.361 (17)	58.54 (2)
Pt1^vii—Pt2—Sr1^iv	123.55 (2)	121.21 (3)	125.86 (3)
Pt1^vii—Pt2—As1^vi	99.88 (4)	99.78 (4)	99.99 (4)
Pt1^vii—Pt2—As1^xi	79.93 (4)	79.86 (4)	80.01 (4)
Pt3—Pt2—Pt3ⁱ	90.78 (2)	90.749 (18)	90.81 (3)
Pt3—Pt2—Pt3^vii	89.22 (3)	81.72 (3)	96.78 (4)
Pt3—Pt2—Pt3^viii	175.25 (4)	172.47 (4)	180.0 (5)
Pt3—Pt2—Sr1^ix	63.74 (2)	61.83 (3)	65.71 (3)
Pt3—Pt2—Sr1ⁱⁱ	64.84 (2)	62.93 (3)	66.82 (3)
Pt3—Pt2—Sr1^x	115.15 (2)	113.472 (18)	116.74 (2)
Pt3—Pt2—Sr1^iv	116.24 (2)	114.556 (18)	117.85 (2)
Pt3—Pt2—As1^vi	54.81 (2)	54.47 (2)	55.09 (2)
Pt3—Pt2—As1^xi	125.09 (3)	119.40 (4)	130.64 (4)
Pt3ⁱ—Pt2—Pt3^vii	175.25 (4)	172.47 (4)	180.0 (5)
Pt3ⁱ—Pt2—Pt3^viii	89.22 (3)	81.72 (3)	96.78 (4)
Pt3ⁱ—Pt2—Sr1^ix	115.14 (2)	113.472 (18)	116.74 (2)
Pt3ⁱ—Pt2—Sr1ⁱⁱ	116.25 (2)	114.556 (18)	117.85 (2)
Pt3ⁱ—Pt2—Sr1^x	63.74 (2)	61.83 (3)	65.71 (3)
Pt3ⁱ—Pt2—Sr1^iv	64.85 (2)	62.93 (3)	66.82 (3)
Pt3ⁱ—Pt2—As1^vi	54.81 (2)	54.47 (2)	55.09 (2)
Pt3ⁱ—Pt2—As1^xi	125.09 (3)	119.40 (4)	130.64 (4)
Pt3^vii—Pt2—Pt3^viii	90.78 (2)	90.749 (18)	90.81 (3)
Pt3^vii—Pt2—Sr1^ix	64.85 (2)	62.93 (3)	66.82 (3)
Pt3^vii—Pt2—Sr1ⁱⁱ	63.74 (2)	61.83 (3)	65.71 (3)
Pt3^vii—Pt2—Sr1^x	116.25 (2)	114.556 (18)	117.85 (2)
Pt3^vii—Pt2—Sr1^iv	115.14 (2)	113.472 (18)	116.74 (2)
Pt3^vii—Pt2—As1^vi	125.09 (3)	119.40 (4)	130.64 (4)
Pt3^vii—Pt2—As1^xi	54.81 (2)	54.47 (2)	55.09 (2)
Pt3^viii—Pt2—Sr1^ix	116.24 (2)	114.556 (18)	117.85 (2)
Pt3^viii—Pt2—Sr1ⁱⁱ	115.15 (2)	113.472 (18)	116.74 (2)
Pt3^viii—Pt2—Sr1^x	64.84 (2)	62.93 (3)	66.82 (3)
Pt3^viii—Pt2—Sr1^iv	63.74 (2)	61.83 (3)	65.71 (3)
Pt3^viii—Pt2—As1^vi	125.09 (3)	119.40 (4)	130.64 (4)
Pt3^viii—Pt2—As1^xi	54.81 (2)	54.47 (2)	55.09 (2)
Sr1^ix—Pt2—Sr1ⁱⁱ	104.87 (4)	104.40 (4)	105.37 (5)
Sr1^ix—Pt2—Sr1^x	75.13 (4)	75.11 (4)	75.15 (4)
Sr1^ix—Pt2—Sr1^iv	179.70 (9)	179.52 (5)	180.0 (5)
Sr1^ix—Pt2—As1^vi	62.39 (4)	60.15 (5)	64.65 (6)
Sr1^ix—Pt2—As1^xi	117.60 (4)	115.13 (6)	120.03 (6)
Sr1ⁱⁱ—Pt2—Sr1^x	179.70 (9)	179.52 (5)	180.0 (5)
Sr1ⁱⁱ—Pt2—Sr1^iv	75.13 (4)	75.11 (4)	75.15 (4)
Sr1ⁱⁱ—Pt2—As1^vi	117.59 (4)	115.13 (6)	120.03 (6)
Sr1ⁱⁱ—Pt2—As1^xi	62.40 (4)	60.15 (5)	64.65 (6)
Sr1^x—Pt2—Sr1^iv	104.87 (4)	104.40 (4)	105.37 (5)
Sr1^x—Pt2—As1^vi	62.40 (4)	60.15 (5)	64.65 (6)
Sr1^x—Pt2—As1^xi	117.59 (4)	115.13 (6)	120.03 (6)
Sr1^iv—Pt2—As1^vi	117.60 (4)	115.13 (6)	120.03 (6)
Sr1^iv—Pt2—As1^xi	62.39 (4)	60.15 (5)	64.65 (6)
As1^vi—Pt2—As1^xi	175.69 (4)	173.17 (5)	180.0 (5)
Pt1—Pt3—Pt2	58.831 (17)	58.576 (15)	59.076 (16)
Pt1—Pt3—Pt2ⁱ	58.831 (17)	58.576 (15)	59.076 (16)
Pt1—Pt3—Pt4	105.38 (2)	105.32 (2)	105.44 (2)
Pt1—Pt3—Pt4^xii	164.43 (3)	164.33 (3)	164.53 (3)
Pt1—Pt3—Pt5	114.5 (5)	112.8 (5)	117.1 (6)
Pt1—Pt3—Pt5^xiii	117.5 (5)	114.9 (5)	119.8 (5)
Pt1—Pt3—Pt5^xiv	117.5 (5)	114.9 (5)	119.8 (5)
Pt1—Pt3—Pt5^xv	114.5 (5)	112.8 (5)	117.1 (6)
Pt1—Pt3—Sr1^ix	127.21 (4)	123.94 (4)	130.27 (4)
Pt1—Pt3—Sr1ⁱⁱ	57.45 (3)	57.35 (4)	57.57 (3)
Pt1—Pt3—Sr1^xvi	127.20 (4)	123.94 (4)	130.27 (4)
Pt1—Pt3—Sr1^v	57.45 (3)	57.35 (4)	57.57 (3)
Pt1—Pt3—As1^vi	79.04 (4)	78.99 (4)	79.08 (4)
Pt2—Pt3—Pt2ⁱ	89.21 (2)	89.18 (2)	89.24 (3)
Pt2—Pt3—Pt4	127.46 (5)	124.20 (5)	130.71 (5)
Pt2—Pt3—Pt4^xii	129.00 (5)	126.37 (5)	131.56 (5)
Pt2—Pt3—Pt5	172.2 (4)	169.3 (3)	176.0 (5)
Pt2—Pt3—Pt5^xiii	173.1 (3)	169.6 (2)	177.2 (3)
Pt2—Pt3—Pt5^xiv	84.0 (2)	80.4 (2)	88.0 (2)
Pt2—Pt3—Pt5^xv	83.9 (2)	80.4 (2)	87.9 (2)
Pt2—Pt3—Sr1^ix	68.89 (3)	65.21 (3)	72.41 (3)
Pt2—Pt3—Sr1ⁱⁱ	68.10 (3)	64.51 (3)	71.57 (3)
Pt2—Pt3—Sr1^xvi	116.60 (3)	116.01 (3)	117.03 (3)
Pt2—Pt3—Sr1^v	115.06 (3)	114.43 (3)	115.54 (3)
Pt2—Pt3—As1^vi	54.66 (2)	54.35 (2)	54.97 (2)
Pt2ⁱ—Pt3—Pt4	127.51 (5)	124.20 (5)	130.71 (5)
Pt2ⁱ—Pt3—Pt4^xii	128.96 (5)	126.37 (5)	131.56 (5)
Pt2ⁱ—Pt3—Pt5	83.9 (2)	80.4 (2)	87.9 (2)
Pt2ⁱ—Pt3—Pt5^xiii	84.0 (2)	80.4 (2)	88.0 (2)
Pt2ⁱ—Pt3—Pt5^xiv	173.1 (3)	169.6 (2)	177.2 (3)
Pt2ⁱ—Pt3—Pt5^xv	172.2 (4)	169.3 (3)	176.0 (5)
Pt2ⁱ—Pt3—Sr1^ix	116.60 (3)	116.01 (3)	117.03 (3)
Pt2ⁱ—Pt3—Sr1ⁱⁱ	115.06 (3)	114.43 (3)	115.54 (3)
Pt2ⁱ—Pt3—Sr1^xvi	68.87 (3)	65.21 (3)	72.41 (3)
Pt2ⁱ—Pt3—Sr1^v	68.11 (3)	64.51 (3)	71.57 (3)
Pt2ⁱ—Pt3—As1^vi	54.66 (2)	54.35 (2)	54.97 (2)
Pt4—Pt3—Pt4^xii	59.246 (18)	59.135 (18)	59.354 (18)
Pt4—Pt3—Pt5	56.6 (4)	54.4 (4)	58.0 (4)
Pt4—Pt3—Pt5^xiii	57.2 (4)	55.4 (4)	60.2 (4)
Pt4—Pt3—Pt5^xiv	57.2 (4)	55.4 (4)	60.2 (4)
Pt4—Pt3—Pt5^xv	56.6 (4)	54.4 (4)	58.0 (4)
Pt4—Pt3—Sr1^ix	111.61 (4)	109.52 (5)	113.71 (5)
Pt4—Pt3—Sr1ⁱⁱ	62.75 (4)	60.90 (4)	64.74 (4)
Pt4—Pt3—Sr1^xvi	111.65 (4)	109.52 (5)	113.71 (5)
Pt4—Pt3—Sr1^v	62.78 (4)	60.90 (4)	64.74 (4)
Pt4—Pt3—As1^vi	174.97 (5)	174.42 (5)	175.55 (4)
Pt4^xii—Pt3—Pt5	57.6 (4)	56.0 (4)	60.0 (4)
Pt4^xii—Pt3—Pt5^xiii	56.7 (4)	54.5 (4)	58.0 (4)
Pt4^xii—Pt3—Pt5^xiv	56.7 (4)	54.5 (4)	58.0 (4)
Pt4^xii—Pt3—Pt5^xv	57.6 (4)	56.0 (4)	60.0 (4)
Pt4^xii—Pt3—Sr1^ix	64.13 (4)	62.26 (4)	66.10 (4)
Pt4^xii—Pt3—Sr1ⁱⁱ	110.64 (4)	109.02 (5)	112.22 (5)
Pt4^xii—Pt3—Sr1^xvi	64.11 (4)	62.26 (4)	66.10 (4)
Pt4^xii—Pt3—Sr1^v	110.61 (4)	109.02 (5)	112.22 (5)
Pt4^xii—Pt3—As1^vi	116.40 (4)	116.35 (4)	116.46 (4)
Pt5—Pt3—Pt5^xiii	3.0 (9)	2.9 (8)	3.2 (9)
Pt5—Pt3—Pt5^xiv	102.1 (4)	101.8 (4)	102.6 (3)
Pt5—Pt3—Pt5^xv	102.2 (3)	102.2 (3)	102.2 (3)
Pt5—Pt3—Sr1^ix	116.5 (7)	114.5 (5)	118.7 (6)
Pt5—Pt3—Sr1ⁱⁱ	111.9 (7)	110.2 (6)	114.3 (6)
Pt5—Pt3—Sr1^xvi	63.5 (7)	60.7 (6)	66.1 (7)
Pt5—Pt3—Sr1^v	59.1 (7)	57.3 (6)	62.1 (7)
Pt5—Pt3—As1^vi	122.5 (5)	119.7 (4)	125.2 (5)
Pt5^xiii—Pt3—Pt5^xiv	102.4 (3)	102.4 (3)	102.4 (3)
Pt5^xiii—Pt3—Pt5^xv	102.1 (4)	101.8 (4)	102.6 (3)
Pt5^xiii—Pt3—Sr1^ix	113.5 (7)	111.8 (6)	116.0 (6)
Pt5^xiii—Pt3—Sr1ⁱⁱ	114.9 (7)	113.0 (6)	117.0 (6)
Pt5^xiii—Pt3—Sr1^xvi	60.0 (7)	58.0 (6)	63.0 (7)
Pt5^xiii—Pt3—Sr1^v	62.6 (7)	59.9 (6)	65.2 (7)
Pt5^xiii—Pt3—As1^vi	120.0 (6)	117.9 (4)	122.9 (5)
Pt5^xiv—Pt3—Pt5^xv	3.0 (9)	2.9 (8)	3.2 (9)
Pt5^xiv—Pt3—Sr1^ix	60.0 (7)	58.0 (6)	63.0 (7)
Pt5^xiv—Pt3—Sr1ⁱⁱ	62.7 (7)	59.9 (6)	65.2 (7)
Pt5^xiv—Pt3—Sr1^xvi	113.5 (7)	111.8 (6)	116.0 (6)
Pt5^xiv—Pt3—Sr1^v	114.9 (7)	113.0 (6)	117.0 (6)
Pt5^xiv—Pt3—As1^vi	120.0 (6)	117.9 (4)	122.9 (5)
Pt5^xv—Pt3—Sr1^ix	63.5 (7)	60.7 (6)	66.1 (7)
Pt5^xv—Pt3—Sr1ⁱⁱ	59.1 (7)	57.3 (6)	62.1 (7)
Pt5^xv—Pt3—Sr1^xvi	116.5 (7)	114.5 (5)	118.7 (6)
Pt5^xv—Pt3—Sr1^v	111.9 (7)	110.2 (6)	114.3 (6)
Pt5^xv—Pt3—As1^vi	122.5 (5)	119.7 (4)	125.2 (5)
Sr1^ix—Pt3—Sr1ⁱⁱ	109.92 (4)	103.79 (5)	115.95 (5)
Sr1^ix—Pt3—Sr1^xvi	70.36 (3)	70.297 (10)	70.42 (5)
Sr1^ix—Pt3—Sr1^v	172.85 (5)	171.17 (5)	175.04 (5)
Sr1^ix—Pt3—As1^vi	64.88 (4)	64.36 (4)	65.37 (4)
Sr1ⁱⁱ—Pt3—Sr1^xvi	172.87 (5)	171.17 (5)	175.04 (5)
Sr1ⁱⁱ—Pt3—Sr1^v	69.19 (3)	69.133 (9)	69.26 (5)
Sr1ⁱⁱ—Pt3—As1^vi	120.58 (5)	117.68 (5)	123.28 (4)
Sr1^xvi—Pt3—Sr1^v	109.92 (4)	103.79 (5)	115.95 (5)
Sr1^xvi—Pt3—As1^vi	64.87 (4)	64.36 (4)	65.37 (4)
Sr1^v—Pt3—As1^vi	120.59 (5)	117.68 (5)	123.28 (4)
Pt3—Pt4—Pt3^xvii	176.31 (5)	174.71 (4)	178.43 (3)
Pt3—Pt4—Pt4^xii	60.598 (18)	60.520 (18)	60.679 (18)
Pt3—Pt4—Pt4^xvii	121.26 (2)	121.08 (2)	121.43 (2)
Pt3—Pt4—Pt5	55.6 (3)	52.6 (3)	58.3 (3)
Pt3—Pt4—Pt5^xvii	125.8 (3)	119.3 (3)	133.0 (3)
Pt3—Pt4—Pt5^xiii	55.4 (3)	51.9 (3)	57.7 (3)
Pt3—Pt4—Pt5^xviii	124.2 (3)	118.3 (3)	132.7 (3)
Pt3—Pt4—Pt5^xix	124.0 (3)	118.3 (3)	132.7 (3)
Pt3—Pt4—Pt5^xiv	55.4 (3)	51.9 (3)	57.7 (3)
Pt3—Pt4—Pt5^xx	125.7 (3)	119.3 (3)	133.0 (3)
Pt3—Pt4—Pt5^xv	55.6 (3)	52.6 (3)	58.3 (3)
Pt3—Pt4—Sr1ⁱⁱ	67.72 (3)	66.01 (3)	69.48 (3)
Pt3—Pt4—Sr1ⁱ	112.66 (4)	111.00 (3)	114.37 (3)
Pt3—Pt4—Sr1^xxi	112.67 (4)	111.00 (3)	114.37 (3)
Pt3—Pt4—Sr1^v	67.72 (3)	66.01 (3)	69.48 (3)
Pt3^xvii—Pt4—Pt4^xii	117.68 (2)	117.53 (2)	117.84 (2)
Pt3^xvii—Pt4—Pt4^xvii	60.157 (17)	60.088 (17)	60.225 (17)
Pt3^xvii—Pt4—Pt5	122.4 (3)	117.3 (3)	130.8 (3)
Pt3^xvii—Pt4—Pt5^xvii	55.0 (3)	51.8 (3)	57.2 (3)
Pt3^xvii—Pt4—Pt5^xiii	124.6 (3)	118.3 (3)	130.9 (3)
Pt3^xvii—Pt4—Pt5^xviii	55.3 (3)	52.4 (3)	57.7 (3)
Pt3^xvii—Pt4—Pt5^xix	55.3 (3)	52.4 (3)	57.7 (3)
Pt3^xvii—Pt4—Pt5^xiv	124.7 (3)	118.3 (3)	130.9 (3)
Pt3^xvii—Pt4—Pt5^xx	55.1 (3)	51.8 (3)	57.2 (3)
Pt3^xvii—Pt4—Pt5^xv	122.4 (3)	117.3 (3)	130.8 (3)
Pt3^xvii—Pt4—Sr1ⁱⁱ	113.36 (4)	111.25 (4)	115.53 (4)
Pt3^xvii—Pt4—Sr1ⁱ	65.96 (3)	64.13 (3)	67.85 (3)
Pt3^xvii—Pt4—Sr1^xxi	65.99 (3)	64.13 (3)	67.85 (3)
Pt3^xvii—Pt4—Sr1^v	113.32 (4)	111.25 (4)	115.53 (4)
Pt4^xii—Pt4—Pt4^xvii	175.51 (6)	173.60 (6)	177.98 (2)
Pt4^xii—Pt4—Pt5	57.9 (5)	55.7 (5)	61.4 (5)
Pt4^xii—Pt4—Pt5^xvii	123.2 (5)	117.8 (5)	129.3 (5)
Pt4^xii—Pt4—Pt5^xiii	56.8 (5)	53.7 (5)	58.8 (5)
Pt4^xii—Pt4—Pt5^xviii	120.6 (5)	115.3 (5)	126.8 (5)
Pt4^xii—Pt4—Pt5^xix	120.5 (5)	115.3 (5)	126.8 (5)
Pt4^xii—Pt4—Pt5^xiv	56.8 (5)	53.7 (5)	58.8 (5)
Pt4^xii—Pt4—Pt5^xx	123.1 (5)	117.8 (5)	129.3 (5)
Pt4^xii—Pt4—Pt5^xv	58.0 (5)	55.7 (5)	61.4 (5)
Pt4^xii—Pt4—Sr1ⁱⁱ	115.73 (3)	111.45 (3)	119.82 (3)
Pt4^xii—Pt4—Sr1ⁱ	64.42 (3)	63.48 (2)	65.54 (2)
Pt4^xii—Pt4—Sr1^xxi	64.43 (3)	63.48 (2)	65.54 (2)
Pt4^xii—Pt4—Sr1^v	115.67 (3)	111.45 (3)	119.82 (3)
Pt4^xvii—Pt4—Pt5	121.2 (5)	116.0 (5)	128.4 (5)
Pt4^xvii—Pt4—Pt5^xvii	56.2 (5)	53.6 (5)	58.1 (5)
Pt4^xvii—Pt4—Pt5^xiii	124.7 (5)	118.4 (5)	131.0 (5)
Pt4^xvii—Pt4—Pt5^xviii	57.1 (5)	55.1 (5)	60.7 (5)
Pt4^xvii—Pt4—Pt5^xix	57.2 (5)	55.1 (5)	60.7 (5)
Pt4^xvii—Pt4—Pt5^xiv	124.7 (5)	118.4 (5)	131.0 (5)
Pt4^xvii—Pt4—Pt5^xx	56.3 (5)	53.6 (5)	58.1 (5)
Pt4^xvii—Pt4—Pt5^xv	121.2 (5)	116.0 (5)	128.4 (5)
Pt4^xvii—Pt4—Sr1ⁱⁱ	65.69 (3)	65.31 (3)	66.33 (2)
Pt4^xvii—Pt4—Sr1ⁱ	113.87 (3)	109.31 (3)	118.32 (3)
Pt4^xvii—Pt4—Sr1^xxi	113.92 (3)	109.31 (3)	118.32 (3)
Pt4^xvii—Pt4—Sr1^v	65.70 (3)	65.31 (3)	66.33 (2)
Pt5—Pt4—Pt5^xvii	172.0 (6)	168.9 (6)	178.4 (9)
Pt5—Pt4—Pt5^xiii	2.5 (8)	2.4 (8)	2.7 (9)
Pt5—Pt4—Pt5^xviii	174.7 (6)	170.2 (5)	179.4 (7)
Pt5—Pt4—Pt5^xix	73.6 (7)	70.4 (7)	80.0 (7)
Pt5—Pt4—Pt5^xiv	99.7 (7)	99.2 (6)	100.1 (7)
Pt5—Pt4—Pt5^xx	78.8 (7)	72.6 (7)	89.2 (6)
Pt5—Pt4—Pt5^xv	101.5 (6)	101.3 (6)	101.6 (7)
Pt5—Pt4—Sr1ⁱⁱ	116.1 (4)	113.7 (3)	118.8 (3)
Pt5—Pt4—Sr1ⁱ	63.3 (4)	59.1 (3)	69.5 (3)
Pt5—Pt4—Sr1^xxi	117.1 (6)	114.9 (6)	120.3 (6)
Pt5—Pt4—Sr1^v	60.9 (6)	57.9 (6)	65.9 (6)
Pt5^xvii—Pt4—Pt5^xiii	173.9 (6)	170.8 (5)	179.0 (7)
Pt5^xvii—Pt4—Pt5^xviii	2.5 (8)	2.5 (7)	2.7 (9)
Pt5^xvii—Pt4—Pt5^xix	98.8 (6)	98.3 (6)	99.2 (7)
Pt5^xvii—Pt4—Pt5^xiv	85.6 (6)	74.7 (6)	91.4 (6)
Pt5^xvii—Pt4—Pt5^xx	96.6 (6)	96.5 (6)	96.8 (6)
Pt5^xvii—Pt4—Pt5^xv	78.9 (7)	72.6 (6)	89.2 (6)
Pt5^xvii—Pt4—Sr1ⁱⁱ	63.5 (4)	58.9 (3)	69.5 (3)
Pt5^xvii—Pt4—Sr1ⁱ	115.8 (3)	112.3 (3)	118.1 (4)
Pt5^xvii—Pt4—Sr1^xxi	63.7 (6)	59.2 (5)	67.8 (5)
Pt5^xvii—Pt4—Sr1^v	116.6 (6)	113.8 (5)	118.5 (6)
Pt5^xiii—Pt4—Pt5^xviii	172.2 (7)	169.9 (6)	176.4 (9)
Pt5^xiii—Pt4—Pt5^xix	79.5 (7)	72.5 (6)	89.5 (6)
Pt5^xiii—Pt4—Pt5^xiv	97.5 (6)	97.4 (6)	97.8 (6)
Pt5^xiii—Pt4—Pt5^xx	85.6 (6)	74.7 (6)	91.4 (6)
Pt5^xiii—Pt4—Pt5^xv	99.7 (7)	99.2 (6)	100.1 (7)
Pt5^xiii—Pt4—Sr1ⁱⁱ	117.5 (3)	114.0 (3)	120.0 (4)
Pt5^xiii—Pt4—Sr1ⁱ	63.3 (4)	58.8 (3)	68.6 (3)
Pt5^xiii—Pt4—Sr1^xxi	116.0 (6)	113.2 (5)	117.9 (6)
Pt5^xiii—Pt4—Sr1^v	64.7 (6)	59.8 (5)	68.6 (6)
Pt5^xviii—Pt4—Pt5^xix	100.5 (6)	100.3 (6)	100.7 (7)
Pt5^xviii—Pt4—Pt5^xiv	79.6 (7)	72.5 (6)	89.5 (6)
Pt5^xviii—Pt4—Pt5^xx	98.8 (7)	98.3 (6)	99.2 (8)
Pt5^xviii—Pt4—Pt5^xv	73.6 (7)	70.4 (7)	80.0 (7)
Pt5^xviii—Pt4—Sr1ⁱⁱ	64.0 (4)	59.3 (3)	70.3 (3)
Pt5^xviii—Pt4—Sr1ⁱ	114.4 (4)	112.1 (3)	116.9 (3)
Pt5^xviii—Pt4—Sr1^xxi	60.4 (6)	57.2 (5)	65.3 (6)
Pt5^xviii—Pt4—Sr1^v	117.8 (6)	115.6 (6)	120.9 (6)
Pt5^xix—Pt4—Pt5^xiv	172.2 (7)	169.9 (6)	176.4 (8)
Pt5^xix—Pt4—Pt5^xx	2.5 (8)	2.5 (8)	2.7 (9)
Pt5^xix—Pt4—Pt5^xv	174.7 (6)	170.2 (5)	179.4 (8)
Pt5^xix—Pt4—Sr1ⁱⁱ	117.7 (6)	115.6 (6)	120.9 (6)
Pt5^xix—Pt4—Sr1ⁱ	60.3 (6)	57.2 (5)	65.3 (6)
Pt5^xix—Pt4—Sr1^xxi	114.5 (4)	112.1 (3)	116.9 (3)
Pt5^xix—Pt4—Sr1^v	63.8 (4)	59.3 (3)	70.3 (3)
Pt5^xiv—Pt4—Pt5^xx	173.9 (6)	170.8 (5)	179.0 (7)
Pt5^xiv—Pt4—Pt5^xv	2.5 (8)	2.4 (7)	2.7 (9)
Pt5^xiv—Pt4—Sr1ⁱⁱ	64.7 (6)	59.8 (5)	68.6 (6)
Pt5^xiv—Pt4—Sr1ⁱ	116.0 (6)	113.2 (5)	117.9 (6)
Pt5^xiv—Pt4—Sr1^xxi	63.3 (4)	58.8 (3)	68.6 (3)
Pt5^xiv—Pt4—Sr1^v	117.5 (3)	114.0 (3)	120.0 (4)
Pt5^xx—Pt4—Pt5^xv	172.0 (6)	168.9 (5)	178.4 (8)
Pt5^xx—Pt4—Sr1ⁱⁱ	116.5 (6)	113.8 (5)	118.5 (6)
Pt5^xx—Pt4—Sr1ⁱ	63.7 (6)	59.2 (5)	67.8 (5)
Pt5^xx—Pt4—Sr1^xxi	115.9 (3)	112.3 (3)	118.1 (4)
Pt5^xx—Pt4—Sr1^v	63.4 (4)	58.9 (3)	69.5 (3)
Pt5^xv—Pt4—Sr1ⁱⁱ	60.9 (6)	57.9 (6)	65.9 (6)
Pt5^xv—Pt4—Sr1ⁱ	117.1 (6)	114.9 (6)	120.3 (6)
Pt5^xv—Pt4—Sr1^xxi	63.3 (4)	59.1 (3)	69.5 (3)
Pt5^xv—Pt4—Sr1^v	116.1 (4)	113.7 (3)	118.8 (3)
Sr1ⁱⁱ—Pt4—Sr1ⁱ	174.98 (5)	171.91 (3)	179.61 (6)
Sr1ⁱⁱ—Pt4—Sr1^xxi	108.06 (5)	100.71 (4)	115.61 (4)
Sr1ⁱⁱ—Pt4—Sr1^v	72.44 (4)	72.27 (3)	72.60 (5)
Sr1ⁱ—Pt4—Sr1^xxi	71.59 (4)	71.45 (3)	71.73 (5)
Sr1ⁱ—Pt4—Sr1^v	107.96 (5)	100.71 (4)	115.61 (4)
Sr1^xxi—Pt4—Sr1^v	174.97 (5)	171.91 (4)	179.61 (6)
Pt3—Pt5—Pt3^xiii	102.1 (5)	101.5 (7)	102.9 (6)
Pt3—Pt5—Pt4	67.8 (3)	64.7 (2)	72.7 (3)
Pt3—Pt5—Pt4^xii	67.4 (3)	63.7 (2)	71.5 (3)
Pt3—Pt5—Pt4^xiii	139.6 (13)	137.3 (18)	143.4 (14)
Pt3—Pt5—Pt4^xxvi	148.4 (13)	145.8 (15)	150.1 (17)
Pt3—Pt5—Pt5^xiii	89 (5)	79 (6)	98 (6)
Pt3—Pt5—Pt5^xxii	107.1 (9)	106.6 (12)	107.8 (8)
Pt3—Pt5—Pt5^xix	112.2 (9)	111.4 (8)	113.5 (10)
Pt3—Pt5—Pt5^xxiii	107.1 (9)	106.7 (8)	107.8 (10)
Pt3—Pt5—Pt5^xx	112.1 (9)	111.2 (7)	112.6 (8)
Pt3—Pt5—Sr1ⁱ	128.9 (3)	128.5 (3)	129.1 (4)
Pt3—Pt5—Sr1^xvi	71.3 (6)	69.9 (6)	73.9 (6)
Pt3—Pt5—Sr1^v	75.6 (6)	73.5 (5)	77.5 (6)
Pt3^xiii—Pt5—Pt4	146.5 (13)	143.6 (15)	148.3 (17)
Pt3^xiii—Pt5—Pt4^xii	141.6 (13)	139.5 (18)	145.2 (14)
Pt3^xiii—Pt5—Pt4^xiii	67.5 (3)	63.7 (2)	71.3 (3)
Pt3^xiii—Pt5—Pt4^xxvi	68.0 (3)	64.6 (2)	72.9 (3)
Pt3^xiii—Pt5—Pt5^xiii	88 (5)	79 (6)	98 (6)
Pt3^xiii—Pt5—Pt5^xxii	108.3 (9)	107.8 (12)	109.0 (8)
Pt3^xiii—Pt5—Pt5^xix	110.9 (9)	110.1 (8)	112.2 (10)
Pt3^xiii—Pt5—Pt5^xxiii	108.3 (9)	107.9 (8)	109.0 (10)
Pt3^xiii—Pt5—Pt5^xx	110.9 (9)	110.0 (7)	111.3 (9)
Pt3^xiii—Pt5—Sr1ⁱ	128.9 (3)	128.4 (3)	129.2 (3)
Pt3^xiii—Pt5—Sr1^xvi	72.5 (6)	71.0 (6)	75.2 (6)
Pt3^xiii—Pt5—Sr1^v	74.3 (6)	72.2 (5)	76.1 (6)
Pt4—Pt5—Pt4^xii	65.85 (16)	63.17 (11)	69.08 (17)
Pt4—Pt5—Pt4^xiii	140.6 (7)	133.9 (6)	145.9 (5)
Pt4—Pt5—Pt4^xxvi	103.4 (10)	92.2 (9)	109.6 (11)
Pt4—Pt5—Pt5^xiii	122 (3)	118 (5)	126 (4)
Pt4—Pt5—Pt5^xxii	105.1 (6)	103.7 (6)	108.0 (6)
Pt4—Pt5—Pt5^xix	53.5 (6)	50.0 (6)	55.1 (6)
Pt4—Pt5—Pt5^xxiii	105.2 (6)	102.8 (6)	107.3 (6)
Pt4—Pt5—Pt5^xx	51.9 (6)	46.4 (4)	55.1 (6)
Pt4—Pt5—Sr1ⁱ	70.8 (4)	67.3 (3)	73.4 (3)
Pt4—Pt5—Sr1^xvi	127.6 (6)	124.9 (6)	132.4 (6)
Pt4—Pt5—Sr1^v	72.3 (8)	70.0 (7)	73.6 (8)
Pt4^xii—Pt5—Pt4^xiii	96.2 (10)	88.6 (9)	105.2 (9)
Pt4^xii—Pt5—Pt4^xxvi	138.6 (6)	131.4 (5)	144.2 (5)
Pt4^xii—Pt5—Pt5^xiii	58 (3)	53 (3)	62 (5)
Pt4^xii—Pt5—Pt5^xxii	47.0 (5)	44.1 (4)	52.4 (5)
Pt4^xii—Pt5—Pt5^xix	107.3 (5)	104.6 (6)	108.5 (6)
Pt4^xii—Pt5—Pt5^xxiii	49.3 (5)	44.3 (5)	52.4 (4)
Pt4^xii—Pt5—Pt5^xx	107.7 (6)	104.4 (5)	109.2 (6)
Pt4^xii—Pt5—Sr1ⁱ	69.3 (4)	65.3 (3)	71.9 (3)
Pt4^xii—Pt5—Sr1^xvi	69.2 (7)	67.5 (7)	71.4 (7)
Pt4^xii—Pt5—Sr1^v	131.8 (5)	127.6 (5)	135.3 (5)
Pt4^xiii—Pt5—Pt4^xxvi	66.07 (16)	63.10 (11)	69.10 (17)
Pt4^xiii—Pt5—Pt5^xiii	55 (3)	52 (3)	59 (5)
Pt4^xiii—Pt5—Pt5^xxii	47.4 (5)	44.5 (5)	52.8 (5)
Pt4^xiii—Pt5—Pt5^xix	108.1 (6)	105.1 (6)	109.4 (6)
Pt4^xiii—Pt5—Pt5^xxiii	49.4 (5)	44.7 (5)	52.9 (5)
Pt4^xiii—Pt5—Pt5^xx	108.5 (6)	105.0 (5)	110.2 (7)
Pt4^xiii—Pt5—Sr1ⁱ	70.2 (4)	66.6 (3)	72.6 (3)
Pt4^xiii—Pt5—Sr1^xvi	68.4 (7)	66.7 (8)	70.9 (8)
Pt4^xiii—Pt5—Sr1^v	131.6 (5)	127.1 (5)	135.1 (6)
Pt4^xxvi—Pt5—Pt5^xiii	120 (3)	115 (5)	124 (4)
Pt4^xxvi—Pt5—Pt5^xxii	104.4 (6)	103.1 (6)	106.9 (6)
Pt4^xxvi—Pt5—Pt5^xix	52.9 (6)	50.2 (6)	54.5 (5)
Pt4^xxvi—Pt5—Pt5^xxiii	104.5 (6)	102.3 (6)	106.4 (6)
Pt4^xxvi—Pt5—Pt5^xx	51.1 (5)	45.9 (4)	54.6 (5)
Pt4^xxvi—Pt5—Sr1ⁱ	69.6 (4)	66.0 (3)	72.5 (3)
Pt4^xxvi—Pt5—Sr1^xvi	128.0 (6)	125.3 (5)	132.7 (6)
Pt4^xxvi—Pt5—Sr1^v	72.9 (8)	70.6 (7)	74.2 (8)
Pt5^xiii—Pt5—Pt5^xxii	27 (9)	17 (11)	39 (8)
Pt5^xiii—Pt5—Pt5^xix	147 (9)	132 (11)	162 (11)
Pt5^xiii—Pt5—Pt5^xxiii	31 (9)	18 (11)	46 (11)
Pt5^xiii—Pt5—Pt5^xx	152 (9)	140 (9)	163 (11)
Pt5^xiii—Pt5—Sr1ⁱ	89 (9)	74 (11)	104 (11)
Pt5^xiii—Pt5—Sr1^xvi	27 (9)	14 (11)	40 (11)
Pt5^xiii—Pt5—Sr1^v	152 (9)	138 (11)	165 (11)
Pt5^xxii—Pt5—Pt5^xix	115.6 (7)	113.5 (6)	117.3 (7)
Pt5^xxii—Pt5—Pt5^xxiii	1.0 (5)	0.7 (5)	1.4 (4)
Pt5^xxii—Pt5—Pt5^xx	114.9 (7)	113.9 (7)	116.6 (7)
Pt5^xxii—Pt5—Sr1ⁱ	57.4 (5)	56.1 (6)	58.5 (6)
Pt5^xxii—Pt5—Sr1^xvi	57.3 (7)	55.6 (7)	58.9 (8)
Pt5^xxii—Pt5—Sr1^v	174.6 (8)	172.0 (7)	179.7 (7)
Pt5^xix—Pt5—Pt5^xxiii	115.4 (7)	112.2 (7)	116.9 (7)
Pt5^xix—Pt5—Pt5^xx	1.3 (5)	0.8 (6)	1.8 (5)
Pt5^xix—Pt5—Sr1ⁱ	57.9 (6)	55.8 (6)	59.2 (6)
Pt5^xix—Pt5—Sr1^xvi	174.9 (9)	171.2 (9)	176.8 (8)
Pt5^xix—Pt5—Sr1^v	61.1 (8)	59.4 (8)	62.7 (8)
Pt5^xxiii—Pt5—Pt5^xx	116.1 (7)	113.7 (6)	117.6 (7)
Pt5^xxiii—Pt5—Sr1ⁱ	57.4 (6)	55.9 (5)	58.3 (6)
Pt5^xxiii—Pt5—Sr1^xvi	59.5 (8)	58.0 (7)	60.2 (8)
Pt5^xxiii—Pt5—Sr1^v	176.4 (9)	171.3 (8)	179.0 (8)
Pt5^xx—Pt5—Sr1ⁱ	58.1 (6)	57.4 (6)	59.6 (5)
Pt5^xx—Pt5—Sr1^xvi	174.0 (9)	169.4 (7)	177.7 (8)
Pt5^xx—Pt5—Sr1^v	58.6 (8)	57.6 (7)	61.0 (7)
Sr1ⁱ—Pt5—Sr1^xvi	115.9 (9)	111.6 (7)	118.5 (10)
Sr1ⁱ—Pt5—Sr1^v	118.0 (9)	115.0 (8)	121.8 (9)
Sr1^xvi—Pt5—Sr1^v	126.0 (5)	121.4 (4)	132.0 (4)
Pt1^xxiv—Sr1—Pt1^xxv	89.83 (5)	89.17 (6)	90.65 (6)
Pt1^xxiv—Sr1—Pt2^xxiv	48.29 (3)	45.87 (3)	50.83 (3)
Pt1^xxiv—Sr1—Pt2^xxvii	78.62 (4)	75.84 (4)	81.32 (5)
Pt1^xxiv—Sr1—Pt3^xxiv	50.03 (3)	48.96 (4)	51.11 (4)
Pt1^xxiv—Sr1—Pt3^xxvii	80.47 (4)	79.73 (4)	81.26 (3)
Pt1^xxiv—Sr1—Pt3^xxviii	95.29 (4)	90.71 (5)	99.98 (5)
Pt1^xxiv—Sr1—Pt3^xxv	124.80 (5)	121.04 (5)	128.37 (5)
Pt1^xxiv—Sr1—Pt4^xxiv	88.91 (5)	86.77 (2)	91.24 (2)
Pt1^xxiv—Sr1—Pt4ⁱ	103.80 (6)	101.22 (4)	106.56 (3)
Pt1^xxiv—Sr1—Pt4^xxv	171.68 (5)	165.74 (8)	177.97 (7)
Pt1^xxiv—Sr1—Pt4^viii	137.90 (4)	131.82 (6)	144.14 (6)
Pt1^xxiv—Sr1—Pt5ⁱ	135.0 (2)	133.7 (3)	136.90 (18)
Pt1^xxiv—Sr1—Pt5^viii	135.1 (2)	133.1 (3)	136.2 (2)
Pt1^xxiv—Sr1—Pt5^xxix	93.5 (2)	87.9 (2)	97.4 (3)
Pt1^xxiv—Sr1—Pt5^xxx	126.0 (2)	121.5 (2)	130.0 (2)
Pt1^xxiv—Sr1—Pt5^xxxi	93.6 (2)	88.7 (2)	98.3 (3)
Pt1^xxiv—Sr1—Pt5^xxxii	126.01 (19)	120.8 (2)	129.4 (2)
Pt1^xxiv—Sr1—As1^xxiv	42.70 (4)	42.26 (4)	43.11 (4)
Pt1^xxiv—Sr1—As1^xxv	77.76 (4)	75.95 (3)	79.57 (4)
Pt1^xxv—Sr1—Pt2^xxiv	78.57 (4)	75.84 (4)	81.32 (5)
Pt1^xxv—Sr1—Pt2^xxvii	48.34 (3)	45.87 (3)	50.83 (3)
Pt1^xxv—Sr1—Pt3^xxiv	124.73 (5)	121.04 (5)	128.37 (5)
Pt1^xxv—Sr1—Pt3^xxvii	95.38 (4)	90.71 (5)	99.98 (5)
Pt1^xxv—Sr1—Pt3^xxviii	80.47 (4)	79.73 (4)	81.26 (3)
Pt1^xxv—Sr1—Pt3^xxv	50.05 (3)	48.96 (4)	51.11 (4)
Pt1^xxv—Sr1—Pt4^xxiv	171.56 (5)	165.74 (8)	177.97 (7)
Pt1^xxv—Sr1—Pt4ⁱ	138.02 (4)	131.82 (6)	144.14 (6)
Pt1^xxv—Sr1—Pt4^xxv	88.92 (5)	86.77 (2)	91.24 (2)
Pt1^xxv—Sr1—Pt4^viii	103.83 (6)	101.22 (4)	106.56 (3)
Pt1^xxv—Sr1—Pt5ⁱ	135.1 (2)	133.1 (3)	136.2 (2)
Pt1^xxv—Sr1—Pt5^viii	135.0 (2)	133.7 (3)	136.90 (18)
Pt1^xxv—Sr1—Pt5^xxix	125.90 (19)	120.8 (2)	129.4 (2)
Pt1^xxv—Sr1—Pt5^xxx	93.7 (2)	88.7 (2)	98.3 (3)
Pt1^xxv—Sr1—Pt5^xxxi	125.9 (2)	121.5 (2)	130.0 (2)
Pt1^xxv—Sr1—Pt5^xxxii	93.6 (2)	87.9 (2)	97.4 (3)
Pt1^xxv—Sr1—As1^xxiv	77.79 (4)	75.95 (3)	79.57 (4)
Pt1^xxv—Sr1—As1^xxv	42.69 (4)	42.26 (4)	43.11 (4)
Pt2^xxiv—Sr1—Pt2^xxvii	104.87 (5)	104.39 (6)	105.33 (6)
Pt2^xxiv—Sr1—Pt3^xxiv	47.03 (2)	45.39 (3)	48.78 (3)
Pt2^xxiv—Sr1—Pt3^xxvii	127.97 (6)	125.95 (7)	129.95 (7)
Pt2^xxiv—Sr1—Pt3^xxviii	47.36 (2)	45.65 (3)	49.18 (3)
Pt2^xxiv—Sr1—Pt3^xxv	128.34 (6)	126.36 (7)	130.28 (7)
Pt2^xxiv—Sr1—Pt4^xxiv	94.75 (3)	92.63 (5)	96.93 (5)
Pt2^xxiv—Sr1—Pt4ⁱ	139.06 (5)	135.02 (7)	143.26 (7)
Pt2^xxiv—Sr1—Pt4^xxv	138.95 (6)	135.04 (6)	143.01 (6)
Pt2^xxiv—Sr1—Pt4^viii	95.21 (3)	93.14 (5)	97.32 (5)
Pt2^xxiv—Sr1—Pt5ⁱ	128.2 (5)	127.0 (5)	130.1 (5)
Pt2^xxiv—Sr1—Pt5^viii	126.9 (5)	124.7 (5)	128.1 (5)
Pt2^xxiv—Sr1—Pt5^xxix	64.1 (3)	61.2 (3)	66.1 (3)
Pt2^xxiv—Sr1—Pt5^xxx	169.9 (3)	167.0 (3)	172.2 (3)
Pt2^xxiv—Sr1—Pt5^xxxi	64.9 (3)	62.3 (3)	67.2 (3)
Pt2^xxiv—Sr1—Pt5^xxxii	168.9 (3)	166.0 (3)	171.0 (3)
Pt2^xxiv—Sr1—As1^xxiv	86.22 (5)	83.76 (5)	88.69 (5)
Pt2^xxiv—Sr1—As1^xxv	41.47 (3)	39.45 (3)	43.61 (4)
Pt2^xxvii—Sr1—Pt3^xxiv	128.38 (6)	126.36 (7)	130.28 (7)
Pt2^xxvii—Sr1—Pt3^xxvii	47.39 (2)	45.65 (3)	49.18 (3)
Pt2^xxvii—Sr1—Pt3^xxviii	128.01 (6)	125.95 (7)	129.95 (7)
Pt2^xxvii—Sr1—Pt3^xxv	47.06 (2)	45.39 (3)	48.78 (3)
Pt2^xxvii—Sr1—Pt4^xxiv	139.01 (6)	135.04 (6)	143.01 (6)
Pt2^xxvii—Sr1—Pt4ⁱ	95.25 (3)	93.14 (5)	97.32 (5)
Pt2^xxvii—Sr1—Pt4^xxv	94.79 (3)	92.63 (5)	96.93 (5)
Pt2^xxvii—Sr1—Pt4^viii	139.13 (5)	135.02 (7)	143.26 (7)
Pt2^xxvii—Sr1—Pt5ⁱ	126.9 (5)	124.7 (5)	128.1 (5)
Pt2^xxvii—Sr1—Pt5^viii	128.2 (5)	127.0 (5)	130.1 (5)
Pt2^xxvii—Sr1—Pt5^xxix	168.9 (3)	166.0 (3)	171.0 (3)
Pt2^xxvii—Sr1—Pt5^xxx	64.9 (3)	62.3 (3)	67.2 (3)
Pt2^xxvii—Sr1—Pt5^xxxi	169.9 (3)	167.0 (3)	172.2 (3)
Pt2^xxvii—Sr1—Pt5^xxxii	64.2 (3)	61.2 (3)	66.1 (3)
Pt2^xxvii—Sr1—As1^xxiv	41.51 (3)	39.45 (3)	43.61 (4)
Pt2^xxvii—Sr1—As1^xxv	86.27 (5)	83.76 (5)	88.69 (5)
Pt3^xxiv—Sr1—Pt3^xxvii	109.91 (5)	108.90 (2)	111.06 (2)
Pt3^xxiv—Sr1—Pt3^xxviii	69.71 (3)	63.70 (3)	75.96 (4)
Pt3^xxiv—Sr1—Pt3^xxv	172.92 (7)	171.67 (8)	175.16 (7)
Pt3^xxiv—Sr1—Pt4^xxiv	49.51 (3)	48.52 (2)	50.66 (2)
Pt3^xxiv—Sr1—Pt4ⁱ	92.70 (5)	90.45 (4)	95.13 (4)
Pt3^xxiv—Sr1—Pt4^xxv	135.63 (5)	132.50 (5)	138.91 (5)
Pt3^xxiv—Sr1—Pt4^viii	91.21 (4)	85.04 (4)	97.54 (4)
Pt3^xxiv—Sr1—Pt5ⁱ	93.4 (4)	92.1 (4)	95.4 (4)
Pt3^xxiv—Sr1—Pt5^viii	92.4 (4)	90.7 (4)	93.5 (4)
Pt3^xxiv—Sr1—Pt5^xxix	44.78 (18)	40.45 (17)	48.14 (19)
Pt3^xxiv—Sr1—Pt5^xxx	138.64 (18)	137.66 (16)	139.9 (2)
Pt3^xxiv—Sr1—Pt5^xxxi	45.18 (19)	41.01 (18)	48.8 (2)
Pt3^xxiv—Sr1—Pt5^xxxii	139.62 (17)	138.17 (15)	140.3 (2)
Pt3^xxiv—Sr1—As1^xxiv	88.65 (5)	88.00 (4)	89.44 (4)
Pt3^xxiv—Sr1—As1^xxv	87.44 (4)	83.05 (5)	91.97 (5)
Pt3^xxvii—Sr1—Pt3^xxviii	172.79 (7)	171.51 (8)	175.09 (7)
Pt3^xxvii—Sr1—Pt3^xxv	69.83 (3)	63.70 (3)	75.96 (4)
Pt3^xxvii—Sr1—Pt4^xxiv	92.30 (5)	90.06 (3)	94.70 (4)
Pt3^xxvii—Sr1—Pt4ⁱ	49.91 (3)	49.11 (2)	50.83 (2)
Pt3^xxvii—Sr1—Pt4^xxv	91.74 (4)	85.60 (4)	97.83 (4)
Pt3^xxvii—Sr1—Pt4^viii	135.36 (5)	132.40 (5)	138.34 (5)
Pt3^xxvii—Sr1—Pt5ⁱ	92.5 (4)	90.7 (4)	93.6 (4)
Pt3^xxvii—Sr1—Pt5^viii	93.4 (4)	92.2 (4)	95.5 (4)
Pt3^xxvii—Sr1—Pt5^xxix	139.20 (17)	137.70 (15)	139.9 (2)
Pt3^xxvii—Sr1—Pt5^xxx	45.75 (19)	41.45 (18)	49.3 (2)
Pt3^xxvii—Sr1—Pt5^xxxi	138.17 (18)	137.13 (16)	139.5 (2)
Pt3^xxvii—Sr1—Pt5^xxxii	45.33 (18)	40.83 (17)	48.60 (18)
Pt3^xxvii—Sr1—As1^xxiv	42.70 (3)	41.74 (4)	43.65 (4)
Pt3^xxvii—Sr1—As1^xxv	131.78 (6)	128.65 (6)	134.68 (5)
Pt3^xxviii—Sr1—Pt3^xxv	109.92 (5)	108.90 (2)	111.06 (2)
Pt3^xxviii—Sr1—Pt4^xxiv	91.63 (4)	85.60 (4)	97.83 (4)
Pt3^xxviii—Sr1—Pt4ⁱ	135.31 (5)	132.40 (5)	138.34 (5)
Pt3^xxviii—Sr1—Pt4^xxv	92.28 (5)	90.06 (3)	94.70 (4)
Pt3^xxviii—Sr1—Pt4^viii	49.90 (3)	49.11 (2)	50.83 (2)
Pt3^xxviii—Sr1—Pt5ⁱ	93.4 (4)	92.2 (4)	95.5 (4)
Pt3^xxviii—Sr1—Pt5^viii	92.4 (4)	90.7 (4)	93.6 (4)
Pt3^xxviii—Sr1—Pt5^xxix	45.23 (18)	40.83 (17)	48.60 (18)
Pt3^xxviii—Sr1—Pt5^xxx	138.20 (18)	137.13 (16)	139.5 (2)
Pt3^xxviii—Sr1—Pt5^xxxi	45.65 (19)	41.45 (18)	49.3 (2)
Pt3^xxviii—Sr1—Pt5^xxxii	139.23 (17)	137.70 (15)	139.9 (2)
Pt3^xxviii—Sr1—As1^xxiv	131.72 (6)	128.65 (6)	134.68 (5)
Pt3^xxviii—Sr1—As1^xxv	42.69 (3)	41.74 (4)	43.65 (4)
Pt3^xxv—Sr1—Pt4^xxiv	135.69 (5)	132.50 (5)	138.91 (5)
Pt3^xxv—Sr1—Pt4ⁱ	91.32 (4)	85.04 (4)	97.54 (4)
Pt3^xxv—Sr1—Pt4^xxv	49.52 (3)	48.52 (2)	50.66 (2)
Pt3^xxv—Sr1—Pt4^viii	92.73 (5)	90.45 (4)	95.13 (4)
Pt3^xxv—Sr1—Pt5ⁱ	92.4 (4)	90.7 (4)	93.5 (4)
Pt3^xxv—Sr1—Pt5^viii	93.4 (4)	92.1 (4)	95.4 (4)
Pt3^xxv—Sr1—Pt5^xxix	139.60 (17)	138.17 (15)	140.3 (2)
Pt3^xxv—Sr1—Pt5^xxx	45.28 (19)	41.01 (18)	48.8 (2)
Pt3^xxv—Sr1—Pt5^xxxi	138.62 (18)	137.66 (16)	139.9 (2)
Pt3^xxv—Sr1—Pt5^xxxii	44.89 (18)	40.45 (17)	48.14 (19)
Pt3^xxv—Sr1—As1^xxiv	87.53 (4)	83.05 (5)	91.97 (5)
Pt3^xxv—Sr1—As1^xxv	88.65 (5)	88.00 (4)	89.44 (4)
Pt4^xxiv—Sr1—Pt4ⁱ	49.88 (3)	48.45 (3)	51.17 (3)
Pt4^xxiv—Sr1—Pt4^xxv	93.14 (5)	88.83 (6)	97.58 (6)
Pt4^xxiv—Sr1—Pt4^viii	71.86 (4)	64.35 (4)	79.34 (4)
Pt4^xxiv—Sr1—Pt5ⁱ	47.2 (3)	44.9 (3)	49.7 (3)
Pt4^xxiv—Sr1—Pt5^viii	46.5 (3)	43.5 (3)	48.4 (3)
Pt4^xxiv—Sr1—Pt5^xxix	46.92 (18)	44.59 (18)	49.49 (17)
Pt4^xxiv—Sr1—Pt5^xxx	93.4 (3)	93.0 (2)	94.2 (3)
Pt4^xxiv—Sr1—Pt5^xxxi	46.79 (18)	44.09 (19)	48.67 (18)
Pt4^xxiv—Sr1—Pt5^xxxii	94.5 (3)	94.1 (2)	94.8 (3)
Pt4^xxiv—Sr1—As1^xxiv	106.44 (5)	103.48 (3)	109.56 (3)
Pt4^xxiv—Sr1—As1^xxv	129.27 (5)	123.68 (6)	135.06 (7)
Pt4ⁱ—Sr1—Pt4^xxv	71.96 (4)	64.35 (4)	79.34 (4)
Pt4ⁱ—Sr1—Pt4^viii	91.89 (5)	88.17 (6)	95.83 (6)
Pt4ⁱ—Sr1—Pt5ⁱ	46.0 (3)	43.0 (3)	47.7 (3)
Pt4ⁱ—Sr1—Pt5^viii	46.5 (3)	44.4 (3)	49.1 (3)
Pt4ⁱ—Sr1—Pt5^xxix	94.1 (3)	93.7 (2)	94.4 (3)
Pt4ⁱ—Sr1—Pt5^xxx	46.80 (19)	44.05 (19)	48.82 (19)
Pt4ⁱ—Sr1—Pt5^xxxi	93.0 (3)	92.6 (2)	93.7 (3)
Pt4ⁱ—Sr1—Pt5^xxxii	47.12 (19)	44.56 (19)	49.53 (18)
Pt4ⁱ—Sr1—As1^xxiv	85.88 (4)	84.18 (3)	87.68 (3)
Pt4ⁱ—Sr1—As1^xxv	175.14 (6)	173.28 (8)	179.68 (6)
Pt4^xxv—Sr1—Pt4^viii	49.89 (3)	48.45 (3)	51.17 (3)
Pt4^xxv—Sr1—Pt5ⁱ	46.5 (3)	43.5 (3)	48.4 (3)
Pt4^xxv—Sr1—Pt5^viii	47.2 (3)	44.9 (3)	49.7 (3)
Pt4^xxv—Sr1—Pt5^xxix	94.5 (3)	94.1 (2)	94.8 (3)
Pt4^xxv—Sr1—Pt5^xxx	46.84 (18)	44.09 (19)	48.67 (18)
Pt4^xxv—Sr1—Pt5^xxxi	93.4 (3)	93.0 (2)	94.2 (3)
Pt4^xxv—Sr1—Pt5^xxxii	46.97 (18)	44.59 (18)	49.49 (17)
Pt4^xxv—Sr1—As1^xxiv	129.38 (5)	123.68 (6)	135.06 (7)
Pt4^xxv—Sr1—As1^xxv	106.41 (5)	103.48 (3)	109.56 (3)
Pt4^viii—Sr1—Pt5ⁱ	46.5 (3)	44.4 (3)	49.1 (3)
Pt4^viii—Sr1—Pt5^viii	45.9 (3)	43.0 (3)	47.7 (3)
Pt4^viii—Sr1—Pt5^xxix	47.06 (19)	44.56 (19)	49.53 (18)
Pt4^viii—Sr1—Pt5^xxx	93.0 (3)	92.6 (2)	93.7 (3)
Pt4^viii—Sr1—Pt5^xxxi	46.74 (19)	44.05 (19)	48.82 (19)
Pt4^viii—Sr1—Pt5^xxxii	94.1 (3)	93.7 (2)	94.4 (3)
Pt4^viii—Sr1—As1^xxiv	175.14 (6)	173.28 (8)	179.68 (6)
Pt4^viii—Sr1—As1^xxv	85.86 (4)	84.18 (3)	87.68 (3)
Pt5ⁱ—Sr1—Pt5^viii	2.4 (7)	2.3 (7)	2.5 (7)
Pt5ⁱ—Sr1—Pt5^xxix	65.3 (7)	64.4 (8)	65.9 (8)
Pt5ⁱ—Sr1—Pt5^xxx	61.0 (7)	60.6 (7)	61.8 (8)
Pt5ⁱ—Sr1—Pt5^xxxi	64.0 (7)	63.0 (7)	65.0 (7)
Pt5ⁱ—Sr1—Pt5^xxxii	62.3 (7)	61.9 (9)	63.2 (6)
Pt5ⁱ—Sr1—As1^xxiv	131.9 (4)	129.4 (5)	133.4 (4)
Pt5ⁱ—Sr1—As1^xxv	131.9 (4)	130.4 (5)	134.6 (4)
Pt5^viii—Sr1—Pt5^xxix	62.4 (7)	61.9 (9)	63.2 (6)
Pt5^viii—Sr1—Pt5^xxx	63.9 (7)	63.0 (7)	65.0 (7)
Pt5^viii—Sr1—Pt5^xxxi	61.0 (7)	60.6 (7)	61.8 (8)
Pt5^viii—Sr1—Pt5^xxxii	65.3 (7)	64.4 (8)	65.9 (8)
Pt5^viii—Sr1—As1^xxiv	132.0 (4)	130.4 (5)	134.6 (4)
Pt5^viii—Sr1—As1^xxv	131.9 (4)	129.4 (5)	133.4 (4)
Pt5^xxix—Sr1—Pt5^xxx	126.6 (5)	125.9 (5)	127.4 (4)
Pt5^xxix—Sr1—Pt5^xxxi	1.2 (5)	0.7 (5)	1.7 (5)
Pt5^xxix—Sr1—Pt5^xxxii	128.1 (5)	127.8 (4)	128.2 (5)
Pt5^xxix—Sr1—As1^xxiv	133.6 (2)	129.0 (2)	136.6 (2)
Pt5^xxix—Sr1—As1^xxv	85.4 (3)	80.1 (2)	89.2 (3)
Pt5^xxx—Sr1—Pt5^xxxi	125.1 (5)	124.2 (6)	126.6 (5)
Pt5^xxx—Sr1—Pt5^xxxii	1.2 (5)	0.7 (5)	1.7 (6)
Pt5^xxx—Sr1—As1^xxiv	85.8 (3)	81.0 (2)	90.1 (3)
Pt5^xxx—Sr1—As1^xxv	133.6 (2)	129.7 (2)	137.1 (2)
Pt5^xxxi—Sr1—Pt5^xxxii	126.6 (5)	125.9 (6)	127.4 (5)
Pt5^xxxi—Sr1—As1^xxiv	133.5 (2)	129.7 (2)	137.1 (2)
Pt5^xxxi—Sr1—As1^xxv	85.7 (3)	81.0 (2)	90.1 (3)
Pt5^xxxii—Sr1—As1^xxiv	85.5 (3)	80.1 (2)	89.2 (3)
Pt5^xxxii—Sr1—As1^xxv	133.7 (2)	129.0 (2)	136.6 (2)
As1^xxiv—Sr1—As1^xxv	96.08 (5)	95.43 (6)	96.89 (6)
Pt1—As1—Pt1^xxxiii	180.0 (5)	180.0 (5)	180.0 (5)
Pt1—As1—Pt2^xxxiii	125.75 (4)	125.71 (4)	125.79 (4)
Pt1—As1—Pt2^xxxiv	125.75 (4)	125.71 (4)	125.79 (4)
Pt1—As1—Pt3^xxxiii	124.79 (4)	124.77 (4)	124.81 (4)
Pt1—As1—Pt3^xxxiv	124.79 (4)	124.77 (4)	124.81 (4)
Pt1—As1—Sr1ⁱⁱ	64.44 (3)	61.93 (3)	67.04 (3)
Pt1—As1—Sr1ⁱⁱⁱ	64.44 (3)	61.93 (3)	67.04 (3)
Pt1—As1—Sr1^iv	64.46 (3)	61.93 (3)	67.04 (3)
Pt1—As1—Sr1^v	64.46 (3)	61.93 (3)	67.04 (3)
Pt1^xxxiii—As1—Pt2^xxxiii	54.25 (4)	54.21 (4)	54.29 (4)
Pt1^xxxiii—As1—Pt2^xxxiv	54.25 (4)	54.21 (4)	54.29 (4)
Pt1^xxxiii—As1—Pt3^xxxiii	55.21 (4)	55.19 (4)	55.23 (4)
Pt1^xxxiii—As1—Pt3^xxxiv	55.21 (4)	55.19 (4)	55.23 (4)
Pt1^xxxiii—As1—Sr1ⁱⁱ	115.56 (3)	112.96 (3)	118.07 (3)
Pt1^xxxiii—As1—Sr1ⁱⁱⁱ	115.56 (3)	112.96 (3)	118.07 (3)
Pt1^xxxiii—As1—Sr1^iv	115.54 (3)	112.96 (3)	118.07 (3)
Pt1^xxxiii—As1—Sr1^v	115.54 (3)	112.96 (3)	118.07 (3)
Pt2^xxxiii—As1—Pt2^xxxiv	108.50 (7)	108.43 (7)	108.58 (7)
Pt2^xxxiii—As1—Pt3^xxxiii	70.53 (4)	69.94 (4)	71.17 (5)
Pt2^xxxiii—As1—Pt3^xxxiv	70.52 (4)	69.94 (4)	71.17 (5)
Pt2^xxxiii—As1—Sr1ⁱⁱ	76.132 (12)	71.790 (18)	80.346 (18)
Pt2^xxxiii—As1—Sr1ⁱⁱⁱ	138.03 (3)	135.78 (4)	140.24 (4)
Pt2^xxxiii—As1—Sr1^iv	76.092 (12)	71.790 (18)	80.346 (18)
Pt2^xxxiii—As1—Sr1^v	138.05 (3)	135.78 (4)	140.24 (4)
Pt2^xxxiv—As1—Pt3^xxxiii	70.52 (4)	69.94 (4)	71.17 (5)
Pt2^xxxiv—As1—Pt3^xxxiv	70.53 (4)	69.94 (4)	71.17 (5)
Pt2^xxxiv—As1—Sr1ⁱⁱ	138.03 (3)	135.78 (4)	140.24 (4)
Pt2^xxxiv—As1—Sr1ⁱⁱⁱ	76.132 (12)	71.790 (18)	80.346 (18)
Pt2^xxxiv—As1—Sr1^iv	138.05 (3)	135.78 (4)	140.24 (4)
Pt2^xxxiv—As1—Sr1^v	76.092 (12)	71.790 (18)	80.346 (18)
Pt3^xxxiii—As1—Pt3^xxxiv	110.42 (7)	110.38 (7)	110.47 (7)
Pt3^xxxiii—As1—Sr1ⁱⁱ	72.43 (3)	71.96 (3)	72.89 (3)
Pt3^xxxiii—As1—Sr1ⁱⁱⁱ	142.63 (3)	138.87 (3)	146.29 (3)
Pt3^xxxiii—As1—Sr1^iv	142.60 (3)	138.87 (3)	146.29 (3)
Pt3^xxxiii—As1—Sr1^v	72.43 (3)	71.96 (3)	72.89 (3)
Pt3^xxxiv—As1—Sr1ⁱⁱ	142.63 (3)	138.87 (3)	146.29 (3)
Pt3^xxxiv—As1—Sr1ⁱⁱⁱ	72.43 (3)	71.96 (3)	72.89 (3)
Pt3^xxxiv—As1—Sr1^iv	72.43 (3)	71.96 (3)	72.89 (3)
Pt3^xxxiv—As1—Sr1^v	142.60 (3)	138.87 (3)	146.29 (3)
Sr1ⁱⁱ—As1—Sr1ⁱⁱⁱ	128.89 (7)	123.85 (7)	134.07 (7)
Sr1ⁱⁱ—As1—Sr1^iv	83.92 (5)	83.84 (5)	83.99 (5)
Sr1ⁱⁱ—As1—Sr1^v	74.69 (4)	74.61 (4)	74.78 (6)
Sr1ⁱⁱⁱ—As1—Sr1^iv	74.69 (4)	74.61 (4)	74.78 (6)
Sr1ⁱⁱⁱ—As1—Sr1^v	83.92 (5)	83.84 (5)	83.99 (5)
Sr1^iv—As1—Sr1^v	128.93 (7)	123.85 (7)	134.07 (7)

Symmetry codes: (i) −x₁+1/2, −x₂+3/2, x₃+1/2, x₄; (ii) x₁, x₂−1/2, x₃+1/2, x₄; (iii) −x₁+1/2, −x₂+1, x₃, x₄; (iv) −x₁, −x₂+1, −x₃, −x₄; (v) x₁+1/2, x₂−1/2, −x₃+1/2, −x₄; (vi) x₁, x₂, x₃−1, x₄; (vii) −x₁, x₂, −x₃, −x₄+1/2; (viii) x₁−1/2, −x₂+3/2, −x₃+1/2, −x₄+1/2; (ix) x₁, x₂−1/2, x₃−1/2, x₄; (x) −x₁, −x₂+1, −x₃−1, −x₄; (xi) −x₁, x₂, −x₃+1, −x₄+1/2; (xii) −x₁+1/2, −x₂, x₃−1, x₄; (xiii) −x₁+1, x₂, −x₃, −x₄+1/2; (xiv) x₁−1/2, x₂, −x₃, −x₄; (xv) −x₁+1/2, x₂, x₃, x₄+1/2; (xvi) x₁+1/2, x₂−1/2, −x₃−1/2, −x₄; (xvii) −x₁+1/2, −x₂, x₃, x₄; (xviii) x₁−1/2, −x₂, −x₃, −x₄+1/2; (xix) −x₁+1, −x₂, −x₃, −x₄; (xx) x₁, −x₂, x₃, x₄+1/2; (xxi) −x₁, −x₂+3/2, −x₃+1/2, −x₄; (xxii) −x₁+1, −x₂, −x₃−1, −x₄; (xxiii) x₁, −x₂, x₃−1, x₄+1/2; (xxiv) x₁, x₂+1/2, x₃−1/2, x₄; (xxv) −x₁, x₂+1/2, −x₃+1/2, −x₄+1/2; (xxvi) x₁+1/2, −x₂, −x₃, −x₄+1/2; (xxvii) x₁, x₂+1/2, x₃+1/2, x₄; (xxviii) −x₁, x₂+1/2, −x₃−1/2, −x₄+1/2; (xxix) x₁−1/2, x₂+1/2, −x₃−1/2, −x₄; (xxx) x₁−1/2, x₂+1/2, −x₃+1/2, −x₄; (xxxi) −x₁+1/2, x₂+1/2, x₃−1/2, x₄+1/2; (xxxii) −x₁+1/2, x₂+1/2, x₃+1/2, x₄+1/2; (xxxiii) x₁, x₂, x₃+1, x₄; (xxxiv) −x₁+1/2, −x₂+3/2, x₃+3/2, x₄.

Acknowledgements

We thank Ana Akrap, Laszlo Mihaly, Karoly Holczer and Phil Allen for useful discussions.

Funding information

The following funding is acknowledged: Swiss National Science Foundation through its SINERGIA network MPBH and NCCR Marvel.

References

Behnia, K. (2015). Fundamentals of Thermoelectricity. Oxford University Press. Google Scholar
Belitz, D. & Schirmacher, W. (1983). J. Phys. C. Solid State Phys. 16, 913–926. CrossRef Web of Science Google Scholar
Chizhov, P. S., Prots, Y., Antipov, E. V. & Grin, Y. (2009). Z. Anorg. Allg. Chem. p. 635. Google Scholar
Fujioka, M., Ishimaru, M., Shibuya, T., Kamihara, Y., Tabata, C., Amitsuka, H., Miura, A., Tanaka, M., Takano, Y., Kaiju, H. & Nishii, J. (2016). J. Am. Chem. Soc. 138, 9927–9934. Web of Science CrossRef Google Scholar
Giannozzi, P., Baroni, S., Bonini, N., Calandra, M., Car, R., Cavazzoni, C., Ceresoli, D., Chiarotti, G. L., Cococcioni, M., Dabo, I. & Dal Corso, A. (2009). J. Phys. Cond. Mater. 21, 395502–1–19. Web of Science CrossRef Google Scholar
Gurvitch, M. (1981). Phys. Rev. B, 24, 7404–7407. CrossRef Web of Science Google Scholar
Hu, K. K., Gao, B., Ji, Q. C., Ma, Y. H., Zhang, H., Mu, G., Huang, F. Q., Cai, C. B. & Xie, X. M. (2016). Front. Phys. 11, 117403-1–5. Google Scholar
Jaćimović, J., Gaál, R., Magrez, A., Piatek, J., Forró, L., Nakao, S., Hirose, Y. & Hasegawa, T. (2013). Appl. Phys. Lett. 102, 013901-1–3. Google Scholar
Janssen, T., Chapuis, G. & de Boissieu, M. (2010). Aperiodic Crystals, From Modulated Phases to Quasicrystals, pp. 268–304. IUCr/Oxford University Press. Google Scholar
Kamihara, Y., Watanabe, T., Hirano, M. & Hosono, H. (2008). J. Am. Chem. Soc. 130, 3296–3297. Web of Science CrossRef PubMed CAS Google Scholar
Ku, H. C., Chen, I. A., Huang, C. H., Chen, C. W., You, Y. B., Tai, M. F. & Hsu, Y. Y. (2013). Physica C, 493, 93–95. Web of Science CrossRef Google Scholar
Kudo, K., Nishikubo, Y. & Nohara, M. (2010). J. Phys. Soc. Jpn, 79, 123710-1–4. Web of Science CrossRef Google Scholar
Lv, B., Jawdat, B. I., aan, I., Wu, Z., Sorolla, M. II, Gooch, M., Zhao, K., Deng, L., Xue, Y., Lorenz, B., Guloy, A. M. & Chu, C. (2014). Inorg. Chem. 54, 1049–1054. Web of Science CrossRef Google Scholar
Miliyanchuk, K., Kneidinger, F., Blaas-Schenner, C., Reith, D., Podloucky, R., Rogl, P., Khan, T., Salamakha, L., Hilscher, G., Michor, H., Bauer, E. & Hillier, A. D. (2011). J. Phys. Conf. Ser. 273, 012078-1–4. CrossRef Google Scholar
Moll, P. J. (2018). Annu. Rev. Condens. Matter Phys. 9, 147–162. Web of Science CrossRef Google Scholar
Moll, P. J., Puzniak, R., Balakirev, F., Rogacki, K., Karpinski, J., Zhigadlo, N. D. & Batlogg, B. (2010). Nat. Mater. 9, 628–633. Web of Science CrossRef Google Scholar
Mooij, J. H. (1973). Phys. Status Solidi A, 17, 521–530. CrossRef Web of Science Google Scholar
Nishikubo, Y., Kudo, K. & Nohara, M. (2011). J. Phys. Soc. Jpn, 80, 055002-1–2. Web of Science CrossRef Google Scholar
Oxford Diffraction (2014). CrysAlisPRO. Agilent Technologies, Oxford. Google Scholar
Palatinus, L. & Chapuis, G. (2007). J. Appl. Cryst. 40, 786–790. Web of Science CrossRef CAS IUCr Journals Google Scholar
Petříček, V., Dušek, M. & Palatinus, L. (2014). Z. Kristallogr. Cryst. Mater. 229, 345–352. Google Scholar
Sipos, B., Kusmartseva, A. F., Akrap, A., Berger, H., Forró, L. & Tutiš, E. (2008). Nat. Mater. 7, 960–965. Web of Science CrossRef Google Scholar
Smaalen, S. van, Campbell, B. J. & Stokes, H. T. (2013). Acta Cryst. A69, 75–90. Web of Science CrossRef IUCr Journals Google Scholar
Stokes, H. T., Campbell, B. J. & van Smaalen, S. (2011). Acta Cryst. A67, 45–55. Web of Science CrossRef CAS IUCr Journals Google Scholar
Subedi, A., Ortenzi, L. & Boeri, L. (2013). Phys. Rev. B, 87, 144504-1–7. Google Scholar
Takayama, T., Kuwano, K., Hirai, D., Katsura, Y., Yamamoto, A. & Takagi, H. (2012). Phys. Rev. Lett. 108, 237001-1–5. Web of Science CrossRef Google Scholar
Takeuchi, T., Muranaka, H., Settai, R. D., Matsuda, T., Yamamoto, E., Haga, Y. & Ōnuki, Y. (2009). J. Phys. Soc. Jpn, 78, 085001–1–2. Web of Science CrossRef Google Scholar
Tsuei, C. C. (1986). Phys. Rev. Lett. 57, 1943–1946. CrossRef Web of Science Google Scholar
Voit, J., Perfetti, L., Zwick, F., Berger, H., Margaritondo, G., Grüner, G., Höchst, H. & Grioni, M. (2000). Science, 290, 501–503. Web of Science CrossRef Google Scholar
Zhou, Z., Palatinus, L. & Sun, J. (2016). Inorg. Chem. Front. 3, 1351–1362. Web of Science CrossRef Google Scholar
Zocco, D. A., Krannich, S., Heid, R., Bohnen, K. P., Wolf, T., Forrest, T., Bosak, A. & Weber, F. (2015). Phys. Rev. B, 92, 220504-1–5. Web of Science CrossRef Google Scholar

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IUCrJ

Volume 5| Part 4| July 2018| Pages 470-477

ISSN: 2052-2525

https://doi.org/10.1107/S2052252518007303

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