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Figure 2
PXRD patterns of pristine and water-treated (a) AEPz-SnS-1 and (b) trenH-SnS-1. The positions of the (100) and (002) peaks of the pristine samples are shown. The peak at 0.86 Å−1 corresponds to (102). The calculated patterns are based on the crystal structure of trenH-SnS-1 (Filsø et al., 2017BB7). Peaks from a minor SnO2 impurity are observed at 1.88 and 2.38 Å−1 in the 20 and 60 min trenH-SnS-1 samples. The same batch of trenH-SnS-1 was used for preparation of all samples presented in Figs. 2[link](b) and 2[link](d), and the SnO2 peaks are barely observable except for samples with low thio­stannate crystallinity, i.e. 20 and 60 min trenH-SnS-1 (see Figs. S1b and S6). PDFs of pristine and water-treated (c) AEPz-SnS-1 and (d) trenH-SnS-1.

IUCrJ
Volume 6| Part 5| September 2019| Pages 804-814
ISSN: 2052-2525
https://doi.org/10.1107/S2052252519006791