Extraordinary structural complexity of ilmajokite: a multilevel hierarchical framework structure of natural origin

The crystal structure of ilmajokite, a rare Na-K-Ba-Ce-titanosilicate from the Khibiny mountains, Kola peninsula, Russia, has been solved using single-crystal X-ray diffraction data. The crystal structure is based on a 3D titanosilicate framework consisting of trigonal prismatic titanosilicate (TPTS) clusters centered by Ce³⁺ in [9]-coordination. Four adjacent TPTS clusters are linked into four-membered rings within the (010) plane and connected via ribbons parallel to 101. The ribbons are organized into layers parallel to (010) and modulated along the a axis with a modulation wavelength of csinβ = 32.91 Å and an amplitude of ∼b/2 = 13.89 Å. The layers are linked by additional silicate tetrahedra. Na⁺, K⁺, Ba²⁺ and H₂O groups occur in the framework cavities and have different occupancies and coordination environments. The crystal structure of ilmajokite can be separated into eight hierarchical levels: atoms, coordination polyhedra, TPTS clusters, rings, ribbons, layers, the framework and the whole structure. The information-based analysis allows estimation of the complexity of the structure as 8.468 bits per atom and 11990.129 bits per cell. According to this analysis, ilmajokite is the third-most complex mineral known to date after ewingite and morrisonite, and is the most complex mineral framework structure, comparable in complexity to paulingite-(Ca) (11 590.532 bits per cell).

1. Introduction

Minerals constitute a distinct group of crystalline materials formed by natural geochemical or biogeochemical processes without any anthropogenic influence. Approximately 5500 different mineral species are known today with more than 100 new species discovered every year. Many of these minerals have their synthetic counterparts, but there are many minerals that have no artificial analogs (Khomyakov, 1994). Their existence and formation under natural conditions represent a serious challenge for both mineralogists and material scientists looking for new structural architectures with interesting physical and chemical properties. Recently, a number of highly complex minerals has been characterized with structural features never before seen in synthetic materials. In particular, the crystal structures of charoite and denisovite are based on different kinds of silicate nanotubules (Rozhdestvenskaya et al., 2009, 2010, 2017), and ewingite (Olds et al., 2017) and morrisonite (Kampf et al., 2016) contain novel types of nanoscale heteropolyhedral clusters.

One interesting group of minerals with unique and important properties are titanosilicates. Due to their microporosity and catalytic activity, titanosilicates continue to attract considerable attention in the fields of materials science and nanochemistry (Rocha & Anderson, 2000; Noh et al., 2012; Milyutin et al., 2017; Oleksiienko et al., 2017; Přech, 2018; Cuko et al., 2018; Figueiredo et al., 2018). At the same time, they are of great interest from the viewpoint of mineralogy and geochemistry given their large diversity mostly in alkaline rocks such as those occurring in the alkaline massifs of the Kola peninsula, Russia, and Mont-Saint-Hilaire, Quebec, Canada (Cámara et al., 2017; Sokolova et al., 2017; Sokolova & Cámara, 2017; Selivanova et al., 2018; Zolotarev et al., 2018; Andrade et al., 2018; Lykova et al., 2018; Pakhomovsky et al., 2018; Pekov et al., 2019; Zhitova et al., 2019). Indeed, most titanosilicate materials used in industry were found as minerals before their unique properties were recognized. For instance, ETS-4 (Engelhardt titanosilicate-4; Kuznicki et al., 2001) is a synthetic analog of zorite, first described by Soviet mineralogists in the Kola peninsula in 1973 (Mer'kov et al., 1973). The ion-exchanger UOP-910, which is used for the removal of Cs-137 from radioactive-waste solutions (Anthony et al., 1994), is a natural counterpart of sitinakite, a microporous titanosilicate from hydrothermal veins of the Khibiny massif, Kola peninsula, Russia (Sokolova et al., 1989; Men'shikov et al., 1992). Another family of recently described microporous titanosilicates, the ivanyukite-group minerals (Yakovenchuk et al., 2009), have the pharmacosiderite-type structure, well known as a useful synthetic material since the 1990s (Harrison et al., 1995). There are many other unique natural titanosilicates with interesting structures that have no precedents among synthetic materials. For instance, yuksporite is based on nanoscale porous titanosilicate tubes that have never been prepared under laboratory conditions to date (Krivovichev et al., 2004).

Herein we report on the structural and chemical features of ilmajokite, a rare titanosilicate from the Lovozero tundra, Kola peninsula, Russia. The mineral occurs in the `Yubileynaya' pegmatite vein, Karnasurt Mountain, near the river Ilmajok and lake Ilma. Ilmajokite is found as crystals and crystalline crusts on the surfaces of voids in natrolite (Bussen et al., 1972). The fresh crystals are yellowish and transparent. In air, they slowly become cloudy and fragment into separate plates and fibers. The chemical formula, determined by wet chemical analysis, was given as (Na_8.8Ba_0.5REE_0.7)_Σ = 10(Ti_4.99(Fe,Al,Nb)_0.01)_Σ = 5(Si_13.9Al_0.01)_Σ = 14O₂₂(OH)₄₄·nH₂O (the formula was proposed by I. D. Borneman-Starynkevich). The admixture of nahcolite, NaHCO₃, was mentioned, which significantly increased the observed amount of Na. Ilmajokite has a large quantity of H₂O (24.54 wt%), which is released on heating; the mineral loses up to 12.7% at 175°C, although 6.5% is still retained at 320°C. Release of H₂O starts as low as 60°C but it is not complete until 760°C (Bussen et al., 1972). H-speciation was determined by infra-red (IR) spectroscopy based on broad absorptions at 1618 and 3389–2889 cm⁻¹.

The instability of ilmajokite crystals under atmospheric conditions prevented detailed crystallographic study for a long time. Bussen et al. (1972) determined the mineral to be probably monoclinic with unit-cell parameters a ≃ 23, b ≃ 24.4, c ≃ 37 Å. A later study by Goiko et al. (1974) on fresh material held hermetically after extraction from the pegmatite confirmed the monoclinic symmetry and determined the unit-cell parameters to be a = 39.80, b = 29.5, c = 29.83 Å, β = 96.63°, V = 34788 ų, possible space groups C2/c or Cc. Cámara et al. (2010) investigated single crystals of ilmajokite provided by E. I. Semenov in 2004 (sample ILM01). The study at room temperature gave a C-centered monoclinic cell with a = 35.774 (4), b = 27.407 (3), c = 31.131 (5) Å, β = 95.66 (1)°, V = 30374 (7) ų. The R_int value was very high (∼32%) and no model could be obtained from these data. A low-temperature data collection at 125 K slightly enhanced the data quality, but no solution could be found. The cell refinement confirmed a C-centered cell with a = 35.32 (16), b = 26.93 (12), c = 30.68 (14) Å, β = 95.84 (2)°, V = 29034 (403) ų. A further study was done later by some of the authors (FC, LB, FCH and ES) on another crystal provided by C. Ferraris (Muséum National d'Histoire Naturelle, Paris, France; catalog number 197.68) in 2010 (ILM02), extracted from a sample deposited at the National School of Mines, Paris, France. This time, a high-performing BRUKER APEX II ULTRA single-crystal diffractometer was used (Turbo X-ray source coupled with the HELIOS Mo optics provides up to 60 times more intense data from small crystals) at the Department of Geological Sciences of the University of Manitoba, Canada. The results were very similar to the previous ones [refined unit cell: a = 36.084 (18), b = 27.726 (13), c = 31.248 (15) Å, β = 98.051 (5)°, V = 30953 (45) ų] but with a better internal agreement factor (R_int ≃ 5%). Yet again, systematic absences were compatible with space groups C2/c or Cc, but no model could be obtained from these data as they were very weak at d < 2.3 Å (Fig. S1 of the supporting information), and show high mosaicity. Interestingly, mosaicity begins at lower resolution along [Fig. S1(b)].

Considerable attempts have been made by separate groups to obtain the structure model for ilmajokite, but with no success. Recently, the first author (AAZ) found a single crystal of ilmajokite in the collections of the Fersman Mineralogical Museum of the Russian Academy of Sciences (Moscow, Russia) which allowed data collection good enough to resolve the atomic arrangement of this unusual mineral. The good quality of the crystal was due to the fact that it was covered by lacquer soon after extraction of the sample from the host rock.

2. Materials and methods

2.1. Sample description

The holotype sample was obtained from the Fersman Mineralogical Museum of the Russian Academy of Sciences (Moscow, Russia), where it is stored under catalog number 86969. The sample originates from the Yubileinaya pegmatite (Karnasurt Mountain, Lovozero, Kola Peninsula) (Pekov, 2001) where it is one of the latest primary minerals. We checked several single crystals and we were able to obtain acceptable X-ray diffraction data for one of them. The crystal selected for data collection was a yellowish transparent plate was 0.15 × 0.08 × 0.04 mm in size.

2.2. Chemical composition

The chemical composition of ilmajokite was determined on ilmajokite crystals from the sample ILM02 using a CAMECA SX-100 electron-microprobe at the Department of Geological Sciences of the University of Manitoba, Canada, operating in wavelength-dispersion mode with an accelerating voltage of 15 kV, a specimen current of 5 nA, a beam size of 15 µm and count times on peak and background of 20 and 10 s, respectively. The results are reported in Table S1 of the supporting information. Even with such a large beam, the material showed significant beam damage (Fig. S2) and Na loss (see, for instance, analyses 5, 8, 9 and 10, Table S1). Overlap of BaLβ on CeLα and CeMζ on FKα were accounted for. The elements Zn, Sr, Gd and U were sought but not detected. Data were reduced using the PAP procedure by Pouchou & Pichoir (1985).

Analyses show Na loss even under mild conditions (5 nA and 15 µm defocalized beam) with a progressive loss of Na. Also, the formation of cracks on the surface denotes volatilization under vacuum (typical for micro and mesoporous hydrated phases). Totals decrease from 90 wt% to ca 86 wt%. Fluorine is absent. Normalization on the basis of 218 charges (see Section 3.4 crystal-chemical formula) using the average of points 1, 2, 3, 4 and 11 (in a separate fragment) gave the empirical formula (Na_9.55K_1.09Ba_0.84Ca_0.08Th_0.08)_Σ11.64(REE_1.99Y_0.01)₂(Ti_11.98Ta_0.05Nb_0.01Mn_0.01Mg_0.01Fe²⁺_0.01Zr_0.01)_Σ12.08[Si_37.72Al_0.03]O₁₀₉, with REE = Ce_0.99La_0.59Nd_0.27Pr_0.10Sm_0.03Dy_0.01.

2.3. Single-crystal X-ray diffraction

Single-crystal X-ray diffraction study of ilmajokite was done at the Resource Center `X-ray Diffraction Methods' of St Petersburg State University using the Bruker Kappa APEX DUO diffractometer (microfocus tube) equipped with a CCD area detector. The study was done using monochromatic Mo Kα X-radiation (λ = 0.71073 Å), with frame widths of 0.5° in ω and 30 s counting time for each frame. The intensity data were reduced and corrected for Lorentz, polarization and background effects using the Bruker software APEX2 (Bruker-AXS, 2014). A semiempirical absorption-correction based upon the intensities of equivalent reflections was applied using SADABS (Sheldrick, 2007). The structure was solved and refined in the space group C2/c to R₁ = 0.081 (wR₂ = 0.233) for 14 797 unique observed reflections with I ≥ 2σ(I) using the SHELX program package (Sheldrick, 2015) within the Olex2 shell (Dolomanov et al., 2009). Crystal data, data collection information and refinement details are given in Table 1.

Table 1
Crystal data and structure refinement for ilmajokite

Crystal data
Chemical formula	Ba0.45H44.25Ce1.04K0.55Na5.62O76.74Si18.76Ti6
Mr	2445.37
Crystal system, space group	Monoclinic, C2/c
Temperature (K)	296
a, b, c (Å)	35.908 (5), 27.784 (3), 33.126 (4)
β (°)	96.494 (3)
V (Å^3)	32836 (7)
Z	16
Radiation type	Mo Kα
μ (mm^−1)	1.79
Crystal size (mm)	0.15 × 0.08 × 0.04
Data collection
Diffractometer	Bruker Kappa APEX DUO
Absorption correction	Multi-scan
No. of measured, independent, observed [I > 2σ(I)] reflections	108441, 21527, 14797
Rint	0.130
θmax (°)	22.7
(sin θ/λ)max (Å^−1)	0.543
Refinement
R[F^2 > 2σ(F^2)], wR(F^2), S	0.081, 0.264, 0.97
No. of parameters	1847
No. of restraints	18
H-atom treatment	H-atom parameters not defined
	w = 1/[σ^2(Fo^2) + (0.1738P)^2 + 608.3564P] where P = (Fo^2 + 2Fc^2)/3
Δρmax, Δρmin (e Å^−3)	1.89, −2.80

The unit-cell parameters of ilmajokite determined in our study correspond well with those reported by Cámara et al. (2010) for their room-temperature study. The most significant difference is for the c parameter, which in our study is about 2 Å longer than that determined by Cámara et al. (2010). It is most likely that this difference is due to the different hydration states of the two samples, which also explains the lower quality of the diffraction data for the crystal with the smaller c parameter (see Fig. S1).

3. Results

3.1. Atom coordination

The crystal structure of ilmajokite contains 236 symmetrically independent sites, including 1 Ba, 2 REE (rare-earth elements, with Ce as the dominant component), 12 Ti, 41 Si, 15 Na, 3 K, 84 O, 38 OH and 40 H₂O sites. Cation coordination numbers, average bond lengths and their variations, and bond-valence sums are given in Table 2. The coordination of Ti⁴⁺ and Si⁴⁺ cations is octahedral and tetrahedral, as is typical for many other natural and synthetic titanosilicates (Krivovichev, 2005). The low coordination numbers and bond-valence sums for several alkali-metal (Na, K) sites are due to their low occupancies (up to 0.22). Of 84 O sites, 38 are bridging between adjacent Si atoms; 44 are bridging between Si and Ti atoms; 5 are bonded to Si, Ti and Ce atoms; 6 are bonded to two Ti and one Ce atoms each; one is bonded to two Ti and one Si atoms. Of 38 OH groups, 4 are bonded to two Ti atoms, and the remaining 34 are terminal (silanol) groups of SiO₄ tetrahedra. The bond-valence sums for the O atoms, OH and H₂O groups (without contributions from the H atoms) are in the ranges 1.73–2.28, 0.89–1.42 and 0.0–0.58, respectively. The most significant deviations from the expected values (2.00, 1.20 and 0–0.40, respectively) are observed for disordered cation sites that cannot be estimated correctly.

Table 2
Coordination numbers (CNs) of cations, average bond lengths and their variations (Å), and bond-valence sums (BVS, in valence units, v.u.) for the crystal structure of ilmajokite

Bond valence units were calculated using parameters from Gagné & Hawthorne (2015).

Atom	CN	Bond lengths		BVS
		Average	Range (min–max)
Ba	10	2.899	2.818–2.968	1.91
K	6, 7	2.816	2.403–3.308	1.03–1.27
Na	3, 5, 6, 7, 8	2.555	1.999–3.022	0.42–1.10
Ce	9	2.543	2.481–2.626	3.00
Ti	6	1.955	1.853–2.105	3.99–4.17
Si	4	1.621	1.512–1.671	3.87–4.27

3.2. Local topological features

The crystal structure of ilmajokite is based on a titanosilicate framework of unprecedented complexity. Analysis of the local topological features of the SiO₄ tetrahedra shows that they belong to ten different types, from Q² (two-connected) to Q⁵ groups [herein, Qⁿ indicates a tetrahedron that shares its O corners with n adjacent coordination polyhedra (only Si and Ti polyhedra are taken into account)]. The Q⁵ type is not typical for silicate frameworks of corner-sharing tetrahedra (Liebau, 1985), but occurs in octahedral–tetrahedral frameworks. In ilmajokite, it corresponds to the Si10O₄ tetrahedron that shares three of its corners with three adjacent tetrahedra and one corner with two TiO₆ octahedra sharing a common edge (see below). In order to distinguish between silicate tetrahedra of the same type but with different chemical environments, we use the notation Qⁿ_{mTi + kSi}, where m + k = n. For instance, there are three types of Q³ tetrahedra in ilmajokite, Q³_Ti + 2Si, Q³_3Si and Q³_2Ti + Si. The complete local topological classification of silicate tetrahedra in ilmajokite is given in Table 3. It is noteworthy that all Q²_2Si tetrahedra are only partly occupied with site occupancies less than 0.5.

Table 3
Topological types of Si tetrahedra in the crystal structure of ilmajokite

General type	Specific type	Si Sites
Q^2	Q^2Si + Ti	3, 21
	Q^22Si	17†, 37†, 38†, 39†, 40†, 41†
	Q^22Ti	36
Q^3	Q^32Si + Ti	2, 8, 9, 14, 19, 29, 33, 35
	Q^33Si	5, 13, 24, 25
	Q^32Ti + Si	20, 31
Q^4	Q^42Ti + 2Si	1, 4, 6, 12, 15, 16, 18, 22, 23, 26, 27, 28, 32, 34
	Q^44Ti	7
	Q^43Si + Ti	11, 30
Q^5	Q^53Si + 2Ti	10

†Partially occupied sites.

3.3. Structural organization

The projection of the crystal structure of ilmajokite along the c axis is shown in Fig. 1. The titanosilicate framework has a complex organization that can be described as follows. Two TiO₆ octahedra share a common edge to form a [Ti₂O₁₀] dimer. Three dimers with parallel orientation form a trigonal prism centered by Ce³⁺ in [9]-coordination. The triple-dimer titanate structure is surrounded by SiO₄ tetrahedra to form a trigonal prismatic titanosilicate cluster, further denoted as a TPTS cluster. There are two symmetrically different TPTS clusters centered by the Ce1 and Ce2 atoms [Figs. 2(a) and 2(c)]. For further description of the structural topology of the framework, we adopt a nodal representation, where each Ti and Si polyhedron is symbolized by a node of respective color and two nodes are linked by an edge if the two corresponding polyhedra share a common O atom. This approach is widely used for the description of complex topologies observed in zeolite-type tetrahedral (Baerlocher et al., 2007; Smith, 2000) and heteropolyhedral (Krivovichev, 2005; Krivovichev et al., 2005) frameworks. The nodal representation of the two independent TPTS clusters in ilmajokite is given in Figs. 2(b) and 2(d).

Figure 1 Projection of the crystal structure of ilmajokite along the c axis. Legend: Si tetrahedra – yellow, Ti octahedra – blue; H2O molecules, Na, K, Ba and Ce atoms are shown as red, light-blue, green, brown and orange spheres, respectively.

Figure 2 TPTS clusters in the crystal structure of ilmajokite shown in (a) and (c) polyhedral and (b) and (d) nodal representations. The numbering scheme corresponds to the numbering of Si and Ti atoms from the experiment. The Ce-centered Ti6 trigonal prism is highlighted in yellow. The legend follows that of Fig. 1.

Four adjacent TPTS clusters are linked via the Si9–Si19 links and the Si7O₄ tetrahedron (note that this is the only Q⁴_4Ti tetrahedron in the crystal structure) to form a four-membered ring (Fig. 3). The rings are arranged within the (010) plane [Fig. 4(a)] and linked via partly occupied Si39, Si40 and Si41 polyhedra (Q²_2Si type) into ribbons parallel to [Fig. 4(b)]. A schematic description of the topology of the chain is given in Fig. 5. The ribbons are organized into layers parallel to (010). The view of the layers along the a axis [Fig. 6(a)] shows that they are modulated with a modulation wavelength of csinβ = 32.91 Å and an amplitude of ∼b/2 = 13.89 Å. The layers are linked via Si14, Si14 and Si31 tetrahedra; with the first two partly occupied (the Q²_2Si type) and the last fully occupied (the Q³_2Ti + Si type). Thus the most condensed unit in the titanosilicate framework is the four-membered ring of the TPTS clusters, whereas the linkage of the rings proceeds via Si14, Si31, Si37, Si38, Si39, Si40 and Si41 tetrahedra; with only Si31 fully occupied, whereas the others are less than half-occupied.

Figure 3 Four-membered ring of the TPTS clusters shown in (a) polyhedral and (b) nodal representations. Legend and numbering scheme follow that of Fig. 1.

Figure 4 (a) Arrangement of the four-membered rings of the TPTS clusters within the (010) plane and (b) their linkage through additional Si39, Si40 and Si41 nodes into ribbons.

Figure 5 Schematic representation of the topology of ribbons formed by TPTS (CeTi6Si17) clusters in ilmajokite (four-membered rings are highlighted in gray).

Figure 6 (a) Arrangement of layers of ribbons of TPTS clusters along the b axis and (b) their linkage into a 3D framework via Si14, Si31 and Si37 nodes.

Na⁺, K⁺, Ba²⁺ and H₂O groups occur in the framework cavities and have different occupancies and coordination environments (Table 2).

It is noteworthy that the mosaicity observed in the ILM02 crystal has lower resolution in the direction of the ribbons, reflecting damage in the structure of that crystal, probably related to amorphization by dehydration.

3.4. Crystal-chemical formula

The crystal-chemical formula determined from the structure refinement is Na_11.24K_1.10Ba_0.90Ce₂Ti₁₂Si_37.52O₉₄(OH)_30.38·(H₂O)_29.06, in close agreement between the sums of the positive (+218.22) and negative (−218.38) charges, which is remarkable in view of the difficulties associated with the structure refinement. There is also a very good agreement with the results of the electron-microprobe analysis (see Section 2.2), particularly considering the difficulty due to dehydration and Na migration under the beam. Assuming that the selected points with less Na are closer to the actual H₂O content, the formula is in accordance with 14 H₂O groups per formula unit and the following empirical formula: (Na_9.55K_1.09Ba_0.84Ca_0.08Th_0.08)_Σ11.64(REE_1.99Y_0.01)₂(Ti_11.96Ta_0.05Nb_0.01Mn_0.01Mg_0.01Fe²⁺_0.01Zr_0.01)_Σ12.06[Si_37.68Al_0.03]O₉₄(OH)₃₀·(H₂O)_14.18, with REE = Ce_0.99La_0.59Nd_0.27Pr_0.10Sm_0.03Dy_0.01.

Taking into account the presence of the titanosilicate framework and its silicate sub-framework, the detailed crystal-chemical formula of ilmajokite may be written as Na_11.24K_1.10Ba_0.90〈Ce₂{Ti₁₂[Si_37.52O₈₈(OH)_26.38]O₆(OH)₄}〉·(H₂O)_29.06, where square, curly and angular brackets denote silicate, titanosilicate and rare-earth-titanosilicate substructures. On the basis of both chemical and structural data, the ideal crystal-chemical formula of ilmajokite can be written as Na₁₁KBaCe₂Ti₁₂Si_37.5O₉₄(OH)₃₁^.29H₂O, which requires SiO₂ 46.06, TiO₂ 19.60, Ce₂O₃ 6.69, BaO 3.14, Na₂O 6.97, K₂O 0.96, H₂O 16.58 (total 100 wt%). The amount of H₂O in the crystal-chemical formula disagrees with the value of 24.54 wt% reported by Bussen et al. (1972), which could be due to the possibility of variable hydration states frequently observed for microporous framework minerals. The two-step dehydration described by Bussen et al. (1972) may correspond to the loss of zeolitic H₂O and the complete dehydration associated with the hydroxyl groups.

The ideal formula of the silicate sub-framework, assuming full occupancy of the partly occupied Si and associated OH sites, and excluding the Si37–Si38 disorder, can be written as [Si₄₀O₈₈(OH)₃₂]⁴⁸⁻ or [Si₅O₁₁(OH)₄]⁶⁻ with the amazingly simple Si:O ratio of 1:3. It is interesting to note that the Si:O 1:3 ratio has previously been reported for other rather complex silicate minerals such as hyttsjöite, Pb₁₈Ba₂Ca₅Mn₂²⁺Fe₂³⁺[Si₃₀O₉₀]Cl(H₂O)₆ (Grew et al., 1996); aerinite, Ca₆FeAl(Fe,Mg)₂(Al,Mg)₆[Si₁₂O₃₆](OH)₁₂H)(H₂O)₁₂(CO₃) (Rius et al., 2004, 2009); and sveinbergeite, (H₂O)₂(Ca(H₂O))(Fe₆²⁺Fe³⁺)Ti₂[Si₄O₁₂]₂O₂(OH)₄((OH)H₂O)) (Khomyakov et al., 2011). We note that the silicate subframework found in the crystal structure of ilmajokite is new and has not been observed previously in any mineral or inorganic compound (Pushcharovsky et al., 2016).

4. Discussion

4.1. Hierarchical analysis

The economist and Nobel laureate Herbert Simon once noted that `hierarchy… is one of the central structural schemes that the architect of complexity uses' (Simon, 1962). The high number of hierarchical levels of structural organization (hierarchical depth) reflects the high degree of complexity of a system. As has been noted previously [see, e.g. Makovicky (1997); Ferraris et al. (2004); Hawthorne (2014)], the crystal structures of minerals and inorganic compounds have a hierarchical organization [see Krivovichev (2017) for a detailed discussion and examples]. From this point of view, the crystal structure of ilmajokite possesses a multilevel hierarchical structure (Fig. 7). The first (lowest) level consists of atoms that are grouped into coordination polyhedra (second level). The TiO₆ octahedra are linked to form dimers (third level). The dimers together with SiO₄ tetrahedra and centering Ce³⁺ cations comprise TPTS clusters (fourth level). The clusters are linked to form four-membered rings (fifth level), which are further interlinked to form ribbons (sixth level). The ribbons are united into a three-dimensional octahedral–tetrahedral framework (seventh level), which, together with alkali metal, Ba²⁺ cations and H₂O molecules complete the structure organization (eighth level). The subdivision of the structure into eight levels reflects its high complexity which is considered in the next section.

Figure 7 Hierarchial organization of the crystal structure of ilmajokite separated into eight hierarchy levels (highlighted in gray).

4.2. Complexity analysis

The complexity of the crystal structure of ilmajokite can be quantitatively estimated using information-based complexity measures recently proposed by Krivovichev (2012, 2013, 2014). Since the positions of the H atoms were not determined from the single-crystal diffraction experiment, the procedure of H-correction was applied as described by Pankova et al. (2018). The resulting parameters are as follows: the number of atoms per reduced unit cell, v, is equal to 1416; the amount of Shannon information per atom, I_G, is 8.468 bits; and the amount of Shannon information per unit cell, I_G, total, is 11 990.129 bits. The parameters without H-corrections are v = 972, I_G = 7.925 bits per atom, I_G, total = 7702.918 bits per cell, which means that hydration is responsible for ca 36% of the total structural complexity. The total value of Shannon information places ilmajokite as the third-most complex mineral known to date after ewingite, Mg₄Ca₄(UO₂)₁₂(CO₃)₁₅O₂(OH)₆·69H₂O [23 477.507 bits per cell with H-correction and 12 684.86 bits per cell without H-correction (∼46% of total complexity is due to H atoms); Olds et al. (2017)] and morrisonite, Ca₁₁(As³⁺V₂⁴⁺V₁₀⁵⁺As₆⁵⁺O₅₁)₂·78H₂O [13 588.350 bits per cell with H-correction and 7553.229 bits per cell after H-correction (H atoms are responsible for ∼44% of structural complexity); Kampf et al. (2016)]. Since both ewingite and morrisonite contain nanoscale clusters, ilmajokite is the most complex with a framework structure, and in terms of its complexity, is very close to paulingite-(Ca), Ca₅(Al₁₀Si₃₂O₈₄)·34H₂O [11 590.532 bits per cell with H-correction and 6766.998 bits per cell after H-correction (∼42% complexity is due to H atoms); Passaglia et al. (2001)].

5. Conclusions

Under natural conditions, ilmajokite forms as one of the latest minerals of hydrothermal activity, which includes several stages and a range of precursor phases that precede the crystallization of the mineral. The extreme complexity of ilmajokite is the result of a combination of a number of factors, including its high chemical complexity and seggregation of chemically different elements (Na, K, Ba, Ce, Ti, Si) into their own crystallographic sites (the most interesting is the absence of any detectable K–Ba substitution), the presence of polynuclear TPTS clusters of nanoscale size (the diameter of the cluster is around 1.4 nm), condensation of the TPTS clusters into larger four-membered units, the high hydration state, etc.

Supporting information

Computing details

(I)

Crystal data

0.06(Ba7.21Ce16.68K8.85Na90.08O1228.82Si300.33Ti96)	F(000) = 18664
Mr = 2445.37	Dx = 1.943 Mg m^−3
Monoclinic, C2/c	Mo Kα radiation, λ = 0.71073 Å
a = 35.908 (5) Å	Cell parameters from 21527 reflections
b = 27.784 (3) Å	θ = 2.4–22.5°
c = 33.126 (4) Å	µ = 1.78 mm^−1
β = 96.494 (3)°	T = 296 K
V = 32836 (7) Å^3	Prism, yellow
Z = 16	0.15 × 0.08 × 0.04 mm

Data collection

Bruker APEX-II CCD diffractometer	14797 reflections with I > 2σ(I)
Graphite monochromator	Rint = 0.130
φ and ω scans	θmax = 22.7°, θmin = 0.9°
Absorption correction: multi-scan SADABS-2008/1 (Bruker,2008) was used for absorption correction. wR2(int) was 0.1858 before and 0.0891 after correction. The Ratio of minimum to maximum transmission is 0.7712. The λ/2 correction factor is 0.0015.	h = −38→29
Tmin = 0.574, Tmax = 0.745	k = −30→29
108441 measured reflections	l = −35→35
21527 independent reflections

Refinement

Refinement on F^2	18 restraints
Least-squares matrix: full	w = 1/[σ^2(Fo^2) + (0.1738P)^2 + 608.3564P] where P = (Fo^2 + 2Fc^2)/3
R[F^2 > 2σ(F^2)] = 0.081	(Δ/σ)max = 0.001
wR(F^2) = 0.264	Δρmax = 1.89 e Å^−3
S = 0.97	Δρmin = −2.80 e Å^−3
21527 reflections	Extinction correction: SHELXL-2014/7 (Sheldrick 2014), Fc^*=kFc[1+0.001xFc^2λ^3/sin(2θ)]^-1/4
1847 parameters	Extinction coefficient: 0.000146 (17)

Special details

Geometry. All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes.

Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Ų)

	x	y	z	Uiso*/Ueq	Occ. (<1)
Ce1	0.20679 (2)	0.91394 (3)	0.32979 (2)	0.0237 (3)	1.032 (4)
Ce2	0.46087 (2)	0.25029 (3)	0.47339 (2)	0.0208 (3)	1.053 (4)
Ba	0.61658 (3)	0.33323 (4)	0.45904 (3)	0.0311 (4)	0.900 (4)
Ti1	0.10729 (6)	0.89377 (8)	0.30245 (7)	0.0195 (6)
Ti2	0.14972 (6)	0.81237 (9)	0.34976 (7)	0.0207 (6)
Ti3	0.27994 (7)	0.85909 (10)	0.28013 (7)	0.0286 (6)
Ti4	0.24803 (8)	0.94456 (11)	0.43058 (8)	0.0369 (7)
Ti5	0.26275 (7)	0.44254 (10)	0.26648 (7)	0.0278 (6)
Ti6	0.20854 (7)	0.02466 (10)	0.38579 (8)	0.0328 (7)
Ti7	0.38037 (7)	0.30425 (9)	0.51024 (7)	0.0249 (6)
Ti8	0.48977 (6)	0.26694 (9)	0.37312 (7)	0.0205 (6)
Ti9	0.50811 (6)	0.34914 (8)	0.43224 (7)	0.0195 (6)
Ti10	0.50057 (7)	0.13685 (8)	0.50814 (7)	0.0233 (6)
Ti11	0.51812 (6)	0.22140 (8)	0.56760 (7)	0.0215 (6)
Ti12	0.36370 (7)	0.22388 (9)	0.44925 (8)	0.0285 (6)
Si1	0.30241 (11)	0.87893 (17)	0.37873 (12)	0.0337 (10)
Si2	0.36080 (11)	0.88931 (17)	0.32477 (13)	0.0388 (11)
Si3	0.22256 (16)	0.8795 (2)	0.50752 (15)	0.0607 (15)
Si4	0.20909 (11)	0.83869 (15)	0.42709 (11)	0.0289 (9)
Si5	0.27520 (11)	0.78142 (17)	0.40462 (12)	0.0363 (11)
Si6	0.23085 (11)	0.78012 (14)	0.32142 (11)	0.0267 (9)
Si7	0.06318 (10)	0.83058 (13)	0.36330 (11)	0.0212 (8)
Si8	0.16965 (11)	0.71079 (14)	0.30562 (12)	0.0281 (9)
Si9	0.42208 (11)	0.27362 (14)	0.29845 (11)	0.0260 (9)
Si10	0.17031 (12)	0.45845 (18)	0.23636 (14)	0.0423 (12)
Si11	0.21716 (12)	0.54196 (17)	0.25906 (15)	0.0430 (12)
Si12	0.27852 (11)	0.53795 (15)	0.21048 (13)	0.0324 (10)
Si13	0.35970 (12)	0.54720 (15)	0.24532 (13)	0.0331 (10)
Si14	0.37330 (12)	0.57436 (15)	0.10173 (13)	0.0329 (10)
Si15	0.37344 (10)	0.50147 (13)	0.16430 (12)	0.0249 (9)
Si16	0.35260 (10)	0.44389 (14)	0.27146 (11)	0.0234 (9)
Si17	0.1525 (2)	0.4340 (3)	0.3203 (2)	0.052 (3)	0.633 (15)
Si18	0.22126 (13)	0.36572 (18)	0.31622 (13)	0.0451 (12)
Si19	0.41971 (10)	0.38615 (14)	0.29463 (11)	0.0240 (9)
Si20	0.30131 (12)	0.30380 (17)	0.45548 (14)	0.0398 (11)
Si21	0.46164 (11)	0.45180 (13)	0.42781 (11)	0.0236 (8)
Si22	0.44292 (10)	0.38262 (13)	0.48730 (11)	0.0210 (8)
Si23	0.40694 (10)	0.21807 (14)	0.36960 (11)	0.0243 (9)
Si24	0.43473 (12)	0.11394 (15)	0.37805 (13)	0.0339 (10)
Si25	0.49389 (11)	0.38657 (13)	0.56719 (11)	0.0241 (9)
Si26	0.50831 (11)	0.16017 (14)	0.41145 (11)	0.0258 (9)
Si27	0.45142 (10)	0.29297 (13)	0.58135 (11)	0.0212 (8)
Si28	0.41587 (11)	0.12646 (14)	0.46470 (12)	0.0287 (9)
Si29	0.38108 (11)	0.31928 (15)	0.60925 (12)	0.0310 (10)
Si30	0.33821 (12)	0.11906 (16)	0.48102 (13)	0.0361 (10)
Si31	0.27229 (14)	0.04940 (19)	0.45557 (14)	0.0474 (13)
Si32	0.54329 (10)	0.32112 (13)	0.52464 (11)	0.0203 (8)
Si33	0.60230 (10)	0.26199 (14)	0.56801 (11)	0.0253 (9)
Si34	0.59034 (11)	0.16589 (14)	0.53065 (12)	0.0270 (9)
Si35	0.56963 (11)	0.10876 (15)	0.45833 (13)	0.0326 (10)
Si36	0.51176 (12)	0.11585 (15)	0.60418 (13)	0.0341 (10)
Na1	0.4253 (2)	0.7946 (3)	0.3443 (3)	0.057 (4)	0.82 (2)
Na2	0.0844 (2)	0.7166 (3)	0.3724 (2)	0.065 (2)
Na3	0.5606 (3)	0.0475 (3)	0.5539 (4)	0.084 (5)	0.86 (3)
Na4	0.0616 (2)	0.9434 (3)	0.3873 (3)	0.059 (3)	0.91 (2)
Na5	0.3750 (2)	0.4260 (3)	0.3930 (3)	0.075 (4)	0.90 (3)
Na6	0.4605 (3)	0.5536 (4)	0.5058 (3)	0.072 (4)	0.84 (3)
Na7	0.3229 (5)	0.8768 (10)	0.4955 (6)	0.141 (13)	0.57 (3)
Na8	0.3411 (3)	0.9747 (4)	0.4266 (3)	0.088 (5)	0.91 (3)
Na9	0.2246 (5)	0.5999 (8)	0.1417 (5)	0.177 (12)	0.81 (3)
Na10	0.35283 (17)	0.3272 (2)	0.33565 (18)	0.0468 (16)
Na11	0.3086 (4)	0.2362 (4)	0.2831 (3)	0.095 (6)	0.80 (3)
Na12	0.0128 (4)	0.9098 (9)	0.2834 (4)	0.149 (12)	0.69 (3)
Na13	0.4477 (8)	0.0101 (11)	0.5738 (9)	0.050*	0.226 (14)
Na14	0.2971 (4)	0.9593 (5)	0.5245 (4)	0.078 (6)	0.62 (3)
Na15	0.3743 (7)	0.7204 (8)	0.2777 (7)	0.050*	0.285 (14)
K1	0.0223 (7)	0.7352 (13)	0.2750 (7)	0.082 (11)*	0.22 (2)
K2	0.2967 (3)	0.6363 (4)	0.0491 (3)	0.112 (5)	0.588 (17)
K3	0.2438 (6)	0.4800 (8)	0.3626 (7)	0.102 (10)*	0.290 (17)
OB1	0.3280 (4)	0.1283 (5)	0.5251 (3)	0.071 (4)
OB2	0.5875 (2)	0.3041 (3)	0.5358 (3)	0.024 (2)
OB3	0.5330 (2)	0.3599 (3)	0.5590 (3)	0.028 (2)
OB4	0.4727 (2)	0.4050 (3)	0.5239 (3)	0.026 (2)
OB5	0.3815 (3)	0.4139 (3)	0.3047 (3)	0.028 (2)
OB6	0.6136 (2)	0.2154 (3)	0.5412 (3)	0.033 (2)
OB7	0.3037 (3)	0.8217 (4)	0.3919 (3)	0.039 (3)
OB8	0.4100 (3)	0.3297 (3)	0.3027 (3)	0.034 (2)
OB9	0.3928 (3)	0.5300 (3)	0.1283 (3)	0.030 (2)
OB10	0.3455 (3)	0.8927 (4)	0.3697 (3)	0.038 (3)
OB11	0.3736 (3)	0.5411 (4)	0.2013 (3)	0.038 (3)
OB12	0.2516 (3)	0.7593 (4)	0.3645 (3)	0.034 (2)
OB13	0.1762 (3)	0.6570 (3)	0.3241 (3)	0.044 (3)
OB14	0.4208 (3)	0.2895 (3)	0.6145 (3)	0.030 (2)
OB15	0.2421 (3)	0.5640 (4)	0.2268 (3)	0.045 (3)
OB16	0.2349 (4)	0.3269 (5)	0.3531 (3)	0.070 (4)
OB17	0.2711 (3)	0.2802 (5)	0.4830 (4)	0.065 (4)
OB18	0.3896 (3)	0.3746 (3)	0.6221 (3)	0.042 (3)
OB19	0.3124 (3)	0.0767 (4)	0.4594 (3)	0.049 (3)
OB20	0.3810 (3)	0.0996 (3)	0.4843 (3)	0.042 (3)
OB21	0.4138 (3)	0.1060 (4)	0.4186 (3)	0.039 (3)
OB22	0.5959 (3)	0.1507 (3)	0.4839 (3)	0.028 (2)
OB23	0.5499 (3)	0.1364 (4)	0.4173 (3)	0.036 (2)
OB24	0.4795 (3)	0.1192 (3)	0.3920 (3)	0.036 (2)
OB25	0.4188 (3)	0.1640 (3)	0.3561 (3)	0.038 (3)
OB26	0.2461 (3)	0.8034 (4)	0.4333 (3)	0.037 (3)
OB27	0.3938 (2)	0.2458 (3)	0.3269 (3)	0.028 (2)
OB28	0.1971 (3)	0.8487 (4)	0.4730 (3)	0.036 (2)
OB29	0.1444 (3)	0.4438 (4)	0.1949 (3)	0.042 (3)
OB30	0.3701 (3)	0.4985 (3)	0.2714 (3)	0.031 (2)
OB31	0.4671 (3)	0.3473 (3)	0.5853 (3)	0.030 (2)
OB32	0.3149 (3)	0.5569 (4)	0.2406 (3)	0.040 (3)
OB33	0.1809 (3)	0.3864 (5)	0.3275 (4)	0.063 (4)
OB34	0.1809 (3)	0.5155 (4)	0.2338 (4)	0.051 (3)
OB35	0.1470 (3)	0.4489 (6)	0.2752 (4)	0.074 (4)
OB36	0.2023 (3)	0.5856 (4)	0.2844 (3)	0.060 (3)
OB37	0.4325 (2)	0.4271 (3)	0.4562 (3)	0.025 (2)
OB38	0.2097 (3)	0.7337 (3)	0.2983 (3)	0.030 (2)
OS1	0.5161 (2)	0.2744 (3)	0.5247 (2)	0.022 (2)
OS2	0.2003 (2)	0.8210 (3)	0.3294 (3)	0.026 (2)
OS3	0.0522 (2)	0.8565 (3)	0.4047 (3)	0.025 (2)
OS4	0.2625 (2)	0.7995 (3)	0.2947 (3)	0.027 (2)
OS5	0.0339 (2)	0.7878 (3)	0.3496 (3)	0.024 (2)
OS6	0.4978 (2)	0.4178 (3)	0.4301 (3)	0.024 (2)
OS7	0.3641 (2)	0.3180 (4)	0.5619 (3)	0.034 (2)
OS8	0.5418 (2)	0.3484 (3)	0.4818 (2)	0.025 (2)
OS9	0.4043 (2)	0.3662 (3)	0.5038 (3)	0.026 (2)
OS10	0.4008 (2)	0.4569 (3)	0.1778 (3)	0.026 (2)
OS11	0.2938 (3)	0.9116 (4)	0.4165 (3)	0.037 (3)
OS12	0.1510 (3)	0.7438 (3)	0.3378 (3)	0.032 (2)
OS13	0.2152 (3)	0.3367 (4)	0.2729 (3)	0.036 (2)
OS14	0.4639 (3)	0.2643 (3)	0.3191 (3)	0.027 (2)
OS15	0.2809 (3)	0.5558 (3)	0.1649 (3)	0.035 (2)
OS16	0.2510 (3)	0.4085 (4)	0.3134 (3)	0.038 (3)
OS17	0.3123 (2)	0.4462 (3)	0.2890 (3)	0.029 (2)
OS18	0.2471 (3)	0.9163 (4)	0.4844 (3)	0.050 (3)
OS19	0.2423 (3)	0.5024 (4)	0.2859 (3)	0.041 (3)
OS20	0.3285 (3)	0.5715 (4)	0.1013 (3)	0.045 (3)
OS21	0.2472 (3)	0.0649 (4)	0.4130 (3)	0.043 (3)
OS22	0.3333 (3)	0.3306 (4)	0.4853 (3)	0.040 (3)
OS23	0.2819 (3)	−0.0073 (4)	0.4565 (3)	0.047 (3)
OS24	0.3335 (3)	0.1674 (4)	0.4537 (3)	0.038 (3)
OS25	0.4546 (3)	0.1080 (3)	0.4900 (3)	0.030 (2)
OS26	0.5044 (3)	0.1001 (3)	0.5569 (3)	0.038 (3)
OS27	0.3503 (2)	0.4201 (3)	0.2270 (2)	0.022 (2)
OS28	0.5667 (3)	0.2458 (3)	0.5910 (3)	0.025 (2)
OS29	0.1041 (2)	0.8058 (3)	0.3739 (3)	0.025 (2)
OS30	0.0657 (2)	0.8713 (3)	0.3294 (2)	0.021 (2)
OS31	0.4967 (2)	0.1765 (3)	0.4548 (2)	0.022 (2)
OS32	0.5203 (3)	0.1725 (3)	0.6085 (3)	0.030 (2)
OS33	0.1741 (2)	0.8114 (3)	0.4040 (3)	0.026 (2)
OS34	0.5361 (3)	0.0963 (3)	0.4858 (3)	0.035 (2)
OS35	0.2742 (2)	0.8857 (4)	0.3370 (3)	0.032 (2)
OS36	0.2185 (3)	0.8891 (3)	0.4055 (3)	0.031 (2)
OS37	0.5101 (2)	0.2035 (3)	0.3793 (3)	0.025 (2)
OS38	0.3712 (2)	0.2155 (3)	0.3946 (3)	0.029 (2)
OS39	0.3199 (3)	0.2613 (4)	0.4323 (3)	0.038 (3)
OS40	0.3328 (3)	0.8535 (4)	0.2967 (3)	0.039 (3)
OS41	0.4640 (2)	0.3404 (3)	0.4656 (2)	0.020 (2)
OS42	0.4248 (2)	0.3957 (3)	0.2480 (2)	0.022 (2)
OS43	0.4847 (3)	0.2561 (3)	0.5960 (3)	0.024 (2)
OS44	0.5466 (2)	0.1769 (3)	0.5322 (3)	0.026 (2)
OS45	0.2744 (3)	0.4796 (4)	0.2165 (3)	0.033 (2)
OS46	0.3315 (2)	0.4855 (3)	0.1489 (3)	0.027 (2)
OS47	0.4106 (2)	0.1849 (3)	0.4656 (3)	0.028 (2)
OS48	0.4309 (2)	0.2820 (3)	0.5366 (3)	0.023 (2)
OS49	0.4428 (2)	0.2436 (3)	0.3952 (3)	0.025 (2)
OT1	0.5076 (2)	0.2811 (3)	0.4290 (3)	0.022 (2)
OT2	0.3950 (2)	0.2790 (3)	0.4609 (3)	0.021 (2)
OT3	0.2689 (2)	0.3870 (3)	0.2346 (3)	0.022 (2)
OT4	0.2417 (3)	−0.0272 (4)	0.3763 (3)	0.033 (2)
OT5	0.4794 (2)	0.1925 (3)	0.5307 (3)	0.023 (2)
OT6	0.1461 (2)	0.8807 (3)	0.3460 (2)	0.021 (2)
OT7	0.2081 (3)	0.4269 (4)	0.2397 (3)	0.035 (2)
OHT1	0.3594 (3)	0.2389 (3)	0.5091 (3)	0.027 (2)
OHT2	0.4754 (2)	0.3363 (3)	0.3805 (3)	0.024 (2)
OHT3	0.1230 (2)	0.8238 (3)	0.2936 (3)	0.025 (2)
OHT4	0.2054 (3)	−0.0137 (4)	0.4340 (3)	0.036 (2)
OH1	0.1716 (7)	0.4775 (8)	0.3493 (7)	0.080 (7)*	0.633 (15)
OH2	0.2487 (4)	0.0676 (6)	0.4934 (5)	0.085 (4)*
OH3	0.6381 (3)	0.2804 (3)	0.5954 (3)	0.033 (2)*
OH4	0.4397 (3)	0.4570 (4)	0.3827 (3)	0.037 (2)*
OH5	0.4717 (3)	0.5043 (4)	0.4466 (3)	0.038 (3)*
OH6	0.4037 (3)	0.8735 (4)	0.3295 (3)	0.045 (3)*
OH7	0.2979 (3)	0.7383 (4)	0.4284 (3)	0.043 (3)*
OH8	0.3814 (3)	0.5910 (4)	0.2691 (3)	0.051 (3)*
OH9	0.5442 (3)	0.0842 (4)	0.6269 (4)	0.056 (3)*
OH10	0.2494 (5)	0.8414 (7)	0.5368 (6)	0.110 (6)*
OH11	0.1945 (5)	0.9067 (6)	0.5361 (5)	0.099 (5)*
OH12	0.2812 (3)	0.3417 (4)	0.4247 (4)	0.057 (3)*
OH13	0.3549 (3)	0.2961 (4)	0.6400 (3)	0.052 (3)*
OH14	0.1141 (8)	0.4200 (9)	0.3352 (8)	0.094 (8)*	0.633 (15)
OH15	0.4724 (3)	0.1058 (4)	0.6247 (4)	0.058 (3)*
OH16	0.5945 (3)	0.0655 (4)	0.4479 (3)	0.043 (3)*
OH17	0.4560 (3)	0.4022 (3)	0.3248 (3)	0.034 (2)*
OH18	0.4262 (3)	0.0701 (4)	0.3480 (3)	0.054 (3)*
OH19	0.4153 (3)	0.2569 (3)	0.2531 (3)	0.034 (2)*
OH20	0.5034 (3)	0.4305 (3)	0.5967 (3)	0.029 (2)*
OH21	0.3861 (3)	0.5668 (4)	0.0568 (3)	0.043 (3)*
OH22	0.1449 (3)	0.7074 (4)	0.2615 (3)	0.040 (3)*
OH23	0.2470 (13)	0.2012 (12)	0.4438 (11)	0.115 (15)*	0.419 (16)
OH24	0.2015 (6)	0.2786 (9)	0.4607 (9)	0.060 (9)*	0.419 (16)
OH25	0.2726 (5)	0.0943 (12)	0.5664 (10)	0.059 (9)*	0.365 (10)
OH26	0.2156 (10)	0.2570 (9)	0.3981 (10)	0.067 (10)*	0.365 (10)
OH27	0.3167 (12)	0.1624 (10)	0.5948 (11)	0.084 (13)*	0.365 (10)
OH28	0.1638 (8)	0.2793 (14)	0.3485 (11)	0.081 (12)*	0.365 (10)
OH29	0.1281 (9)	0.593 (2)	0.2876 (18)	0.10 (2)*	0.263 (18)
OH30	0.2218 (10)	0.5961 (17)	0.3650 (10)	0.146 (18)*	0.477 (18)
OH31	0.3494 (12)	0.0765 (17)	0.5816 (17)	0.13 (2)*	0.365 (10)
OH32	0.1758 (14)	0.5676 (14)	0.3522 (9)	0.050 (13)*	0.263 (18)
OH33	0.1551 (6)	0.5677 (9)	0.3378 (9)	0.063 (8)*	0.477 (18)
OH34	0.6053 (3)	0.1210 (4)	0.5601 (3)	0.044 (3)*
OW1	0.1674 (14)	0.6236 (17)	0.1386 (14)	0.14 (2)*	0.46 (5)
OW2	0.4437 (15)	0.7495 (17)	0.2963 (16)	0.15 (3)*	0.48 (5)
OW3	0.3441 (5)	0.4262 (6)	0.4567 (5)	0.080 (7)*	0.91 (4)
OW4	0.3399 (11)	0.9156 (14)	0.5758 (11)	0.15 (2)*	0.61 (5)
OW5	0.3572 (11)	0.5058 (13)	0.3821 (11)	0.18 (2)*	0.75 (6)
OW6	0.2859 (11)	0.1618 (14)	0.2948 (12)	0.080*	0.38 (3)
OW7	0.0648 (16)	0.690 (2)	0.3064 (17)	0.10 (3)*	0.30 (4)
OW8	0.2985 (18)	0.542 (2)	0.3459 (18)	0.09 (3)*	0.26 (4)
OW9	0.0084 (12)	0.8296 (13)	0.2633 (11)	0.080 (17)*	0.36 (4)
OW10	0.3952 (4)	0.9906 (5)	0.3910 (4)	0.080*
OW11	0.3952 (3)	0.3424 (3)	0.3943 (3)	0.033 (2)*
OW12	0.4392 (13)	0.8736 (16)	0.2620 (13)	0.13 (2)*	0.47 (5)
OW13	0.6613 (4)	0.2517 (5)	0.4870 (4)	0.066 (4)*
OW14	0.0774 (3)	0.7460 (4)	0.4440 (3)	0.038 (3)*
OW15	0.0160 (9)	0.9756 (11)	0.3388 (9)	0.129 (15)*	0.71 (5)
OW16	0.3188 (3)	0.3874 (4)	0.3651 (3)	0.055 (3)*
OW17	0.3049 (4)	0.2687 (4)	0.3479 (4)	0.059 (3)*
OW18	0.3850 (5)	0.9888 (6)	0.4834 (5)	0.105 (5)*
OW19	0.2518 (11)	0.6988 (14)	0.1533 (12)	0.061 (17)*	0.31 (4)
OW20	0.6064 (5)	0.4206 (7)	0.5092 (6)	0.096 (8)*	0.90 (4)
OW21	0.1490 (6)	0.6947 (8)	0.4112 (6)	0.101 (10)*	0.81 (4)
OW22	0.5200 (8)	−0.0140 (10)	0.5452 (8)	0.114 (14)*	0.67 (5)
OW23	0.2393 (6)	0.2385 (8)	0.2806 (6)	0.105 (10)*	0.84 (4)
OW24	0.0587 (4)	0.9952 (5)	0.4430 (4)	0.073 (6)*	0.93 (4)
OW25	0.0203 (5)	0.7669 (10)	0.2798 (6)	0.030 (9)*	0.50 (5)
OW26	0.3083 (4)	1.0137 (6)	0.3626 (5)	0.085 (4)*
OW27	0.3232 (3)	0.3197 (4)	0.2678 (3)	0.036 (2)*
OW28	0.6292 (3)	0.4195 (4)	0.4175 (3)	0.042 (3)*
OW29	0.3606 (5)	0.7629 (6)	0.3311 (5)	0.068 (8)*	0.76 (4)
OW30	0.3139 (16)	0.842 (2)	0.5463 (16)	0.080*	0.27 (3)
OW31	0.5457 (6)	0.8040 (7)	0.3642 (6)	0.052 (8)*	0.58 (4)
OW32	0.4297 (8)	0.5445 (10)	0.3432 (8)	0.080*	0.54 (3)
OW33	0.6370 (6)	0.2088 (8)	0.7632 (6)	0.124 (11)*	0.92 (5)
OW34	0.4134 (4)	0.1742 (5)	0.5653 (4)	0.056 (5)*	0.95 (4)
OW35	0.3045 (6)	0.3525 (8)	0.6708 (7)	0.110 (11)*	0.83 (5)
OW36	0.4267 (5)	0.0858 (6)	0.5604 (5)	0.077 (7)*	0.82 (4)
OW37	0.3696 (4)	0.0930 (5)	0.2939 (4)	0.080*
OW38	0.1623 (10)	−0.0151 (12)	0.4954 (10)	0.128 (16)*	0.61 (5)
OW39	0.4762 (11)	0.0029 (13)	0.3413 (11)	0.165 (19)*	0.71 (5)
OW40	0.2638 (12)	0.7502 (18)	0.4983 (15)	0.11 (2)*	0.42 (4)
Si37	0.1894 (3)	0.6018 (3)	0.3273 (3)	0.047 (4)*	0.477 (18)
Si38	0.1694 (4)	0.6007 (4)	0.3118 (5)	0.038 (7)*	0.263 (18)
Si39	0.2368 (3)	0.2436 (4)	0.4747 (4)	0.064 (5)*	0.419 (16)
Si40	0.1991 (4)	0.3049 (6)	0.3749 (5)	0.067 (5)*	0.365 (10)
Si41	0.3154 (4)	0.1139 (5)	0.5677 (4)	0.063 (5)*	0.365 (10)

Atomic displacement parameters (Ų)

	U^11	U^22	U^33	U^12	U^13	U^23
Ce1	0.0141 (5)	0.0300 (5)	0.0270 (5)	−0.0019 (3)	0.0014 (3)	−0.0042 (3)
Ce2	0.0159 (5)	0.0199 (5)	0.0258 (5)	−0.0015 (3)	−0.0012 (3)	0.0002 (3)
Ba	0.0187 (6)	0.0431 (7)	0.0313 (6)	−0.0027 (4)	0.0021 (4)	0.0038 (4)
Ti1	0.0139 (13)	0.0228 (14)	0.0212 (12)	−0.0002 (10)	0.0002 (10)	−0.0017 (10)
Ti2	0.0114 (13)	0.0267 (14)	0.0233 (13)	−0.0011 (10)	−0.0008 (10)	−0.0025 (10)
Ti3	0.0151 (13)	0.0413 (17)	0.0295 (14)	0.0030 (12)	0.0026 (11)	0.0001 (12)
Ti4	0.0283 (16)	0.0466 (18)	0.0346 (15)	−0.0128 (13)	−0.0023 (12)	−0.0096 (13)
Ti5	0.0182 (14)	0.0374 (16)	0.0284 (14)	0.0002 (11)	0.0051 (11)	−0.0018 (12)
Ti6	0.0234 (15)	0.0344 (16)	0.0397 (16)	−0.0063 (12)	0.0004 (12)	−0.0147 (12)
Ti7	0.0155 (13)	0.0233 (14)	0.0356 (14)	−0.0028 (11)	0.0018 (11)	−0.0011 (11)
Ti8	0.0148 (13)	0.0246 (14)	0.0209 (12)	−0.0005 (10)	−0.0031 (10)	−0.0007 (10)
Ti9	0.0162 (13)	0.0210 (13)	0.0210 (12)	−0.0034 (10)	0.0014 (10)	−0.0003 (10)
Ti10	0.0195 (13)	0.0168 (13)	0.0322 (14)	−0.0003 (10)	−0.0038 (11)	−0.0010 (11)
Ti11	0.0163 (13)	0.0203 (14)	0.0267 (13)	−0.0007 (10)	−0.0036 (10)	0.0030 (10)
Ti12	0.0177 (14)	0.0274 (15)	0.0393 (15)	−0.0079 (11)	−0.0019 (11)	0.0010 (12)
Si1	0.012 (2)	0.055 (3)	0.033 (2)	−0.0014 (19)	−0.0025 (17)	−0.003 (2)
Si2	0.014 (2)	0.060 (3)	0.042 (2)	−0.007 (2)	0.0004 (18)	0.001 (2)
Si3	0.063 (4)	0.074 (4)	0.044 (3)	−0.009 (3)	−0.001 (3)	−0.005 (3)
Si4	0.015 (2)	0.044 (3)	0.027 (2)	−0.0019 (18)	0.0012 (16)	−0.0023 (18)
Si5	0.019 (2)	0.055 (3)	0.033 (2)	0.007 (2)	−0.0041 (18)	0.000 (2)
Si6	0.017 (2)	0.032 (2)	0.030 (2)	0.0043 (17)	0.0022 (17)	−0.0032 (17)
Si7	0.0119 (19)	0.028 (2)	0.0237 (19)	0.0017 (16)	0.0020 (15)	0.0010 (16)
Si8	0.025 (2)	0.025 (2)	0.033 (2)	0.0060 (17)	−0.0013 (17)	−0.0018 (17)
Si9	0.020 (2)	0.031 (2)	0.025 (2)	0.0010 (17)	−0.0062 (16)	0.0018 (17)
Si10	0.020 (2)	0.060 (3)	0.048 (3)	0.007 (2)	0.006 (2)	−0.009 (2)
Si11	0.027 (2)	0.039 (3)	0.064 (3)	0.010 (2)	0.009 (2)	−0.008 (2)
Si12	0.026 (2)	0.030 (2)	0.042 (2)	0.0077 (18)	0.0066 (19)	0.0002 (19)
Si13	0.031 (2)	0.025 (2)	0.043 (2)	0.0013 (18)	0.0043 (19)	−0.0056 (19)
Si14	0.029 (2)	0.032 (2)	0.038 (2)	−0.0021 (18)	0.0088 (19)	0.0127 (19)
Si15	0.017 (2)	0.021 (2)	0.037 (2)	0.0008 (16)	0.0031 (17)	0.0083 (17)
Si16	0.020 (2)	0.026 (2)	0.0235 (19)	0.0011 (16)	0.0008 (16)	−0.0004 (16)
Si17	0.060 (6)	0.051 (5)	0.053 (5)	0.004 (4)	0.043 (4)	−0.006 (4)
Si18	0.040 (3)	0.061 (3)	0.037 (2)	−0.018 (2)	0.016 (2)	−0.008 (2)
Si19	0.020 (2)	0.028 (2)	0.0225 (19)	0.0014 (17)	−0.0025 (16)	−0.0002 (16)
Si20	0.024 (2)	0.046 (3)	0.049 (3)	−0.004 (2)	0.001 (2)	0.009 (2)
Si21	0.024 (2)	0.017 (2)	0.028 (2)	−0.0022 (16)	0.0006 (16)	0.0037 (16)
Si22	0.020 (2)	0.016 (2)	0.028 (2)	0.0007 (16)	0.0028 (16)	−0.0020 (15)
Si23	0.017 (2)	0.027 (2)	0.028 (2)	−0.0059 (16)	−0.0047 (16)	−0.0008 (17)
Si24	0.035 (2)	0.025 (2)	0.038 (2)	−0.0007 (19)	−0.0114 (19)	−0.0074 (18)
Si25	0.026 (2)	0.017 (2)	0.029 (2)	−0.0047 (16)	0.0048 (17)	−0.0023 (16)
Si26	0.025 (2)	0.022 (2)	0.029 (2)	0.0020 (17)	−0.0031 (17)	−0.0010 (16)
Si27	0.016 (2)	0.019 (2)	0.028 (2)	−0.0026 (15)	0.0030 (16)	0.0013 (16)
Si28	0.024 (2)	0.023 (2)	0.037 (2)	−0.0088 (17)	−0.0047 (18)	0.0018 (17)
Si29	0.025 (2)	0.032 (2)	0.037 (2)	0.0026 (18)	0.0122 (18)	0.0014 (18)
Si30	0.025 (2)	0.045 (3)	0.037 (2)	−0.019 (2)	−0.0016 (18)	0.000 (2)
Si31	0.041 (3)	0.058 (3)	0.044 (3)	−0.027 (2)	0.008 (2)	−0.015 (2)
Si32	0.0126 (19)	0.024 (2)	0.0231 (19)	−0.0008 (15)	−0.0012 (15)	0.0009 (16)
Si33	0.013 (2)	0.031 (2)	0.031 (2)	−0.0004 (16)	−0.0054 (16)	0.0033 (17)
Si34	0.017 (2)	0.027 (2)	0.035 (2)	0.0034 (17)	−0.0034 (17)	0.0031 (17)
Si35	0.027 (2)	0.029 (2)	0.040 (2)	0.0092 (18)	−0.0023 (19)	−0.0018 (19)
Si36	0.035 (2)	0.027 (2)	0.038 (2)	−0.0043 (19)	−0.0085 (19)	0.0120 (18)
Na1	0.037 (5)	0.063 (7)	0.067 (6)	−0.006 (4)	−0.009 (4)	0.025 (4)
Na2	0.064 (5)	0.072 (5)	0.058 (4)	−0.009 (4)	0.006 (4)	−0.003 (4)
Na3	0.064 (7)	0.050 (6)	0.137 (10)	0.009 (5)	0.018 (6)	0.021 (6)
Na4	0.045 (5)	0.045 (5)	0.089 (7)	0.002 (4)	0.012 (4)	−0.011 (4)
Na5	0.039 (5)	0.049 (6)	0.135 (9)	−0.004 (4)	0.002 (5)	−0.010 (5)
Na6	0.072 (7)	0.087 (8)	0.062 (6)	−0.024 (5)	0.024 (5)	−0.024 (5)
Na7	0.068 (13)	0.24 (3)	0.118 (17)	0.048 (14)	0.018 (11)	0.017 (16)
Na8	0.062 (7)	0.126 (10)	0.074 (7)	−0.038 (6)	−0.006 (5)	0.005 (6)
Na9	0.156 (17)	0.25 (2)	0.127 (13)	0.165 (17)	0.007 (11)	0.003 (12)
Na10	0.029 (3)	0.073 (5)	0.037 (3)	−0.007 (3)	−0.003 (3)	−0.004 (3)
Na11	0.162 (13)	0.066 (8)	0.072 (8)	−0.051 (7)	0.072 (8)	−0.023 (5)
Na12	0.041 (9)	0.33 (3)	0.077 (11)	−0.032 (11)	0.011 (7)	0.013 (13)
Na14	0.073 (10)	0.105 (12)	0.052 (8)	−0.003 (8)	−0.011 (6)	−0.003 (7)
K2	0.072 (7)	0.130 (10)	0.129 (9)	−0.038 (6)	−0.005 (6)	0.069 (7)
OB1	0.071 (9)	0.104 (11)	0.038 (7)	−0.019 (8)	0.011 (6)	−0.007 (7)
OB2	0.015 (5)	0.021 (5)	0.034 (5)	0.000 (4)	−0.001 (4)	0.004 (4)
OB3	0.025 (5)	0.027 (5)	0.031 (5)	−0.003 (4)	0.004 (4)	−0.004 (4)
OB4	0.017 (5)	0.027 (5)	0.033 (5)	−0.003 (4)	0.003 (4)	−0.007 (4)
OB5	0.022 (5)	0.036 (6)	0.029 (5)	0.009 (4)	0.005 (4)	0.003 (4)
OB6	0.016 (5)	0.036 (6)	0.045 (6)	−0.003 (4)	−0.001 (4)	−0.006 (5)
OB7	0.023 (6)	0.051 (7)	0.043 (6)	0.004 (5)	0.002 (5)	0.003 (5)
OB8	0.031 (6)	0.032 (6)	0.037 (6)	−0.006 (5)	−0.004 (5)	0.005 (5)
OB9	0.020 (5)	0.028 (6)	0.041 (6)	0.003 (4)	0.002 (4)	0.009 (4)
OB10	0.016 (5)	0.055 (7)	0.042 (6)	−0.015 (5)	0.001 (4)	−0.010 (5)
OB11	0.037 (6)	0.034 (6)	0.043 (6)	0.002 (5)	0.008 (5)	0.006 (5)
OB12	0.030 (6)	0.039 (6)	0.033 (5)	0.013 (5)	0.004 (5)	0.008 (5)
OB13	0.055 (7)	0.023 (6)	0.053 (7)	0.009 (5)	0.008 (6)	0.006 (5)
OB14	0.026 (5)	0.030 (6)	0.036 (5)	0.005 (4)	0.010 (4)	0.002 (4)
OB15	0.025 (6)	0.059 (8)	0.053 (7)	0.018 (5)	0.007 (5)	−0.005 (6)
OB16	0.093 (11)	0.084 (10)	0.035 (7)	−0.024 (8)	0.012 (7)	0.019 (6)
OB17	0.056 (8)	0.088 (10)	0.054 (7)	−0.025 (7)	0.018 (6)	0.010 (7)
OB18	0.055 (7)	0.022 (6)	0.049 (6)	0.009 (5)	0.008 (5)	−0.010 (5)
OB19	0.039 (7)	0.036 (7)	0.066 (8)	−0.024 (5)	−0.015 (6)	−0.001 (5)
OB20	0.024 (6)	0.021 (6)	0.078 (8)	−0.011 (4)	−0.014 (5)	0.002 (5)
OB21	0.041 (7)	0.032 (6)	0.040 (6)	−0.003 (5)	−0.009 (5)	−0.002 (5)
OB22	0.023 (5)	0.027 (5)	0.035 (5)	−0.001 (4)	0.004 (4)	0.001 (4)
OB23	0.031 (6)	0.040 (6)	0.036 (6)	0.019 (5)	0.002 (5)	−0.004 (5)
OB24	0.039 (6)	0.025 (6)	0.042 (6)	0.004 (5)	−0.009 (5)	−0.013 (5)
OB25	0.048 (7)	0.029 (6)	0.035 (6)	−0.006 (5)	−0.009 (5)	0.003 (5)
OB26	0.015 (5)	0.057 (7)	0.037 (6)	0.006 (5)	−0.002 (4)	−0.002 (5)
OB27	0.017 (5)	0.031 (6)	0.034 (5)	−0.006 (4)	−0.007 (4)	0.003 (4)
OB28	0.023 (6)	0.054 (7)	0.031 (5)	0.003 (5)	0.000 (4)	−0.004 (5)
OB29	0.018 (6)	0.051 (7)	0.057 (7)	0.008 (5)	0.001 (5)	−0.004 (5)
OB30	0.033 (6)	0.023 (5)	0.037 (6)	0.000 (4)	0.002 (5)	0.002 (4)
OB31	0.029 (6)	0.021 (5)	0.043 (6)	−0.007 (4)	0.016 (5)	−0.003 (4)
OB32	0.038 (6)	0.031 (6)	0.051 (6)	0.010 (5)	0.007 (5)	−0.001 (5)
OB33	0.043 (7)	0.085 (10)	0.067 (8)	−0.020 (7)	0.033 (6)	−0.035 (7)
OB34	0.028 (6)	0.049 (7)	0.072 (8)	0.020 (5)	−0.013 (6)	−0.010 (6)
OB35	0.032 (7)	0.124 (13)	0.070 (9)	0.015 (7)	0.021 (6)	−0.002 (8)
OB36	0.044 (7)	0.053 (8)	0.088 (9)	0.012 (6)	0.031 (7)	−0.020 (7)
OB37	0.014 (5)	0.022 (5)	0.041 (6)	0.004 (4)	0.004 (4)	0.004 (4)
OB38	0.024 (5)	0.027 (6)	0.040 (6)	0.000 (4)	0.002 (4)	−0.005 (4)
OS1	0.018 (5)	0.023 (5)	0.024 (5)	−0.011 (4)	0.001 (4)	0.002 (4)
OS2	0.016 (5)	0.030 (6)	0.031 (5)	0.006 (4)	0.004 (4)	−0.006 (4)
OS3	0.023 (5)	0.028 (5)	0.023 (5)	−0.008 (4)	0.003 (4)	−0.004 (4)
OS4	0.018 (5)	0.026 (5)	0.039 (6)	0.000 (4)	0.011 (4)	−0.003 (4)
OS5	0.014 (5)	0.032 (6)	0.024 (5)	−0.001 (4)	−0.003 (4)	−0.005 (4)
OS6	0.018 (5)	0.021 (5)	0.034 (5)	−0.006 (4)	0.000 (4)	0.005 (4)
OS7	0.012 (5)	0.041 (6)	0.049 (6)	−0.001 (4)	0.003 (4)	−0.003 (5)
OS8	0.019 (5)	0.035 (6)	0.020 (5)	−0.012 (4)	−0.002 (4)	0.000 (4)
OS9	0.013 (5)	0.026 (5)	0.039 (5)	0.001 (4)	0.004 (4)	−0.001 (4)
OS10	0.020 (5)	0.020 (5)	0.037 (5)	0.005 (4)	0.002 (4)	0.008 (4)
OS11	0.022 (6)	0.050 (7)	0.036 (6)	0.001 (5)	−0.002 (4)	−0.016 (5)
OS12	0.024 (5)	0.036 (6)	0.035 (6)	0.001 (4)	0.004 (4)	−0.006 (4)
OS13	0.029 (6)	0.047 (7)	0.032 (5)	−0.015 (5)	0.007 (4)	0.005 (5)
OS14	0.028 (6)	0.029 (6)	0.022 (5)	0.000 (4)	−0.007 (4)	0.002 (4)
OS15	0.029 (6)	0.026 (6)	0.050 (6)	0.009 (4)	0.005 (5)	0.013 (5)
OS16	0.027 (6)	0.057 (7)	0.030 (5)	−0.010 (5)	0.009 (4)	−0.001 (5)
OS17	0.020 (5)	0.042 (6)	0.027 (5)	0.001 (4)	0.008 (4)	−0.010 (4)
OS18	0.049 (7)	0.071 (8)	0.028 (6)	−0.032 (6)	−0.003 (5)	−0.012 (5)
OS19	0.041 (6)	0.039 (6)	0.046 (6)	0.004 (5)	0.017 (5)	−0.006 (5)
OS20	0.026 (6)	0.045 (7)	0.065 (7)	0.011 (5)	0.008 (5)	0.025 (6)
OS21	0.030 (6)	0.047 (7)	0.050 (6)	−0.015 (5)	0.002 (5)	−0.025 (5)
OS22	0.019 (5)	0.034 (6)	0.065 (7)	0.004 (5)	−0.006 (5)	0.010 (5)
OS23	0.047 (7)	0.044 (7)	0.050 (7)	−0.017 (5)	0.001 (5)	−0.010 (5)
OS24	0.023 (6)	0.036 (6)	0.051 (6)	−0.017 (5)	−0.005 (5)	0.004 (5)
OS25	0.027 (6)	0.021 (5)	0.042 (6)	0.002 (4)	−0.007 (4)	0.007 (4)
OS26	0.039 (6)	0.025 (6)	0.047 (6)	−0.003 (5)	−0.002 (5)	0.007 (5)
OS27	0.018 (5)	0.027 (5)	0.022 (5)	0.002 (4)	0.002 (4)	0.003 (4)
OS28	0.025 (5)	0.023 (5)	0.027 (5)	−0.004 (4)	0.000 (4)	0.003 (4)
OS29	0.015 (5)	0.033 (6)	0.025 (5)	0.002 (4)	0.000 (4)	0.010 (4)
OS30	0.013 (5)	0.026 (5)	0.025 (5)	0.001 (4)	0.008 (4)	0.007 (4)
OS31	0.023 (5)	0.016 (5)	0.024 (5)	−0.001 (4)	−0.004 (4)	−0.002 (4)
OS32	0.028 (6)	0.025 (5)	0.034 (5)	0.000 (4)	−0.008 (4)	0.001 (4)
OS33	0.024 (5)	0.031 (6)	0.022 (5)	−0.008 (4)	−0.005 (4)	0.001 (4)
OS34	0.025 (6)	0.015 (5)	0.061 (7)	0.011 (4)	−0.009 (5)	−0.007 (5)
OS35	0.015 (5)	0.049 (7)	0.031 (5)	0.001 (4)	−0.002 (4)	−0.010 (5)
OS36	0.023 (5)	0.038 (6)	0.033 (5)	−0.005 (4)	0.001 (4)	−0.006 (4)
OS37	0.026 (5)	0.024 (5)	0.026 (5)	0.003 (4)	0.001 (4)	−0.006 (4)
OS38	0.020 (5)	0.035 (6)	0.029 (5)	−0.007 (4)	−0.007 (4)	−0.002 (4)
OS39	0.015 (5)	0.048 (7)	0.050 (6)	−0.009 (5)	−0.005 (5)	0.005 (5)
OS40	0.022 (6)	0.058 (7)	0.038 (6)	0.006 (5)	0.005 (5)	0.011 (5)
OS41	0.018 (5)	0.020 (5)	0.024 (5)	0.004 (4)	0.009 (4)	0.002 (4)
OS42	0.008 (5)	0.034 (6)	0.024 (5)	0.000 (4)	0.001 (4)	0.003 (4)
OS43	0.026 (5)	0.022 (5)	0.024 (5)	−0.008 (4)	−0.001 (4)	−0.006 (4)
OS44	0.016 (5)	0.029 (6)	0.031 (5)	0.002 (4)	−0.008 (4)	−0.003 (4)
OS45	0.029 (6)	0.041 (6)	0.030 (5)	0.005 (5)	0.005 (4)	0.006 (5)
OS46	0.016 (5)	0.028 (6)	0.037 (5)	0.005 (4)	0.004 (4)	0.011 (4)
OS47	0.017 (5)	0.025 (5)	0.041 (6)	−0.004 (4)	−0.002 (4)	0.004 (4)
OS48	0.016 (5)	0.027 (5)	0.027 (5)	−0.003 (4)	0.004 (4)	−0.001 (4)
OS49	0.019 (5)	0.028 (5)	0.029 (5)	−0.003 (4)	0.004 (4)	−0.001 (4)
OT1	0.020 (5)	0.017 (5)	0.030 (5)	0.001 (4)	0.004 (4)	0.000 (4)
OT2	0.009 (4)	0.026 (5)	0.028 (5)	−0.006 (4)	−0.001 (4)	0.005 (4)
OT3	0.013 (5)	0.025 (5)	0.029 (5)	0.000 (4)	0.006 (4)	0.000 (4)
OT4	0.020 (5)	0.043 (6)	0.037 (6)	0.003 (5)	0.001 (4)	0.000 (5)
OT5	0.019 (5)	0.016 (5)	0.032 (5)	−0.004 (4)	0.000 (4)	0.003 (4)
OT6	0.017 (5)	0.022 (5)	0.023 (5)	0.000 (4)	0.000 (4)	0.000 (4)
OT7	0.018 (5)	0.051 (7)	0.036 (6)	−0.001 (5)	0.004 (4)	0.000 (5)
OHT1	0.024 (5)	0.022 (5)	0.032 (5)	−0.003 (4)	−0.002 (4)	0.001 (4)
OHT2	0.014 (5)	0.033 (6)	0.024 (5)	−0.001 (4)	0.001 (4)	0.001 (4)
OHT3	0.019 (5)	0.025 (5)	0.030 (5)	−0.001 (4)	0.002 (4)	−0.002 (4)
OHT4	0.020 (5)	0.054 (7)	0.034 (6)	−0.003 (5)	−0.002 (4)	−0.013 (5)

Geometric parameters (Å, º)

<

Ce1—OT6	2.482 (8)	OB28—Ba^ix	2.906 (10)
Ce1—OT4^i	2.488 (10)	OB28—OW13^ix	3.044 (17)
Ce1—OT3^ii	2.508 (8)	OB28—OW40^viii	3.18 (5)
Ce1—OS45^ii	2.524 (10)	OB28—OW28^ix	3.489 (14)
Ce1—OS35	2.530 (9)	OB29—Si2^iv	1.650 (12)
Ce1—OS46^ii	2.561 (9)	OB29—OB10^iv	2.626 (15)
Ce1—OS36	2.590 (9)	OB29—OT7	2.627 (14)
Ce1—OS2	2.593 (9)	OB29—OB34	2.640 (15)
Ce1—OS27^ii	2.627 (8)	OB29—OS40^iv	2.645 (15)
Ce1—Ti5^ii	3.576 (2)	OB29—OB35	2.655 (17)
Ce1—Ti6^i	3.589 (3)	OB29—OH6^iv	2.670 (15)
Ce1—Ti3	3.592 (3)	OB29—OW10^iv	3.300 (18)
Ce2—OT2	2.484 (8)	OB29—OW26^iv	3.319 (19)
Ce2—OT1	2.504 (8)	OB29—OS35^iv	3.601 (13)
Ce2—OT5	2.518 (8)	OB29—Ti3^iv	3.620 (10)
Ce2—OS41	2.520 (8)	OB30—OH8	2.603 (15)
Ce2—OS31	2.532 (8)	OB30—OS17	2.652 (13)
Ce2—OS1	2.552 (8)	OB30—OB32	2.671 (14)
Ce2—OS47	2.553 (9)	OB30—OS27	2.680 (13)
Ce2—OS49	2.604 (9)	OB30—OW32	3.27 (3)
Ce2—OS48	2.611 (8)	OB30—OS10	3.600 (13)
Ce2—Ti12	3.566 (3)	OB30—OS42	3.601 (12)
Ce2—Ti9	3.578 (2)	OB31—OS43	2.623 (13)
Ce2—Ti7	3.590 (2)	OB31—OH20	2.660 (13)
Ba—OW14^iii	2.818 (10)	OB31—OS48	2.666 (12)
Ba—OW28	2.826 (10)	OB31—OS9	3.359 (13)
Ba—OS3^iii	2.841 (9)	OB32—OH8	2.642 (16)
Ba—OW13	2.870 (13)	OB32—OS15	2.663 (14)
Ba—OS8	2.902 (9)	OB32—OS45	2.665 (14)
Ba—OB28^iii	2.906 (10)	OB32—OW35^x	3.41 (2)
Ba—OS29^iii	2.906 (9)	OB32—OS17	3.475 (14)
Ba—OB2	2.967 (9)	OB32—OS19	3.497 (14)
Ba—OS33^iii	2.970 (9)	OB33—OH14	2.61 (3)
Ba—OW20	2.986 (18)	OB33—OB35	2.65 (2)
Ba—Si7^iii	3.516 (4)	OB33—OH1	2.66 (3)
Ba—Si4^iii	3.602 (4)	OB33—OS16	2.679 (14)
Ti1—OS10^ii	1.907 (9)	OB33—OS13	2.683 (14)
Ti1—OS42^ii	1.919 (8)	OB33—Si40	2.79 (2)
Ti1—OT6	1.924 (8)	OB33—OH27^xii	2.90 (4)
Ti1—OS30	1.929 (8)	OB33—OH28	3.13 (4)
Ti1—OS27^ii	2.037 (9)	OB33—OT7	3.363 (15)
Ti1—OHT3	2.055 (9)	OB34—OB36	2.627 (16)
Ti1—Ti2	3.058 (3)	OB34—OT7	2.647 (15)
Ti1—Na12	3.410 (14)	OB34—OS19	2.668 (15)
Ti1—OS29	3.414 (9)	OB34—OB35	2.677 (19)
Ti1—OS46^ii	3.621 (9)	OB34—OW37^ii	2.895 (18)
Ti1—OB5^ii	3.660 (9)	OB34—OW26^iv	3.262 (19)
Ti2—OT6	1.906 (9)	OB34—OH29	3.48 (7)
Ti2—OS33	1.907 (9)	OB34—Si38	3.561 (16)
Ti2—OS29	1.911 (9)	OB35—OH14	2.56 (3)
Ti2—OS12	1.948 (10)	OB35—OH1	2.64 (3)
Ti2—OHT3	2.020 (9)	OB35—OT7	2.674 (14)
Ti2—OS2	2.023 (9)	OB35—OS40^iv	3.688 (17)
Ti2—OS30	3.431 (9)	OB35—OS19	3.711 (17)
Ti2—OS36	3.609 (9)	OB35—OW12^iv	3.82 (5)
Ti2—OB38	3.627 (9)	OB35—OH33	3.89 (3)
Ti2—Na2	3.680 (8)	OB36—Si37	1.606 (9)
Ti3—OS4	1.854 (9)	OB36—Si38	1.622 (9)
Ti3—OS13^ii	1.889 (9)	OB36—OH32	2.59 (3)
Ti3—OS40	1.922 (10)	OB36—OH33	2.63 (2)
Ti3—OT3^ii	1.928 (9)	OB36—OH29	2.69 (4)
Ti3—OS35	2.056 (9)	OB36—OH30	2.70 (3)
Ti3—OT7^ii	2.058 (10)	OB36—OS19	2.720 (15)
Ti3—Ti5^ii	3.094 (4)	OB36—OW6^ii	3.43 (4)
Ti3—OS16^ii	3.457 (10)	OB37—OS9	2.595 (12)
Ti3—OS2	3.607 (9)	OB37—OS6	2.601 (12)
Ti3—OB29^ii	3.620 (10)	OB37—OH5	2.604 (13)
Ti3—OB10	3.692 (10)	OB37—OH4	2.614 (13)
Ti4—OHT4^i	1.933 (10)	OB37—OS41	2.665 (12)
Ti4—OS23^i	1.941 (10)	OB37—OW3	3.177 (19)
Ti4—OT4^i	1.950 (10)	OB37—OW11	3.305 (13)
Ti4—OS18	1.951 (11)	OB38—OH22	2.606 (14)
Ti4—OS11	1.983 (10)	OB38—OS12	2.620 (13)
Ti4—OS36	1.997 (9)	OB38—OS4	2.646 (13)
Ti4—Ti6^i	2.948 (4)	OB38—OS2	2.672 (13)
Ti4—OS21^i	3.395 (11)	OB38—Na11^ii	2.702 (15)
Ti4—Na14	3.422 (12)	OB38—OW23^ii	3.36 (2)
Ti4—Na8	3.461 (9)	OB38—OW27^ii	3.365 (14)
Ti4—OB28	3.605 (11)	OS1—OT5	2.648 (11)
Ti5—OS17	1.851 (9)	OS1—OS8	2.718 (12)
Ti5—OT3	1.897 (9)	OS1—OS43	2.779 (12)
Ti5—OS16	1.908 (10)	OS1—OS28	2.803 (12)
Ti5—OS19	1.956 (10)	OS1—OS44	2.921 (12)
Ti5—OS45	2.033 (9)	OS1—OS48	3.136 (12)
Ti5—OT7	2.104 (10)	OS1—OS41	3.141 (12)
Ti5—Ti3^iv	3.094 (4)	OS2—OT6	2.664 (12)
Ti5—OS13	3.418 (10)	OS2—OS4	2.693 (12)
Ti5—K3	3.49 (2)	OS2—OS33	2.754 (12)
Ti5—Ce1^iv	3.576 (2)	OS2—OS12	2.816 (13)
Ti5—OS27	3.592 (9)	OS2—OHT3	2.892 (12)
Ti5—OB34	3.634 (10)	OS2—OT3^ii	3.099 (12)
Ti6—OT4	1.916 (10)	OS2—OS36	3.162 (12)
Ti6—OS21	1.926 (10)	OS3—Ti9^ix	1.924 (9)
Ti6—OHT4	1.934 (11)	OS3—OS30	2.626 (11)
Ti6—OS20^iv	1.942 (11)	OS3—OS8^ix	2.634 (12)
Ti6—OS15^iv	1.964 (10)	OS3—OS29	2.634 (13)
Ti6—OS46^iv	2.050 (9)	OS3—OS5	2.672 (12)
Ti6—Ti4^v	2.948 (4)	OS3—OS6^ix	2.791 (13)
Ti6—Na9^iv	3.385 (12)	OS3—OT1^ix	2.809 (12)
Ti6—OS23	3.438 (11)	OS3—OHT2^ix	2.840 (12)
Ti6—Ce1^v	3.589 (3)	OS3—Ba^ix	2.841 (9)
Ti6—OB9^iv	3.619 (9)	OS3—OW28^ix	3.260 (14)
Ti6—OS45^iv	3.727 (9)	OS4—OS13^ii	2.668 (13)
Ti7—OT2	1.907 (9)	OS4—OS35	2.785 (13)
Ti7—OS7	1.909 (10)	OS4—OT3^ii	2.807 (12)
Ti7—OS22	1.939 (10)	OS4—OS40	2.931 (13)
Ti7—OS9	1.947 (9)	OS4—OW23^ii	3.01 (2)
Ti7—OHT1	1.966 (9)	OS4—OW27^ii	3.555 (13)
Ti7—OS48	2.021 (9)	OS5—Ti8^ix	1.932 (9)
Ti7—Ti12	3.025 (4)	OS5—OW25	2.38 (2)
Ti7—OS39	3.394 (10)	OS5—OS29	2.607 (12)
Ti7—OB14	3.616 (9)	OS5—OS14^ix	2.681 (12)
Ti7—OS41	3.636 (8)	OS5—OS30	2.702 (12)
Ti7—K2^vi	3.778 (9)	OS5—OS37^ix	2.716 (13)
Ti8—OS37	1.911 (9)	OS5—OHT2^ix	2.787 (12)
Ti8—OS14	1.923 (9)	OS5—OT1^ix	2.899 (12)
Ti8—OT1	1.929 (9)	OS6—Na6^vii	2.581 (13)
Ti8—OS5^iii	1.932 (9)	OS6—OH5	2.659 (13)
Ti8—OHT2	2.017 (9)	OS6—OH4	2.697 (13)
Ti8—OS49	2.021 (9)	OS6—OS3^iii	2.791 (13)
Ti8—Ti9	3.032 (3)	OS6—OS41	2.793 (12)
Ti8—OW25^iii	3.393 (19)	OS6—OHT2	2.860 (12)
Ti8—OS3^iii	3.432 (9)	OS6—Na4^iii	2.916 (12)
Ti8—OB27	3.657 (9)	OS6—OS8	2.921 (12)
Ti8—Na2^iii	3.678 (8)	OS7—OS22	2.673 (14)
Ti9—OT1	1.893 (9)	OS7—OH13	2.714 (15)
Ti9—OS3^iii	1.924 (9)	OS7—K2^vi	2.721 (13)
Ti9—OS8	1.927 (9)	OS7—OHT1	2.803 (13)
Ti9—OS6	1.942 (9)	OS7—OS48	2.816 (12)
Ti9—OHT2	1.997 (9)	OS7—OS9	2.866 (13)
Ti9—OS41	2.046 (8)	OS7—Si14^vi	3.270 (11)
Ti9—OS5^iii	3.440 (9)	OS8—OS3^iii	2.634 (12)
Ti9—Na6^vii	3.501 (9)	OS8—Na6^vii	2.753 (14)
Ti9—OB37	3.630 (9)	OS8—OT1	2.755 (12)
Ti9—Na4^iii	3.661 (8)	OS8—OS41	2.793 (12)
Ti10—OS25	1.871 (9)	OS8—OW20	3.12 (2)
Ti10—OS26	1.903 (10)	OS9—OH21^vi	2.688 (14)
Ti10—OT5	1.911 (9)	OS9—OS41	2.707 (12)
Ti10—OS34	1.913 (9)	OS9—OS48	2.710 (12)
Ti10—OS31	2.073 (9)	OS9—OS22	2.738 (13)
Ti10—OS44	2.077 (9)	OS9—OT2	2.810 (12)
Ti10—Ti11	3.084 (3)	OS9—OW3	3.017 (19)
Ti10—OS32	3.465 (9)	OS10—Ti1^iv	1.906 (9)
Ti10—Na3	3.517 (9)	OS10—OS46	2.683 (12)
Ti10—OW36	3.616 (18)	OS10—OS30^iv	2.689 (12)
Ti10—OB22	3.625 (9)	OS10—Na4^iv	2.696 (12)
Ti11—OS43	1.875 (9)	OS10—OT6^iv	2.764 (12)
Ti11—OS32	1.914 (9)	OS10—OS27	2.771 (12)
Ti11—OT5	1.919 (9)	OS10—OS42	2.930 (12)
Ti11—OS28	1.950 (9)	OS10—OW15^iv	3.14 (3)
Ti11—OS1	2.043 (9)	OS10—OW28^xi	3.381 (14)
Ti11—OS44	2.055 (9)	OS11—OS23^i	2.673 (14)
Ti11—Na1^vii	3.391 (8)	OS11—OS35	2.744 (13)
Ti11—OS26	3.417 (10)	OS11—OT4^i	2.758 (14)
Ti11—OW31^vii	3.47 (2)	OS11—OS36	2.759 (13)
Ti11—OS48	3.600 (9)	OS11—OS18	2.956 (14)
Ti12—OS38	1.875 (9)	OS11—OW26	3.423 (19)
Ti12—OT2	1.913 (9)	OS12—OH22	2.708 (14)
Ti12—OS39	1.914 (10)	OS12—OS29	2.772 (13)
Ti12—OS24	1.922 (9)	OS12—OHT3	2.787 (13)
Ti12—OS47	2.024 (9)	OS12—OW21	2.79 (2)
Ti12—OHT1	2.050 (9)	OS12—OS33	2.933 (12)
Ti12—OS22	3.422 (11)	OS13—Ti3^iv	1.889 (9)
Ti12—OS49	3.566 (9)	OS13—OS16	2.654 (14)
Ti12—OB20	3.674 (10)	OS13—OS4^iv	2.668 (13)
Ti12—OS48	3.901 (9)	OS13—OT7	2.737 (14)
Si1—OS11	1.604 (10)	OS13—OS40^iv	2.757 (14)
Si1—OS35	1.629 (10)	OS13—OT3	2.796 (12)
Si1—OB7	1.648 (11)	OS13—OW23	2.87 (2)
Si1—OB10	1.654 (10)	OS13—OW33^xv	3.07 (2)
Si1—OS40	3.123 (11)	OS14—OW25^iii	2.53 (2)
Si1—OS36	3.248 (10)	OS14—OH19	2.647 (13)
Si1—Na8	3.319 (11)	OS14—OS5^iii	2.681 (12)
Si1—OT4^i	3.395 (10)	OS14—OS49	2.776 (12)
Si1—OB26	3.548 (11)	OS14—K1^iii	2.80 (3)
Si2—OH6	1.592 (12)	OS14—OHT2	2.850 (12)
Si2—OS40	1.629 (12)	OS14—OS37	2.973 (12)
Si2—OB10	1.645 (11)	OS15—Ti6^ii	1.964 (10)
Si2—OB29^ii	1.650 (12)	OS15—OS21^ii	2.673 (14)
Si2—OS35	3.183 (10)	OS15—OW35^x	2.69 (2)
Si2—OT7^ii	3.254 (10)	OS15—OS45	2.746 (13)
Si2—Na1	3.517 (10)	OS15—OT4^ii	2.754 (14)
Si2—OW29	3.520 (18)	OS15—OS46	2.761 (13)
Si3—OS18	1.600 (12)	OS15—OS20	2.891 (14)
Si3—OB28	1.625 (11)	OS15—OW26^iv	3.434 (18)
Si3—OH11	1.643 (18)	OS16—OS17	2.646 (13)
Si3—OH10	1.667 (19)	OS16—OS19	2.768 (15)
Si3—OS36	3.376 (10)	OS16—OT7	2.782 (14)
Si3—OB26	3.421 (11)	OS16—OT3	2.825 (12)
Si3—Na14	3.472 (15)	OS16—OW16	2.874 (16)
Si3—OW30	3.54 (6)	OS16—Ti3^iv	3.457 (10)
Si3—OW38^i	3.64 (3)	OS17—OS27	2.689 (12)
Si3—OW40^viii	3.65 (5)	OS17—OS45	2.781 (13)
Si4—OS33	1.588 (9)	OS17—OT3	2.783 (12)
Si4—OS36	1.625 (11)	OS17—OS19	2.950 (14)
Si4—OB26	1.647 (10)	OS17—OW16	2.991 (15)
Si4—OB28	1.651 (10)	OS17—OW8	3.32 (6)
Si4—OS18	3.086 (11)	OS18—OS23^i	2.680 (15)
Si4—OS2	3.254 (9)	OS18—OH11	2.70 (2)
Si4—OB12	3.494 (10)	OS18—OH10	2.71 (2)
Si4—OT6	3.510 (9)	OS18—OS36	2.800 (13)
Si4—OW40^viii	3.55 (5)	OS18—OHT4^i	2.870 (16)
Si4—Ba^ix	3.602 (4)	OS19—OS45	2.761 (13)
Si4—OW28^ix	3.629 (11)	OS19—OT7	2.796 (14)
Si5—OB7	1.604 (11)	OS19—OW8	2.88 (6)
Si5—OH7	1.606 (12)	OS20—Ti6^ii	1.942 (11)
Si5—OB26	1.609 (10)	OS20—OH21	2.678 (15)
Si5—OB12	1.615 (11)	OS20—OB18^x	2.680 (15)
Si5—OW40	3.29 (5)	OS20—OS21^ii	2.712 (14)
Si5—OH3^vii	3.556 (10)	OS20—OHT4^ii	2.853 (16)
Si5—OS36	3.621 (11)	OS20—OS46	2.860 (13)
Si5—OS2	3.624 (10)	OS20—OW35^x	3.31 (2)
Si5—OS4	3.653 (10)	OS21—Na9^iv	2.379 (18)
Si5—OS35	3.660 (11)	OS21—OH2	2.660 (18)
Si6—OS4	1.611 (9)	OS21—OS15^iv	2.673 (14)
Si6—OS2	1.621 (9)	OS21—OS23	2.694 (16)
Si6—OB12	1.638 (10)	OS21—OS20^iv	2.712 (14)
Si6—OB38	1.642 (10)	OS21—OHT4	2.785 (15)
Si6—OS12	3.145 (10)	OS21—OT4	2.829 (14)
Si6—OS35	3.334 (11)	OS21—K2^iv	2.908 (13)
Si6—OB7	3.500 (11)	OS21—OW26^v	3.231 (18)
Si6—OT3^ii	3.502 (9)	OS22—OH12	2.604 (16)
Si6—OW27^ii	3.524 (10)	OS22—OS39	2.613 (15)
Si7—OS30	1.603 (9)	OS22—K2^vi	2.766 (14)
Si7—OS5	1.618 (9)	OS22—OHT1	2.798 (13)
Si7—OS29	1.625 (9)	OS22—OT2	2.835 (13)
Si7—OS3	1.637 (9)	OS22—OW3	2.861 (19)
Si7—Na4	3.235 (8)	OS23—Ti4^v	1.941 (10)
Si7—Na2	3.264 (9)	OS23—Na14^v	2.439 (17)
Si7—OHT2^ix	3.271 (9)	OS23—Na8^v	2.494 (15)
Si7—OHT3	3.334 (9)	OS23—OS11^v	2.673 (14)
Si7—OT6	3.393 (9)	OS23—OS18^v	2.680 (15)
Si7—OT1^ix	3.404 (9)	OS23—OH2	2.752 (19)
Si7—OW25	3.49 (2)	OS23—OHT4	2.769 (14)
Si7—Ba^ix	3.516 (4)	OS23—OT4	2.928 (14)
Si8—OS12	1.609 (10)	OS23—OW26^v	3.402 (18)
Si8—OB38	1.615 (10)	OS24—OS39	2.733 (14)
Si8—OB13	1.623 (9)	OS24—OHT1	2.792 (13)
Si8—OH22	1.624 (11)	OS24—OS47	2.795 (13)
Si8—Na11^ii	3.203 (10)	OS24—OS38	2.837 (13)
Si8—OS2	3.318 (10)	OS24—OH23	3.23 (4)
Si8—OHT3	3.560 (10)	OS24—OW1^iv	3.29 (5)
Si8—OB12	3.603 (11)	OS25—OS26	2.696 (13)
Si8—OH29	3.63 (6)	OS25—OW36	2.71 (2)
Si8—OH19^ii	3.658 (11)	OS25—OS47	2.724 (12)
Si9—OH19	1.566 (10)	OS25—OS31	2.767 (13)
Si9—OS14	1.600 (10)	OS25—OT5	2.801 (12)
Si9—OB8	1.629 (10)	OS25—OS34	2.963 (13)
Si9—OB27	1.655 (10)	OS25—OW22^xiii	3.04 (3)
Si9—Na10	3.257 (7)	OS26—OH9	2.617 (15)
Si9—OS49	3.314 (10)	OS26—OH15	2.640 (16)
Si9—OH22^iv	3.470 (11)	OS26—OS32	2.658 (13)
Si9—K1^iv	3.48 (2)	OS26—OS34	2.731 (15)
Si9—OW25^iv	3.502 (19)	OS26—OS44	2.793 (13)
Si9—OHT3^iv	3.570 (9)	OS26—OT5	2.823 (13)
Si9—OHT2	3.593 (9)	OS26—OW36	2.83 (2)
Si9—OB25	3.604 (10)	OS26—OW22	3.25 (3)
Si10—OT7	1.609 (10)	OS27—Ti1^iv	2.037 (9)
Si10—OB29	1.622 (11)	OS27—Ce1^iv	2.627 (8)
Si10—OB35	1.633 (13)	OS27—OT6^iv	2.673 (12)
Si10—OB34	1.635 (13)	OS27—OS42	2.771 (12)
Si10—OS40^iv	3.113 (11)	OS27—OHT3^iv	2.947 (12)
Si10—OS19	3.148 (12)	OS27—OT3	3.101 (12)
Si10—OB33	3.605 (15)	OS27—OS45	3.172 (13)
Si11—OB15	1.593 (12)	OS28—Na1^vii	2.408 (12)
Si11—OB36	1.601 (10)	OS28—OH3	2.726 (13)
Si11—OS19	1.623 (12)	OS28—OS32	2.734 (13)
Si11—OB34	1.640 (12)	OS28—OS44	2.767 (12)
Si11—OS45	3.142 (10)	OS28—OS43	2.983 (13)
Si11—OT7	3.268 (11)	OS29—OS33	2.601 (12)
Si11—OH32	3.64 (4)	OS29—OS30	2.632 (12)
Si11—OB32	3.654 (11)	OS29—OT6	2.788 (12)
Si11—K3	3.86 (2)	OS29—OHT3	2.865 (12)
Si12—OS15	1.600 (10)	OS29—Ba^ix	2.906 (9)
Si12—OB32	1.639 (12)	OS29—OW14	3.093 (13)
Si12—OB15	1.639 (10)	OS30—OS10^ii	2.689 (12)
Si12—OS45	1.642 (11)	OS30—OS42^ii	2.710 (11)
Si12—OS19	3.106 (11)	OS30—OHT3	2.818 (12)
Si12—OS46	3.285 (10)	OS30—OT6	2.888 (11)
Si12—Na9	3.301 (14)	OS30—OW9	3.06 (4)
Si12—OT4^ii	3.406 (10)	OS31—OT5	2.691 (12)
Si12—OB11	3.464 (11)	OS31—OS37	2.707 (12)
Si12—OW35^x	3.48 (2)	OS31—OS34	2.776 (12)
Si13—OB11	1.603 (11)	OS31—OS44	2.958 (12)
Si13—OH8	1.604 (12)	OS31—OT1	3.068 (12)
Si13—OB32	1.620 (11)	OS31—OS47	3.159 (12)
Si13—OB30	1.625 (10)	OS32—Na1^vii	2.528 (12)
Si13—OS27	3.593 (10)	OS32—OH15	2.626 (15)
Si13—OS45	3.626 (11)	OS32—OH9	2.647 (15)
Si13—OS17	3.664 (10)	OS32—OS43	2.663 (13)
Si13—OS46	3.666 (10)	OS32—OW31^vii	2.71 (2)
Si13—OS15	3.669 (11)	OS32—OS44	2.799 (13)
Si14—OS20	1.611 (11)	OS32—OT5	2.873 (12)
Si14—OH21	1.620 (11)	OS33—OS36	2.681 (13)
Si14—OB9	1.625 (10)	OS33—OT6	2.823 (12)
Si14—OB18^x	1.648 (11)	OS33—Ba^ix	2.970 (9)
Si14—OS7^x	3.270 (11)	OS33—OW13^ix	3.289 (16)
Si14—OS46	3.365 (9)	OS33—OW21	3.38 (2)
Si14—OB11	3.424 (10)	OS34—OH16	2.704 (14)
Si14—K2	3.532 (11)	OS34—OS44	2.719 (13)
Si15—OS46	1.597 (10)	OS35—OT3^ii	2.681 (12)
Si15—OS10	1.612 (9)	OS35—OS40	2.767 (13)
Si15—OB11	1.648 (11)	OS35—OT7^ii	2.923 (13)
Si15—OB9	1.650 (10)	OS35—OT4^i	3.043 (13)
Si15—OS20	3.160 (10)	OS36—OT4^i	2.687 (14)
Si15—OS27	3.243 (9)	OS36—OHT4^i	2.915 (14)
Si15—OT6^iv	3.436 (9)	OS36—OT6	3.089 (12)
Si15—Na4^iv	3.446 (9)	OS37—OS5^iii	2.716 (13)
Si15—OW28^xi	3.532 (11)	OS37—OT1	2.721 (12)
Si15—OB30	3.565 (10)	OS37—Na2^iii	2.727 (12)
Si15—OS15	3.652 (10)	OS37—OS49	2.768 (12)
Si16—OS27	1.607 (9)	OS37—OW14^iii	3.264 (13)
Si16—OS17	1.621 (9)	OS37—OW7^iii	3.30 (6)
Si16—OB30	1.643 (10)	OS38—OS39	2.662 (14)
Si16—OB5	1.651 (10)	OS38—OS49	2.685 (12)
Si16—OS42	3.094 (9)	OS38—OS47	2.742 (12)
Si16—OS45	3.320 (10)	OS38—OT2	2.871 (12)
Si16—OT3	3.493 (9)	OS38—OW1^iv	3.05 (5)
Si16—OB32	3.524 (10)	OS38—OW17	3.067 (15)
Si16—OW27	3.606 (10)	OS39—OH12	2.628 (16)
Si17—OB35	1.541 (15)	OS39—OW17	2.797 (16)
Si17—OH14	1.57 (3)	OS39—OT2	2.798 (12)
Si17—OH1	1.64 (2)	OS39—OHT1	2.837 (13)
Si17—OB33	1.672 (16)	OS39—OH23	3.17 (5)
Si17—OH31^xii	3.27 (6)	OS40—OB29^ii	2.645 (15)
Si17—OT7	3.515 (11)	OS40—OH6	2.709 (15)
Si17—OS16	3.638 (13)	OS40—OT7^ii	2.717 (14)
Si17—K3	3.65 (2)	OS40—OS13^ii	2.757 (14)
Si18—OS16	1.607 (11)	OS40—OW29	2.89 (2)
Si18—OS13	1.639 (11)	OS40—OW33^vii	2.93 (2)
Si18—OB33	1.640 (12)	OS40—Si10^ii	3.112 (11)
Si18—OB16	1.662 (13)	OS41—OT1	2.657 (11)
Si18—Si40	2.761 (14)	OS41—OHT2	2.895 (11)
Si18—OT7	3.044 (11)	OS41—OT2	2.997 (11)
Si18—OT3	3.410 (9)	OS42—Ti1^iv	1.919 (8)
Si18—OH28	3.41 (3)	OS42—Na12^iv	2.605 (16)
Si18—OH27^xii	3.48 (4)	OS42—OH17	2.668 (12)
Si18—K3	3.58 (2)	OS42—OS30^iv	2.710 (11)
Si19—OS42	1.599 (9)	OS42—OHT3^iv	2.880 (12)
Si19—OH17	1.612 (10)	OS42—OW9^iv	3.08 (4)
Si19—OB8	1.634 (10)	OS43—OW31^vii	2.46 (2)
Si19—OB5	1.641 (9)	OS43—OS48	2.694 (12)
Si19—OS27	3.295 (9)	OS43—OT5	2.784 (12)
Si19—Na10	3.322 (7)	OS43—OW34	3.489 (15)
Si19—Na12^iii	3.468 (13)	OS44—OT5	2.446 (12)
Si19—OH4	3.525 (10)	OS44—OH34	2.696 (14)
Si19—OHT2	3.567 (9)	OS45—Ce1^iv	2.524 (10)
Si19—OHT3^iv	3.589 (9)	OS45—OT3	2.654 (13)
Si19—OB30	3.634 (10)	OS45—OT7	2.969 (13)
Si20—OH12	1.582 (13)	OS45—OT4^ii	3.070 (13)
Si20—OS39	1.595 (12)	OS46—Ti6^ii	2.050 (9)
Si20—OS22	1.611 (11)	OS46—Ce1^iv	2.561 (9)
Si20—OB17	1.633 (11)	OS46—OT4^ii	2.690 (13)
Si20—OHT1	3.150 (10)	OS46—OHT4^ii	2.911 (13)
Si20—OT2	3.420 (9)	OS46—OT6^iv	3.019 (12)
Si20—OH23	3.45 (4)	OS47—OT2	2.673 (12)
Si20—K2^vi	3.540 (10)	OS47—OHT1	2.883 (13)
Si20—OH24^xii	3.61 (3)	OS47—OT5	3.097 (12)
Si20—OH26	3.67 (4)	OS48—OT2	2.686 (12)
Si21—OS6	1.600 (10)	OS48—OHT1	2.887 (12)
Si21—OH5	1.612 (11)	OS48—OT5	3.054 (12)
Si21—OH4	1.616 (10)	OS49—OT1	2.676 (12)
Si21—OB37	1.634 (9)	OS49—OHT2	2.891 (12)
Si21—Na5	3.273 (9)	OS49—OT2	3.079 (12)
Si21—OS41	3.337 (9)	OT1—OHT2	2.417 (12)
Si21—Na6^vii	3.360 (11)	OT1—OW14^iii	2.683 (13)
Si21—OB4	3.418 (10)	OT1—OS3^iii	2.809 (12)
Si21—OH20^vii	3.628 (10)	OT1—OS5^iii	2.899 (12)
Si21—OHT2	3.630 (9)	OT2—OHT1	2.428 (12)
Si21—OH17	3.665 (10)	OT2—OW11	2.823 (13)
Si21—OW24^iii	3.668 (16)	OT3—Ti3^iv	1.928 (9)
Si22—OS41	1.609 (9)	OT3—OT7	2.470 (12)
Si22—OS9	1.614 (9)	OT3—Ce1^iv	2.509 (8)
Si22—OB37	1.625 (9)	OT3—OS35^iv	2.681 (12)
Si22—OB4	1.644 (9)	OT3—OS4^iv	2.807 (12)
Si22—OS6	3.044 (9)	OT3—OW27	2.835 (13)
Si22—OS48	3.290 (9)	OT3—OS2^iv	3.099 (12)
Si22—OB31	3.408 (10)	OT4—Ti4^v	1.950 (10)
Si22—OT2	3.417 (9)	OT4—OHT4	2.459 (13)
Si22—OW11	3.532 (10)	OT4—Ce1^v	2.488 (10)
Si22—OH21^vi	3.535 (11)	OT4—OS36^v	2.687 (14)
Si23—OS38	1.606 (10)	OT4—OS46^iv	2.690 (13)
Si23—OS49	1.623 (10)	OT4—OW26^v	2.731 (18)
Si23—OB27	1.632 (10)	OT4—OS15^iv	2.754 (14)
Si23—OB25	1.638 (11)	OT4—OS11^v	2.758 (14)
Si23—OS14	3.069 (10)	OT4—OS35^v	3.043 (13)
Si23—OS47	3.300 (10)	OT5—OW34	2.794 (15)
Si23—OB21	3.506 (11)	OT6—OHT3	2.425 (12)
Si23—OT2	3.534 (9)	OT6—OS27^ii	2.674 (12)
Si23—OW11	3.585 (10)	OT6—OW28^ix	2.731 (13)
Si24—OH18	1.582 (12)	OT6—OS10^ii	2.764 (12)
Si24—OB21	1.627 (11)	OT6—OS46^ii	3.019 (12)
Si24—OB24	1.629 (11)	OT7—Ti3^iv	2.058 (10)
Si24—OB25	1.643 (11)	OT7—OS40^iv	2.717 (14)
Si24—OW37	3.480 (15)	OT7—OS35^iv	2.923 (13)
Si24—OS31	3.627 (9)	OHT1—OH24^xii	2.55 (3)
Si24—OS49	3.654 (10)	OHT1—OW34	3.105 (16)
Si24—OW1^iv	3.66 (5)	OHT2—OH17	2.638 (13)
Si25—OH20	1.576 (10)	OHT2—OS5^iii	2.787 (12)
Si25—OB31	1.615 (9)	OHT2—OS3^iii	2.840 (12)
Si25—OB4	1.630 (10)	OHT2—OW11	2.970 (13)
Si25—OB3	1.639 (10)	OHT2—Si7^iii	3.271 (9)
Si25—OH5^vii	3.324 (11)	OHT3—OH19^ii	2.695 (13)
Si25—Na6^vii	3.492 (10)	OHT3—OS42^ii	2.880 (12)
Si25—OS1	3.549 (9)	OHT3—OS27^ii	2.947 (12)
Si25—OS8	3.629 (9)	OHT3—OW27^ii	2.958 (13)
Si25—OS41	3.647 (9)	OHT3—OB8^ii	3.278 (13)
Si26—OS31	1.607 (9)	OHT4—Ti4^v	1.933 (10)
Si26—OS37	1.613 (10)	OHT4—OW38	2.69 (4)
Si26—OB24	1.621 (10)	OHT4—OS20^iv	2.853 (16)
Si26—OB23	1.625 (10)	OHT4—OS18^v	2.870 (16)
Si26—OS34	3.109 (10)	OHT4—OS46^iv	2.912 (13)
Si26—OS49	3.304 (10)	OHT4—OS36^v	2.915 (14)
Si26—OT1	3.411 (9)	OHT4—OH2	3.272 (18)
Si26—OB25	3.519 (11)	OH1—OH32	2.51 (5)
Si26—Na2^iii	3.521 (8)	OH1—OH33	2.59 (4)
Si26—OW14^iii	3.522 (11)	OH1—OH14	2.61 (4)
Si27—OS43	1.605 (10)	OH1—OH31^xii	2.91 (6)
Si27—OS48	1.609 (9)	OH1—Si37	3.60 (2)
Si27—OB31	1.610 (10)	OH1—Si38	3.64 (3)
Si27—OB14	1.643 (9)	OH2—OH25	2.58 (4)
Si27—OS1	3.191 (9)	OH2—K2^iv	2.788 (19)
Si27—OS7	3.206 (10)	OH2—Si41	3.48 (2)
Si27—OW31^vii	3.24 (2)	OH2—Na14^v	3.57 (2)
Si27—OT5	3.465 (9)	OH2—OW38	3.87 (4)
Si27—OB18	3.546 (10)	OH3—OH7^vii	2.564 (14)
Si27—OS9	3.554 (10)	OH3—OW29^vii	2.71 (2)
Si27—OW34	3.588 (13)	OH3—OB7^vii	3.522 (14)
Si27—OB3	3.617 (9)	OH3—Si5^vii	3.556 (10)
Si28—OB21	1.623 (11)	OH3—Na1^vii	3.816 (12)
Si28—OS25	1.624 (10)	OH3—OW13	3.861 (16)
Si28—OS47	1.636 (10)	OH3—OB12^vii	4.181 (13)
Si28—OB20	1.651 (11)	OH3—Na15^vii	4.28 (2)
Si28—OS24	3.151 (11)	OH4—OH17	2.569 (13)
Si28—OS31	3.267 (9)	OH4—OH5	2.643 (14)
Si28—OW36	3.346 (18)	OH4—OW32	2.76 (3)
Si28—OT5	3.497 (9)	OH4—OW5	3.26 (4)
Si28—OB24	3.508 (11)	OH4—OW15^iii	3.29 (3)
Si28—OW34	3.596 (13)	OH5—OH20^vii	2.536 (14)
Si28—OS38	3.641 (10)	OH5—OW24^iii	3.150 (18)
Si29—OH13	1.598 (12)	OH5—Na6^vii	3.184 (15)
Si29—OB18	1.616 (11)	OH5—OB4^vii	3.293 (13)
Si29—OS7	1.618 (11)	OH5—Si25^vii	3.324 (11)
Si29—OB14	1.641 (10)	OH5—OW32	3.75 (3)
Si29—OS48	3.325 (9)	OH6—OH9^vii	2.523 (16)
Si29—OB31	3.366 (10)	OH6—OB29^ii	2.670 (15)
Si29—OH28^xii	3.55 (4)	OH6—OW12	2.70 (5)
Si29—OS20^vi	3.568 (12)	OH6—OW29	3.44 (2)
Si29—OH21^vi	3.624 (11)	OH6—OS32^vii	3.468 (14)
Si29—K2^vi	3.647 (11)	OH6—Si36^vii	3.553 (12)
Si30—OB1	1.565 (11)	OH6—OH34^vii	3.711 (15)
Si30—OB19	1.615 (10)	OH6—OW10	3.868 (18)
Si30—OS24	1.618 (11)	OH7—OH3^vii	2.564 (14)
Si30—OB20	1.623 (11)	OH7—OW40	2.76 (5)
Si30—OS47	3.266 (10)	OH7—OW13^vii	3.024 (17)
Si30—OH31	3.52 (5)	OH7—OH10^viii	3.09 (2)
Si30—OHT1	3.516 (10)	OH7—OB6^vii	3.469 (14)
Si30—OH2	3.582 (16)	OH7—OW40^viii	3.48 (5)
Si30—OB21	3.611 (12)	OH7—Si33^vii	3.570 (11)
Si31—OS23	1.613 (12)	OH7—OB28^viii	4.050 (14)
Si31—OB19	1.619 (11)	OH8—OW32	3.12 (3)
Si31—OS21	1.644 (12)	OH8—OW35^x	4.32 (3)
Si31—OH2	1.667 (16)	OH8—OW8	4.35 (6)
Si31—OHT4	2.994 (10)	OH9—OH6^vii	2.523 (16)
Si31—Na14^v	3.436 (15)	OH9—OH15	2.637 (17)
Si31—Na8^v	3.445 (13)	OH9—OW39^xiii	2.77 (4)
Si31—K2^iv	3.452 (11)	OH9—OW10^vii	3.114 (19)
Si31—OT4	3.460 (11)	OH9—OH34	3.444 (16)
Si31—Na9^iv	3.529 (17)	OH9—Na1^vii	3.635 (15)
Si31—OW26^v	3.610 (16)	OH9—OW12^vii	3.85 (5)
Si31—OB1	3.615 (14)	OH9—OW22	3.87 (3)
Si32—OS8	1.604 (9)	OH10—OW30	2.30 (6)
Si32—OS1	1.624 (9)	OH10—OH11	2.68 (3)
Si32—OB3	1.639 (9)	OH10—OW40^viii	2.82 (5)
Si32—OB2	1.657 (9)	OH10—OW40	2.91 (5)
Si32—OS28	3.082 (9)	OH10—OH7^viii	3.09 (2)
Si32—OS41	3.310 (9)	OH10—OH30^viii	3.73 (4)
Si32—OB4	3.442 (9)	OH11—OW38^i	2.74 (4)
Si32—OT1	3.465 (9)	OH11—OW20^ix	3.21 (3)
Si32—OB31	3.645 (9)	OH11—OHT4^i	4.10 (2)
Si32—OW20	3.647 (19)	OH11—Ba^ix	4.109 (18)
Si33—OH3	1.573 (10)	OH11—OW8^viii	4.15 (6)
Si33—OS28	1.623 (9)	OH11—OH30^viii	4.19 (2)
Si33—OB2	1.633 (9)	OH11—OH7^viii	4.19 (2)
Si33—OB6	1.647 (10)	OH12—OH25^xii	2.67 (3)
Si33—OS44	3.233 (10)	OH12—OW16	2.818 (17)
Si33—OS1	3.278 (9)	OH12—OW3	3.35 (2)
Si33—OW29^vii	3.525 (18)	OH12—Si40	3.370 (19)
Si33—OH7^vii	3.571 (11)	OH12—OH26	3.37 (4)
Si33—OW13	3.614 (14)	OH12—OW17	3.436 (17)
Si34—OS44	1.606 (9)	OH12—OH27^xii	3.50 (4)
Si34—OB6	1.626 (10)	OH13—OH28^xii	2.25 (4)
Si34—OH34	1.636 (11)	OH13—OW35	2.68 (3)
Si34—OB22	1.639 (10)	OH13—OH26^xii	3.07 (4)
Si34—OS34	3.014 (10)	OH13—Si40^xii	3.414 (18)
Si34—OS28	3.167 (10)	OH13—OW19^vi	3.78 (4)
Si34—OW14^iii	3.621 (10)	OH13—K2^vi	3.940 (16)
Si35—OH16	1.561 (12)	OH13—OS20^vi	3.973 (16)
Si35—OS34	1.627 (11)	OH13—OW33^xvi	4.01 (2)
Si35—OB23	1.650 (10)	OH14—OH31^xii	2.92 (6)
Si35—OB22	1.669 (10)	OH14—OH15^xii	3.59 (3)
Si35—OS31	3.218 (9)	OH14—OW12^iv	3.78 (5)
Si35—OS44	3.273 (10)	OH14—OW36^xii	3.91 (3)
Si35—OH34	3.484 (11)	OH14—OH27^xii	3.94 (5)
Si35—Na13^xiii	3.50 (3)	OH14—OW31^xvii	4.23 (3)
Si35—OW18^vii	3.608 (18)	OH14—OH28	4.30 (5)
Si35—OW4^vii	3.62 (4)	OH14—OH33	4.36 (3)
Si36—OH9	1.579 (13)	OH15—OW36	2.60 (2)
Si36—OS32	1.607 (10)	OH15—OW31^vii	2.63 (2)
Si36—OS26	1.617 (11)	OH15—OW34	3.322 (18)
Si36—OH15	1.659 (13)	OH15—OH14^xii	3.59 (3)
Si36—Na3	3.181 (11)	OH15—OW39^xiii	3.65 (4)
Si36—OW31^vii	3.29 (2)	OH16—OW4^vii	2.62 (4)
Si36—OS44	3.288 (10)	OH16—Na13^xiii	2.64 (3)
Si36—OW36	3.335 (19)	OH16—OW18^vii	2.76 (2)
Si36—OT5	3.342 (9)	OH16—Na7^vii	3.69 (3)
Si36—OH6^vii	3.553 (12)	OH16—Na14^vii	3.958 (17)
Na1—OW2	2.18 (5)	OH16—OH34	4.002 (15)
Na1—OH6	2.358 (14)	OH16—OW30^vii	4.16 (6)
Na1—OS28^vii	2.408 (12)	OH17—Na12^iii	2.592 (16)
Na1—OW29	2.48 (2)	OH17—OW15^iii	2.97 (3)
Na1—OS32^vii	2.528 (12)	OH17—OW9^iii	3.55 (4)
Na1—Ti11^vii	3.391 (8)	OH17—OW11	3.737 (13)
Na1—Na15	3.40 (2)	OH18—OW39	2.62 (4)
Na1—OW12	3.58 (4)	OH18—OW37	2.629 (19)
Na1—OH9^vii	3.634 (15)	OH18—OW10^v	2.917 (19)
Na1—OH3^vii	3.816 (12)	OH18—OW1^iv	3.75 (5)
Na1—OS43^vii	3.859 (12)	OH18—OW22^xiii	4.14 (3)
Na2—OW7	2.34 (6)	OH18—OB29^iv	4.464 (16)
Na2—OW14	2.548 (12)	OH18—OH9^xiii	4.473 (17)
Na2—OS29	2.576 (12)	OH19—OH22^iv	2.562 (14)
Na2—OW21	2.59 (2)	OH19—K1^iv	2.59 (3)
Na2—OS37^ix	2.727 (12)	OH19—OW25^iv	2.68 (2)
Na2—OS5	2.732 (12)	OH19—OHT3^iv	2.695 (13)
Na2—OS12	2.866 (12)	OH19—OW7^iv	2.86 (6)
Na2—OB23^ix	3.022 (13)	OH19—OW9^iv	3.50 (4)
Na2—Si26^ix	3.521 (8)	OH19—OS12^iv	3.639 (13)
Na2—Ti8^ix	3.678 (8)	OH19—Si8^iv	3.658 (11)
Na3—OW22	2.24 (3)	OH20—OH5^vii	2.536 (14)
Na3—OS26	2.503 (14)	OH20—OW32^vii	3.02 (3)
Na3—OW10^vii	2.512 (18)	OH20—OW24^viii	3.210 (18)
Na3—OH34	2.593 (15)	OH20—OW15^viii	3.49 (3)
Na3—OW18^vii	2.63 (2)	OH20—Si21^vii	3.628 (10)
Na3—OS34	2.691 (14)	OH20—OH4^vii	3.755 (14)
Na3—OH9	2.749 (16)	OH20—Na6^vii	3.796 (12)
Na3—Na8^vii	3.571 (14)	OH20—OH21^vi	4.270 (14)
Na3—OS44	3.691 (13)	OH21—OS9^x	2.688 (14)
Na3—OH16	3.877 (15)	OH21—OB18^x	2.698 (15)
Na4—OW15	2.34 (3)	OH21—OW24^iv	2.809 (18)
Na4—OW24	2.351 (17)	OH21—OW38^ii	3.24 (4)
Na4—OS3	2.512 (12)	OH21—OS7^x	3.304 (14)
Na4—OW28^ix	2.604 (13)	OH21—OW3^x	3.487 (19)
Na4—OS10^ii	2.696 (12)	OH21—OB4^x	3.498 (14)
Na4—OS30	2.789 (11)	OH21—Si22^x	3.535 (11)
Na4—OS6^ix	2.916 (12)	OH21—Si29^x	3.624 (11)
Na4—OB9^ii	2.990 (12)	OH22—Na11^ii	2.484 (15)
Na4—Si15^ii	3.446 (9)	OH22—OH19^ii	2.562 (14)
Na4—Ti9^ix	3.661 (8)	OH22—OB27^ii	3.277 (13)
Na5—OW5	2.33 (4)	OH22—OH29	3.37 (7)
Na5—OW16	2.378 (15)	OH22—OW7	3.42 (6)
Na5—OW11	2.433 (13)	OH22—Si38	3.463 (18)
Na5—OW3	2.494 (19)	OH22—Si9^ii	3.470 (11)
Na5—OH4	2.536 (13)	OH22—OW27^ii	3.499 (14)
Na5—OB37	2.771 (13)	OH23—Si39	1.627 (10)
Na5—OB5	2.979 (14)	OH23—OH26	2.36 (5)
Na5—Na10	3.381 (11)	OH23—K2^iv	2.42 (5)
Na5—OH17	3.934 (13)	OH23—OB17^xii	2.63 (3)
Na5—OS17	3.937 (13)	OH23—OH24	2.80 (3)
Na5—OS9	4.057 (14)	OH23—Si39^xii	3.10 (3)
Na6—OW24^viii	2.335 (18)	OH23—OW19^iv	3.22 (5)
Na6—OH5	2.463 (13)	OH23—OH24^xii	3.52 (5)
Na6—OW20^vii	2.50 (2)	OH24—Si39	1.625 (10)
Na6—OS6^vii	2.581 (13)	OH24—OH26	2.27 (5)
Na6—OS8^vii	2.754 (14)	OH24—OH27^xii	2.49 (5)
Na6—OB4^vii	2.930 (13)	OH24—OHT1^xii	2.55 (3)
Na6—OH5^vii	3.184 (15)	OH24—OB17^xii	2.59 (2)
Na6—OB3^vii	3.250 (14)	OH24—OB1^xii	2.85 (3)
Na6—Si21^vii	3.360 (11)	OH24—Si40	2.93 (3)
Na6—Si25^vii	3.492 (10)	OH24—Si39^xii	2.97 (3)
Na6—Ti9^vii	3.501 (9)	OH24—Si41^xii	3.17 (3)
Na6—Na4^viii	3.715 (12)	OH24—OH23^xii	3.52 (5)
Na7—OW30	2.00 (6)	OH25—Si41	1.626 (10)
Na7—Na14	2.69 (3)	OH25—OH27	2.58 (4)
Na7—OS11	2.87 (2)	OH25—OH12^xii	2.67 (3)
Na7—OW4	2.87 (4)	OH25—OH31	2.79 (4)
Na7—OS18	2.92 (2)	OH25—K3^xii	3.23 (4)
Na7—OB22^vii	3.01 (2)	OH25—OB16^xii	3.49 (4)
Na7—OH10	3.26 (3)	OH25—Si40^xii	3.50 (3)
Na7—OH34^vii	3.33 (2)	OH25—OB33^xii	3.76 (3)
Na7—OW13^vii	3.65 (3)	OH25—OH24^xii	3.79 (4)
Na7—Na8	3.65 (3)	OH25—OH1^xii	3.81 (4)
Na7—OH16^vii	3.69 (3)	OH26—Si40	1.613 (10)
Na7—OS23^i	3.71 (3)	OH26—OH28	2.42 (4)
Na8—OW18	2.35 (2)	OH26—OH27^xii	2.54 (4)
Na8—OW10	2.426 (18)	OH26—Si39	2.59 (3)
Na8—OS11	2.437 (14)	OH26—OW19^iv	2.71 (5)
Na8—OS23^i	2.494 (15)	OH26—OH13^xii	3.07 (4)
Na8—OW26	2.547 (18)	OH27—Si40^xii	1.51 (3)
Na8—OB10	2.973 (15)	OH27—Si41	1.617 (10)
Na8—OB19^i	3.246 (16)	OH27—OH24^xii	2.49 (5)
Na8—OH34^vii	3.282 (16)	OH27—OH28^xii	2.52 (4)
Na8—Si31^i	3.445 (13)	OH27—OH26^xii	2.54 (4)
Na8—Na3^vii	3.571 (14)	OH27—OB16^xii	2.69 (4)
Na9—OW1	2.15 (5)	OH27—OH31	2.72 (4)
Na9—OS21^ii	2.379 (18)	OH27—OB33^xii	2.90 (4)
Na9—OS15	2.413 (15)	OH27—Si18^xii	3.48 (4)
Na9—OW26^iv	2.67 (3)	OH27—OH12^xii	3.50 (4)
Na9—OW6^ii	2.77 (4)	OH28—Si40	1.620 (10)
Na9—OW19	2.93 (5)	OH28—OH13^xii	2.25 (4)
Na9—OB15	2.987 (19)	OH28—OH27^xii	2.52 (4)
Na9—OW35^x	3.21 (3)	OH28—OW33^xv	2.90 (4)
Na9—Ti6^ii	3.385 (12)	OH28—Si29^xii	3.55 (4)
Na9—OB19^ii	3.52 (2)	OH28—OW19^iv	3.77 (6)
Na9—Si31^ii	3.529 (17)	OH29—Si38	1.621 (10)
Na10—OW16	2.350 (14)	OH29—OH33	1.95 (6)
Na10—OW11	2.367 (11)	OH29—Si37	2.447 (19)
Na10—OW27	2.384 (11)	OH29—OH32	2.68 (5)
Na10—OB8	2.433 (12)	OH29—OW37^ii	2.71 (6)
Na10—OW17	2.435 (14)	OH29—OW7	3.63 (8)
Na10—OB27	2.731 (12)	OH29—OH30	4.00 (3)
Na10—OB5	2.857 (11)	OH30—Si37	1.617 (10)
Na10—Na11	3.364 (12)	OH30—OH32	1.84 (6)
Na10—OS38	3.685 (11)	OH30—Si38	2.43 (2)
Na11—OW6	2.27 (4)	OH30—OH33	2.59 (4)
Na11—OW17	2.346 (15)	OH30—OW4^viii	3.14 (6)
Na11—OW27	2.443 (14)	OH30—OW8	3.27 (8)
Na11—OW23	2.48 (3)	OH30—OH10^viii	3.73 (4)
Na11—OH22^iv	2.484 (15)	OH30—OW30^viii	3.76 (7)
Na11—OB38^iv	2.702 (15)	OH31—Si41	1.630 (10)
Na11—Si8^iv	3.203 (10)	OH31—OH1^xii	2.91 (6)
Na11—OB27	3.246 (17)	OH31—OH14^xii	2.92 (6)
Na11—OW19^iv	3.36 (4)	OH31—OW36	2.95 (5)
Na11—OS4^iv	3.841 (17)	OH31—Si17^xii	3.27 (6)
Na11—OW1^iv	4.09 (5)	OH31—OB33^xii	3.47 (6)
Na12—Na12^xiv	2.30 (3)	OH31—OW34	3.64 (6)
Na12—OW9	2.33 (4)	OH32—OH33	0.84 (4)
Na12—OS30	2.534 (19)	OH32—Si37	1.38 (3)
Na12—OW15	2.58 (4)	OH32—Si38	1.619 (10)
Na12—OH17^ix	2.592 (16)	OH32—OW4^viii	2.55 (5)
Na12—OS42^ii	2.605 (16)	OH33—Si38	1.40 (2)
Na12—OW9^xiv	2.77 (4)	OH33—Si37	1.622 (10)
Na12—OS42^ix	3.269 (16)	OH33—OW4^viii	2.89 (5)
Na12—Si19^ix	3.468 (13)	OH34—OB10^vii	2.784 (14)
Na12—OS10^ii	3.476 (17)	OH34—Na8^vii	3.282 (16)
Na13—OW36	2.26 (3)	OH34—Na7^vii	3.33 (2)
Na13—OH16^xiii	2.64 (3)	OH34—OW18^vii	3.41 (2)
Na13—OW22	2.94 (4)	OW1—OW6^ii	2.82 (6)
Na13—OH15	3.22 (3)	OW1—OW37^ii	2.86 (5)
Na13—OS26	3.31 (3)	OW1—OS38^ii	3.05 (5)
Na13—Si35^xiii	3.50 (3)	OW1—OW26^iv	3.18 (5)
Na13—OW18^v	3.59 (3)	OW1—OS24^ii	3.29 (5)
Na13—OS34^xiii	3.64 (3)	OW1—OB25^ii	3.31 (5)
Na13—OW39^xiii	3.71 (5)	OW1—OB21^ii	3.33 (5)
Na13—OS25	3.91 (3)	OW1—OB19^ii	3.65 (5)
Na13—OH31	4.02 (4)	OW1—Si24^ii	3.65 (5)
Na13—OB23^xiii	4.08 (3)	OW1—OW19	3.67 (6)
Na14—OS18	2.425 (16)	OW1—OH18^ii	3.75 (5)
Na14—OS23^i	2.439 (17)	OW2—OW29	3.34 (6)
Na14—OW4	2.48 (4)	OW2—OW33^vii	3.51 (6)
Na14—OW30	3.38 (6)	OW2—OW12	3.63 (7)
Na14—Si31^i	3.436 (15)	OW2—OS28^vii	3.80 (5)
Na14—OH2^i	3.57 (2)	OW2—OS32^vii	3.92 (5)
Na14—OW18	3.67 (2)	OW2—OS43^vii	4.16 (5)
Na14—OH10	3.74 (2)	OW2—OW31	4.35 (6)
Na15—OW29	2.23 (3)	OW3—OW38^xii	2.96 (4)
Na15—OW33^vii	2.40 (3)	OW3—OW16	3.25 (2)
Na15—OW2	2.63 (6)	OW3—OW5	3.39 (4)
Na15—OH8	3.62 (3)	OW3—OH21^vi	3.487 (19)
Na15—OS40	4.06 (3)	OW3—OW11	3.731 (19)
Na15—OH3^vii	4.28 (2)	OW3—OH2^xii	3.89 (2)
Na15—OW23^ii	4.34 (3)	OW3—K2^vi	4.06 (2)
K1—OW25	0.90 (3)	OW4—OW30	2.41 (7)
K1—OW7	2.16 (6)	OW4—OH32^viii	2.55 (5)
K1—K1^xiv	2.17 (5)	OW4—OH16^vii	2.62 (4)
K1—OW25^xiv	2.40 (3)	OW4—OH33^viii	2.89 (5)
K1—OH19^ii	2.59 (3)	OW4—OW21^viii	3.11 (4)
K1—OW9	2.69 (5)	OW4—OH30^viii	3.14 (6)
K1—OS14^ix	2.80 (3)	OW4—Si37^viii	3.52 (4)
K1—OS5	2.86 (3)	OW4—Si35^vii	3.62 (4)
K1—OW9^xiv	3.06 (5)	OW4—OB22^vii	3.69 (4)
K1—OS14^ii	3.31 (3)	OW4—OH1^viii	3.92 (4)
K1—Si9^ii	3.48 (2)	OW5—OW8	2.51 (7)
K1—OS37^ix	3.64 (3)	OW5—OW32	3.22 (5)
K2—OH23^ii	2.42 (5)	OW5—OW16	3.59 (4)
K2—OS20	2.662 (14)	OW5—OW38^xii	4.20 (5)
K2—OS7^x	2.721 (13)	OW6—OW19^iv	2.52 (6)
K2—OS22^x	2.766 (15)	OW6—OW23	2.72 (5)
K2—OH2^ii	2.788 (19)	OW6—Na9^iv	2.77 (4)
K2—OS21^ii	2.908 (13)	OW6—OW1^iv	2.82 (6)
K2—OB17^x	3.249 (15)	OW6—OB15^iv	2.95 (4)
K2—Si39^ii	3.278 (16)	OW6—OB36^iv	3.43 (4)
K2—Si31^ii	3.452 (11)	OW6—OW17	3.48 (4)
K2—Si20^x	3.540 (10)	OW6—OH22^iv	3.51 (4)
K2—Si29^x	3.647 (11)	OW6—OW37	3.57 (4)
K3—OH1	2.58 (3)	OW6—OW35^xii	3.58 (5)
K3—OS16	2.60 (2)	OW6—OB38^iv	3.70 (4)
K3—OS19	2.61 (2)	OW7—OW25	2.76 (6)
K3—OW8	2.71 (7)	OW7—OH19^ii	2.86 (6)
K3—OH25^xii	3.23 (4)	OW7—OS37^ix	3.30 (6)
K3—OH30	3.32 (5)	OW7—OB23^ix	4.05 (6)
K3—OH32	3.44 (5)	OW8—OH11^viii	4.15 (6)
K3—OB33	3.55 (2)	OW9—OW9^xiv	1.01 (7)
K3—OW16	3.72 (3)	OW9—OW25	1.86 (4)
OB1—Si41	1.584 (9)	OW9—OW25^xiv	2.41 (4)
OB1—OH31	2.42 (4)	OW9—Na12^xiv	2.77 (4)
OB1—OH27	2.57 (3)	OW9—K1^xiv	3.06 (5)
OB1—OB20	2.582 (17)	OW9—OS42^ii	3.08 (4)
OB1—OB19	2.613 (16)	OW9—OS14^ix	3.15 (4)
OB1—OS24	2.630 (14)	OW9—OH19^ii	3.50 (4)
OB1—OH25	2.71 (2)	OW10—Na3^vii	2.512 (18)
OB1—OH24^xii	2.85 (3)	OW10—OH18^i	2.917 (19)
OB1—OHT1	3.333 (16)	OW10—OH9^vii	3.114 (19)
OB1—OH2	3.37 (2)	OW10—OW18	3.12 (2)
OB1—OW34	3.446 (18)	OW10—OW26	3.22 (2)
OB2—OS8	2.596 (12)	OW10—OB29^ii	3.300 (18)
OB2—OH3	2.613 (13)	OW10—OB21^i	3.381 (18)
OB2—OS28	2.615 (12)	OW10—OH34^vii	3.499 (18)
OB2—OB6	2.638 (13)	OW10—OW39^i	3.52 (4)
OB2—OB3	2.675 (12)	OW10—OW22^vii	3.56 (3)
OB2—OS1	2.677 (12)	OW11—OW16	3.072 (15)
OB2—OW14^iii	3.425 (13)	OW12—OW33^vii	3.59 (5)
OB2—OW20	3.44 (2)	OW12—OH14^ii	3.78 (5)
OB2—OW13	3.567 (16)	OW12—OB35^ii	3.82 (5)
OB3—OH20	2.615 (13)	OW12—OH9^vii	3.85 (5)
OB3—OS8	2.630 (12)	OW12—OB29^ii	3.98 (5)
OB3—OB31	2.636 (12)	OW13—OW40^vii	2.68 (4)
OB3—OB4	2.657 (13)	OW13—OW21^iii	2.96 (2)
OB3—OS1	2.673 (12)	OW13—OW30^vii	3.00 (6)
OB3—Na6^vii	3.250 (14)	OW13—OH7^vii	3.024 (17)
OB3—OS28	3.512 (13)	OW13—OB28^iii	3.044 (17)
OB3—OS43	3.647 (12)	OW13—OW14^iii	3.188 (17)
OB4—OB37	2.597 (13)	OW13—OS33^iii	3.289 (16)
OB4—OB31	2.617 (13)	OW13—Na7^vii	3.65 (3)
OB4—OS41	2.629 (12)	OW14—OT1^ix	2.683 (13)
OB4—OH20	2.633 (12)	OW14—Ba^ix	2.818 (10)
OB4—OS9	2.697 (12)	OW14—OB22^ix	3.002 (13)
OB4—Na6^vii	2.930 (13)	OW14—OW13^ix	3.188 (17)
OB4—OW24^viii	3.231 (17)	OW14—OW21	3.23 (2)
OB4—OH5^vii	3.293 (13)	OW14—OS37^ix	3.264 (13)
OB4—OS6	3.348 (12)	OW14—OB23^ix	3.293 (14)
OB5—OB8	2.558 (13)	OW14—OS8^ix	3.415 (13)
OB5—OB30	2.609 (13)	OW14—OB2^ix	3.425 (13)
OB5—OS42	2.620 (12)	OW15—OH17^ix	2.97 (3)
OB5—OS17	2.638 (13)	OW15—OS10^ii	3.14 (3)
OB5—OS27	2.693 (12)	OW15—OH4^ix	3.29 (3)
OB5—OH17	2.701 (13)	OW15—OH20^viii	3.49 (3)
OB5—OW16	3.263 (15)	OW15—OS6^ix	3.55 (3)
OB5—OH4	3.354 (13)	OW15—OW24	3.66 (3)
OB6—OS44	2.617 (12)	OW15—OB9^ii	3.66 (3)
OB6—OS28	2.627 (13)	OW15—OW32^ix	3.66 (4)
OB6—OH3	2.629 (13)	OW16—OW17	3.377 (17)
OB6—OB22	2.639 (13)	OW17—OW19^iv	2.81 (4)
OB6—OH34	2.720 (15)	OW17—OW27	3.143 (15)
OB6—OW13	2.806 (16)	OW17—OW23	3.17 (2)
OB6—OW14^iii	3.441 (14)	OW18—Na3^vii	2.63 (2)
OB6—OH7^vii	3.469 (14)	OW18—OH16^vii	2.76 (2)
OB7—OH7	2.634 (15)	OW18—OB20^i	3.08 (2)
OB7—OB10	2.634 (14)	OW18—OH34^vii	3.41 (2)
OB7—OB12	2.636 (14)	OW18—Na13^i	3.59 (3)
OB7—OB26	2.656 (14)	OW18—OB19^i	3.60 (2)
OB7—OS11	2.662 (14)	OW18—Si35^vii	3.608 (18)
OB7—OS35	2.675 (14)	OW18—OS23^i	3.71 (2)
OB7—OW29	3.44 (2)	OW18—OW22^vii	3.71 (3)
OB7—OS4	3.445 (13)	OW19—OW35^x	2.39 (5)
OB7—OH3^vii	3.522 (14)	OW19—OW23^ii	2.44 (4)
OB8—OB27	2.555 (13)	OW19—OW6^ii	2.52 (6)
OB8—OH19	2.628 (14)	OW19—OH26^ii	2.71 (5)
OB8—OH17	2.653 (13)	OW19—OW17^ii	2.81 (4)
OB8—OS14	2.667 (13)	OW19—OH23^ii	3.22 (5)
OB8—OS42	2.673 (12)	OW19—Na11^ii	3.36 (4)
OB8—OW11	3.160 (13)	OW19—OB16^ii	3.60 (4)
OB8—OW27	3.210 (14)	OW19—Si40^ii	3.61 (4)
OB8—OHT3^iv	3.278 (13)	OW19—OH28^ii	3.77 (6)
OB9—OH21	2.567 (14)	OW20—Na6^vii	2.50 (2)
OB9—OS10	2.606 (12)	OW20—OW38^xviii	2.76 (4)
OB9—OB11	2.606 (13)	OW20—OH11^iii	3.21 (3)
OB9—OS20	2.645 (13)	OW20—OW28	3.23 (2)
OB9—OB18^x	2.658 (13)	OW20—OW24^iii	3.34 (2)
OB9—OS46	2.679 (12)	OW20—OH5^vii	3.91 (2)
OB9—Na4^iv	2.990 (12)	OW20—OB28^iii	4.11 (2)
OB9—OW24^iv	3.238 (18)	OW21—OW30^viii	2.09 (6)
OB9—OW28^xi	3.476 (14)	OW21—OW13^ix	2.96 (2)
OB9—Ti6^ii	3.618 (9)	OW21—OW4^viii	3.11 (4)
OB10—OS11	2.604 (13)	OW21—OB22^ix	3.46 (2)
OB10—OB29^ii	2.626 (15)	OW21—Na7^viii	3.72 (3)
OB10—OS40	2.644 (14)	OW22—OS25^xiii	3.04 (3)
OB10—OH6	2.654 (14)	OW22—OS34^xiii	3.14 (3)
OB10—OS35	2.671 (13)	OW22—OW22^xiii	3.27 (6)
OB10—OH34^vii	2.784 (14)	OW22—OW10^vii	3.56 (3)
OB10—OW10	3.287 (18)	OW22—OB24^xiii	3.59 (3)
OB10—OW26	3.615 (19)	OW22—OB21^xiii	3.60 (3)
OB11—OB30	2.623 (13)	OW22—OW18^vii	3.71 (3)
OB11—OH8	2.627 (15)	OW22—OW39^xiii	3.76 (5)
OB11—OB32	2.637 (14)	OW23—OW19^iv	2.44 (4)
OB11—OS46	2.665 (14)	OW23—OS4^iv	3.01 (2)
OB11—OS10	2.685 (13)	OW23—OB38^iv	3.36 (2)
OB11—OS15	3.436 (14)	OW23—OW35^xii	3.47 (3)
OB11—OS27	3.593 (13)	OW23—OW27	3.83 (2)
OB12—OH7	2.608 (14)	OW23—Ti3^iv	3.93 (2)
OB12—OB38	2.613 (14)	OW24—Na6^viii	2.335 (18)
OB12—OB26	2.615 (14)	OW24—OH21^ii	2.809 (18)
OB12—OS4	2.636 (13)	OW24—OS6^ix	3.063 (17)
OB12—OS2	2.683 (13)	OW24—OH5^ix	3.150 (18)
OB12—OS33	3.517 (13)	OW24—OH20^viii	3.210 (18)
OB12—OS12	3.647 (13)	OW24—OB4^viii	3.231 (17)
OB13—Si37	1.606 (8)	OW24—OB9^ii	3.238 (18)
OB13—Si38	1.627 (9)	OW24—OW20^ix	3.34 (2)
OB13—OB36	2.611 (12)	OW24—OW28^ix	3.467 (18)
OB13—OH30	2.62 (3)	OW24—Si21^ix	3.668 (16)
OB13—OS12	2.634 (12)	OW25—OW25^xiv	2.32 (4)
OB13—OB38	2.637 (13)	OW25—K1^xiv	2.40 (3)
OB13—OH22	2.644 (14)	OW25—OW9^xiv	2.41 (4)
OB13—OH33	2.65 (2)	OW25—OS14^ix	2.53 (2)
OB13—OH32	2.65 (3)	OW25—OH19^ii	2.68 (2)
OB13—OH29	2.68 (4)	OW25—OS14^ii	3.39 (2)
OB13—OW21	3.32 (2)	OW25—Ti8^ix	3.393 (19)
OB14—OB31	2.577 (12)	OW26—Na9^ii	2.67 (3)
OB14—OH13	2.608 (15)	OW26—OT4^i	2.731 (18)
OB14—OS43	2.611 (13)	OW26—OW1^ii	3.18 (5)
OB14—OB18	2.641 (13)	OW26—OS21^i	3.231 (18)
OB14—OS7	2.648 (13)	OW26—OB34^ii	3.262 (19)
OB14—OS48	2.657 (12)	OW26—OB29^ii	3.319 (19)
OB14—OW31^vii	2.92 (2)	OW26—OS23^i	3.402 (18)
OB14—OW34	3.592 (16)	OW26—OS15^ii	3.434 (18)
OB14—OH28^xii	3.90 (3)	OW26—OB15^ii	3.576 (19)
OB15—OB36	2.581 (13)	OW27—OHT3^iv	2.958 (13)
OB15—OS19	2.602 (15)	OW27—OS2^iv	3.234 (13)
OB15—OB34	2.610 (16)	OW27—OB38^iv	3.365 (14)
OB15—OB32	2.611 (14)	OW27—OH22^iv	3.499 (14)
OB15—OS15	2.615 (14)	OW27—Si6^iv	3.524 (10)
OB15—OS45	2.656 (14)	OW28—Na4^iii	2.604 (13)
OB15—OW6^ii	2.95 (4)	OW28—OT6^iii	2.731 (13)
OB15—OW26^iv	3.576 (19)	OW28—OS3^iii	3.260 (14)
OB16—Si40	1.662 (9)	OW28—OW38^xviii	3.27 (3)
OB16—OH26	2.59 (3)	OW28—OS46^xi	3.299 (14)
OB16—OB33	2.62 (2)	OW28—OHT4^xviii	3.300 (14)
OB16—OS13	2.686 (15)	OW28—OS10^xi	3.381 (14)
OB16—OH27^xii	2.69 (4)	OW28—OS36^iii	3.383 (14)
OB16—OS16	2.716 (15)	OW28—OS33^iii	3.463 (14)
OB16—OH12	2.768 (17)	OW28—OW24^iii	3.468 (18)
OB16—OH28	2.86 (3)	OW29—OH3^vii	2.71 (2)
OB16—OW17	3.009 (19)	OW29—OW33^vii	3.23 (3)
OB16—OW16	3.433 (17)	OW29—OS28^vii	3.47 (2)
OB16—OW23	3.45 (3)	OW29—Si33^vii	3.524 (18)
OB17—Si39	1.596 (9)	OW30—OW21^viii	2.09 (6)
OB17—Si39^xii	1.604 (18)	OW30—OW13^vii	3.00 (6)
OB17—OH24	2.53 (2)	OW30—OW40	3.41 (7)
OB17—OH24^xii	2.59 (2)	OW30—OB22^vii	3.50 (6)
OB17—OB17^xii	2.60 (2)	OW30—OH30^viii	3.76 (7)
OB17—OS39	2.616 (16)	OW30—OW40^viii	3.95 (7)
OB17—OH23^xii	2.63 (3)	OW31—OS43^vii	2.46 (2)
OB17—OS22	2.630 (14)	OW31—OH15^vii	2.63 (2)
OB17—OH12	2.633 (17)	OW31—OW34^vii	2.68 (2)
OB17—OH23	2.65 (3)	OW31—OS32^vii	2.71 (2)
OB17—K2^vi	3.249 (15)	OW31—OB14^vii	2.92 (2)
OB18—Si14^vi	1.648 (11)	OW31—Si27^vii	3.24 (2)
OB18—OH13	2.614 (16)	OW31—Si36^vii	3.29 (2)
OB18—OS7	2.622 (14)	OW31—Ti11^vii	3.47 (2)
OB18—OB9^vi	2.658 (13)	OW31—OT5^vii	3.70 (2)
OB18—OS20^vi	2.681 (15)	OW31—OW36^vii	4.00 (3)
OB18—OH21^vi	2.698 (15)	OW31—OS48^vii	4.07 (2)
OB18—OB31	3.253 (14)	OW31—OH14^xviii	4.23 (3)
OB18—OB11^vi	3.610 (13)	OW32—OH20^vii	3.02 (3)
OB18—OW35	3.66 (3)	OW32—OW15^iii	3.66 (4)
OB19—OS23	2.576 (14)	OW32—OB3^vii	4.28 (3)
OB19—OB20	2.589 (14)	OW33—Na15^vii	2.40 (3)
OB19—OS24	2.644 (14)	OW33—OH28^xix	2.90 (4)
OB19—OS21	2.670 (14)	OW33—OS40^vii	2.93 (2)
OB19—OH2	2.671 (19)	OW33—OS13^xix	3.07 (2)
OB19—Na8^v	3.246 (16)	OW33—OW29^vii	3.23 (3)
OB19—Na9^iv	3.52 (2)	OW33—OW2^vii	3.51 (6)
OB19—OW18^v	3.60 (2)	OW33—OW12^vii	3.59 (5)
OB19—OW26^v	3.641 (19)	OW33—OB33^xix	3.64 (2)
OB20—OB21	2.593 (16)	OW33—Ti3^vii	3.93 (2)
OB20—OS25	2.638 (13)	OW33—OW23^xix	3.94 (3)
OB20—OS24	2.665 (14)	OW33—OH6^vii	3.97 (2)
OB20—OS47	2.699 (13)	OW33—Na1^vii	3.99 (2)
OB20—OW36	2.87 (2)	OW34—OW36	2.51 (2)
OB20—OW18^v	3.08 (2)	OW34—OW31^vii	2.68 (2)
OB20—OW34	3.485 (16)	OW35—OW19^vi	2.39 (5)
OB20—OH31	3.60 (6)	OW35—OS15^vi	2.69 (2)
OB21—OH18	2.628 (15)	OW35—Na9^vi	3.21 (3)
OB21—OB24	2.637 (15)	OW35—OS20^vi	3.31 (2)
OB21—OS25	2.640 (13)	OW35—OB32^vi	3.41 (2)
OB21—OB25	2.646 (14)	OW35—OW23^xii	3.47 (3)
OB21—OS47	2.698 (13)	OW35—Si12^vi	3.48 (2)
OB21—OW1^iv	3.33 (5)	OW35—OW6^xii	3.58 (5)
OB21—OW10^v	3.381 (18)	OW35—OH26^xii	3.82 (4)
OB21—OS38	3.457 (14)	OW35—OB15^vi	3.85 (3)
OB22—OS44	2.620 (13)	OW37—OH29^iv	2.71 (6)
OB22—OS34	2.634 (13)	OW37—OW1^iv	2.86 (5)
OB22—OB23	2.634 (13)	OW37—OB34^iv	2.895 (18)
OB22—OH34	2.640 (14)	OW37—OB36^iv	3.452 (19)
OB22—OH16	2.649 (14)	OW37—Si38^iv	3.63 (2)
OB22—OW14^iii	3.002 (13)	OW37—OH22^iv	3.678 (18)
OB22—Na7^vii	3.01 (2)	OW37—OW26^v	4.00 (2)
OB22—OW21^iii	3.46 (2)	OW37—OB15^iv	4.072 (18)
OB22—OW30^vii	3.50 (6)	OW38—OH11^v	2.74 (4)
OB23—OS37	2.587 (13)	OW38—OW20^xvii	2.76 (4)
OB23—OB24	2.615 (14)	OW38—OW3^xii	2.96 (4)
OB23—OS34	2.627 (14)	OW38—OH21^iv	3.24 (4)
OB23—OS31	2.643 (12)	OW38—OW28^xvii	3.27 (3)
OB23—OH16	2.666 (14)	OW38—Si3^v	3.64 (3)
OB23—Na2^iii	3.022 (13)	OW38—OS18^v	3.64 (4)
OB23—OW14^iii	3.293 (14)	OW38—OW24^v	3.93 (4)
OB23—OW21^iii	3.94 (2)	OW38—OS20^iv	4.05 (4)
OB24—OS31	2.637 (12)	OW38—OB28^v	4.08 (4)
OB24—OS37	2.640 (13)	OW39—OH9^xiii	2.77 (4)
OB24—OH18	2.651 (15)	OW39—OW10^v	3.52 (4)
OB24—OB25	2.672 (14)	OW39—OH15^xiii	3.65 (4)
OB24—OS25	3.478 (14)	OW39—Na13^xiii	3.71 (5)
OB24—OS34	3.574 (13)	OW39—OW22^xiii	3.76 (5)
OB24—OW22^xiii	3.59 (3)	OW39—Na3^xiii	4.10 (4)
OB25—OB27	2.589 (13)	OW39—OS26^xiii	4.42 (4)
OB25—OH18	2.639 (15)	OW39—OH6^v	4.43 (4)
OB25—OS49	2.659 (13)	OW40—OW40^viii	1.01 (8)
OB25—OS38	2.663 (14)	OW40—OW13^vii	2.68 (4)
OB25—OW37	3.229 (18)	OW40—OB26^viii	2.77 (5)
OB25—OW1^iv	3.31 (5)	OW40—OH10^viii	2.82 (5)
OB25—OS37	3.463 (14)	OW40—OB28^viii	3.18 (5)
OB25—OS14	3.515 (13)	OW40—OH7^viii	3.48 (5)
OB26—OH7	2.613 (14)	OW40—Si4^viii	3.55 (5)
OB26—OW40	2.63 (5)	Si37—Si38	0.833 (16)
OB26—OB28	2.635 (13)	Si37—OW4^viii	3.52 (4)
OB26—OS33	2.667 (13)	Si38—OW37^ii	3.63 (2)
OB26—OS36	2.702 (14)	Si39—OB17^xii	1.604 (18)
OB26—OW40^viii	2.77 (5)	Si39—Si39^xii	1.87 (3)
OB26—OS11	3.535 (15)	Si39—OH24^xii	2.97 (3)
OB27—OS38	2.607 (13)	Si39—OH23^xii	3.10 (3)
OB27—OS14	2.613 (13)	Si39—K2^iv	3.277 (16)
OB27—OH19	2.666 (13)	Si39—OHT1^xii	3.588 (15)
OB27—OS49	2.705 (12)	Si39—OS22^xii	3.619 (15)
OB27—OH22^iv	3.277 (13)	Si40—OH27^xii	1.51 (3)
OB27—OW17	3.402 (15)	Si40—OH13^xii	3.414 (18)
OB28—OS33	2.561 (13)	Si40—OH25^xii	3.50 (3)
OB28—OS18	2.596 (14)	Si40—OW19^iv	3.61 (4)
OB28—OH11	2.65 (2)	Si41—OH24^xii	3.17 (3)
OB28—OH10	2.67 (2)	Si41—OB33^xii	3.460 (17)
OB28—OS36	2.691 (13)
OT6—Ce1—OT4^i	120.2 (3)	Si31—OS21—K2^iv	94.5 (5)
OT6—Ce1—OT3^ii	118.2 (3)	Ti6—OS21—K2^iv	101.5 (5)
OT4^i—Ce1—OT3^ii	121.6 (3)	Na9^iv—OS21—K2^iv	110.4 (8)
OT6—Ce1—OS45^ii	134.6 (3)	OH2—OS21—K2^iv	59.9 (5)
OT4^i—Ce1—OS45^ii	75.6 (3)	OB19—OS21—K2^iv	98.6 (4)
OT3^ii—Ce1—OS45^ii	63.7 (3)	OS15^iv—OS21—K2^iv	108.5 (5)
OT6—Ce1—OS35	135.9 (3)	OS23—OS21—K2^iv	121.2 (5)
OT4^i—Ce1—OS35	74.7 (3)	OS20^iv—OS21—K2^iv	56.4 (4)
OT3^ii—Ce1—OS35	64.3 (3)	OHT4—OS21—K2^iv	95.3 (5)
OS45^ii—Ce1—OS35	87.9 (3)	OT4—OS21—K2^iv	141.9 (5)
OT6—Ce1—OS46^ii	73.5 (3)	Si31—OS21—OW26^v	89.4 (5)
OT4^i—Ce1—OS46^ii	64.4 (3)	Ti6—OS21—OW26^v	89.9 (4)
OT3^ii—Ce1—OS46^ii	135.7 (3)	Na9^iv—OS21—OW26^v	54.3 (7)
OS45^ii—Ce1—OS46^ii	78.2 (3)	OH2—OS21—OW26^v	126.2 (6)
OS35—Ce1—OS46^ii	138.8 (3)	OB19—OS21—OW26^v	75.5 (5)
OT6—Ce1—OS36	75.0 (3)	OS15^iv—OS21—OW26^v	70.4 (4)
OT4^i—Ce1—OS36	63.9 (3)	OS23—OS21—OW26^v	69.4 (4)
OT3^ii—Ce1—OS36	135.2 (3)	OS20^iv—OS21—OW26^v	131.7 (5)
OS45^ii—Ce1—OS36	139.1 (3)	OHT4—OS21—OW26^v	101.5 (5)
OS35—Ce1—OS36	77.1 (3)	OT4—OS21—OW26^v	53.1 (4)
OS46^ii—Ce1—OS36	88.5 (3)	K2^iv—OS21—OW26^v	163.1 (6)
OT6—Ce1—OS2	63.3 (3)	Si20—OS22—Ti7	127.8 (6)
OT4^i—Ce1—OS2	134.2 (3)	Si20—OS22—OH12	35.0 (4)
OT3^ii—Ce1—OS2	74.8 (3)	Ti7—OS22—OH12	152.7 (6)
OS45^ii—Ce1—OS2	138.3 (3)	Si20—OS22—OS39	35.2 (4)
OS35—Ce1—OS2	77.1 (3)	Ti7—OS22—OS39	95.3 (4)
OS46^ii—Ce1—OS2	136.3 (3)	OH12—OS22—OS39	60.5 (4)
OS36—Ce1—OS2	75.2 (3)	Si20—OS22—OB17	36.1 (4)
OT6—Ce1—OS27^ii	63.0 (3)	Ti7—OS22—OB17	120.6 (5)
OT4^i—Ce1—OS27^ii	134.4 (3)	OH12—OS22—OB17	60.4 (4)
OT3^ii—Ce1—OS27^ii	74.3 (3)	OS39—OS22—OB17	59.9 (4)
OS45^ii—Ce1—OS27^ii	76.0 (3)	Si20—OS22—OS7	135.4 (6)
OS35—Ce1—OS27^ii	138.4 (3)	Ti7—OS22—OS7	45.6 (3)
OS46^ii—Ce1—OS27^ii	75.4 (3)	OH12—OS22—OS7	158.7 (5)
OS36—Ce1—OS27^ii	137.7 (3)	OS39—OS22—OS7	124.5 (5)
OS2—Ce1—OS27^ii	89.9 (3)	OB17—OS22—OS7	102.5 (5)
OT6—Ce1—Ti5^ii	129.86 (19)	Si20—OS22—OS9	152.2 (6)
OT4^i—Ce1—Ti5^ii	102.9 (2)	Ti7—OS22—OS9	45.3 (3)
OT3^ii—Ce1—Ti5^ii	30.4 (2)	OH12—OS22—OS9	134.3 (5)
OS45^ii—Ce1—Ti5^ii	33.7 (2)	OS39—OS22—OS9	120.7 (5)
OS35—Ce1—Ti5^ii	76.5 (2)	OB17—OS22—OS9	164.8 (5)
OS46^ii—Ce1—Ti5^ii	107.5 (2)	OS7—OS22—OS9	64.0 (3)
OS36—Ce1—Ti5^ii	152.9 (2)	Si20—OS22—K2^vi	104.8 (5)
OS2—Ce1—Ti5^ii	104.65 (19)	Ti7—OS22—K2^vi	105.5 (5)
OS27^ii—Ce1—Ti5^ii	68.82 (18)	OH12—OS22—K2^vi	100.8 (5)
OT6—Ce1—Ti6^i	99.9 (2)	OS39—OS22—K2^vi	133.7 (5)
OT4^i—Ce1—Ti6^i	30.4 (2)	OB17—OS22—K2^vi	74.0 (4)
OT3^ii—Ce1—Ti6^i	135.0 (2)	OS7—OS22—K2^vi	60.0 (4)
OS45^ii—Ce1—Ti6^i	72.8 (2)	OS9—OS22—K2^vi	102.7 (4)
OS35—Ce1—Ti6^i	104.8 (2)	Si20—OS22—OHT1	86.8 (5)
OS46^ii—Ce1—Ti6^i	34.0 (2)	Ti7—OS22—OHT1	44.6 (3)
OS36—Ce1—Ti6^i	74.7 (2)	OH12—OS22—OHT1	120.9 (5)
OS2—Ce1—Ti6^i	148.51 (19)	OS39—OS22—OHT1	63.1 (4)
OS27^ii—Ce1—Ti6^i	106.35 (19)	OB17—OS22—OHT1	77.3 (4)
Ti5^ii—Ce1—Ti6^i	106.33 (6)	OS7—OS22—OHT1	61.6 (3)
OT6—Ce1—Ti3	130.3 (2)	OS9—OS22—OHT1	89.6 (4)
OT4^i—Ce1—Ti3	102.7 (2)	K2^vi—OS22—OHT1	105.1 (5)
OT3^ii—Ce1—Ti3	30.8 (2)	Si20—OS22—OT2	96.7 (5)
OS45^ii—Ce1—Ti3	76.6 (2)	Ti7—OS22—OT2	42.1 (3)
OS35—Ce1—Ti3	34.0 (2)	OH12—OS22—OT2	110.9 (5)
OS46^ii—Ce1—Ti3	154.0 (2)	OS39—OS22—OT2	61.6 (3)
OS36—Ce1—Ti3	106.5 (2)	OB17—OS22—OT2	114.3 (5)
OS2—Ce1—Ti3	69.20 (19)	OS7—OS22—OT2	87.2 (4)
OS27^ii—Ce1—Ti3	104.52 (19)	OS9—OS22—OT2	60.5 (3)
Ti5^ii—Ce1—Ti3	51.15 (6)	K2^vi—OS22—OT2	147.1 (5)
Ti6^i—Ce1—Ti3	129.00 (6)	OHT1—OS22—OT2	51.1 (3)
OT2—Ce2—OT1	118.7 (3)	Si20—OS22—OW3	109.9 (6)
OT2—Ce2—OT5	119.7 (3)	Ti7—OS22—OW3	110.3 (5)
OT1—Ce2—OT5	121.5 (3)	OH12—OS22—OW3	75.4 (5)
OT2—Ce2—OS41	73.6 (3)	OS39—OS22—OW3	118.9 (6)
OT1—Ce2—OS41	63.9 (3)	OB17—OS22—OW3	129.1 (6)
OT5—Ce2—OS41	134.4 (3)	OS7—OS22—OW3	112.2 (5)
OT2—Ce2—OS31	136.0 (3)	OS9—OS22—OW3	65.2 (4)
OT1—Ce2—OS31	75.1 (3)	K2^vi—OS22—OW3	92.2 (5)
OT5—Ce2—OS31	64.4 (3)	OHT1—OS22—OW3	152.3 (5)
OS41—Ce2—OS31	138.6 (3)	OT2—OS22—OW3	103.6 (5)
OT2—Ce2—OS1	132.9 (3)	Si20—OS22—Ti12	67.6 (4)
OT1—Ce2—OS1	77.2 (3)	Ti7—OS22—Ti12	61.6 (3)
OT5—Ce2—OS1	63.0 (3)	OH12—OS22—Ti12	93.6 (4)
OS41—Ce2—OS1	76.5 (3)	OS39—OS22—Ti12	33.7 (2)
OS31—Ce2—OS1	89.8 (3)	OB17—OS22—Ti12	80.4 (4)
OT2—Ce2—OS47	64.1 (3)	OS7—OS22—Ti12	96.0 (3)
OT1—Ce2—OS47	134.2 (3)	OS9—OS22—Ti12	93.7 (3)
OT5—Ce2—OS47	75.3 (3)	K2^vi—OS22—Ti12	138.8 (4)
OS41—Ce2—OS47	137.4 (3)	OHT1—OS22—Ti12	36.8 (2)
OS31—Ce2—OS47	76.8 (3)	OT2—OS22—Ti12	34.0 (2)
OS1—Ce2—OS47	137.9 (3)	OW3—OS22—Ti12	128.9 (5)
OT2—Ce2—OS49	74.4 (3)	Si31—OS23—Ti4^v	122.8 (7)
OT1—Ce2—OS49	63.1 (3)	Si31—OS23—Na14^v	114.4 (6)
OT5—Ce2—OS49	136.0 (3)	Ti4^v—OS23—Na14^v	102.1 (6)
OS41—Ce2—OS49	88.7 (3)	Si31—OS23—Na8^v	112.2 (6)
OS31—Ce2—OS49	77.1 (3)	Ti4^v—OS23—Na8^v	101.9 (5)
OS1—Ce2—OS49	140.2 (3)	Na14^v—OS23—Na8^v	100.3 (6)
OS47—Ce2—OS49	75.8 (3)	Si31—OS23—OB19	37.2 (4)
OT2—Ce2—OS48	63.6 (3)	Ti4^v—OS23—OB19	152.0 (6)
OT1—Ce2—OS48	136.0 (3)	Na14^v—OS23—OB19	105.1 (6)
OT5—Ce2—OS48	73.1 (3)	Na8^v—OS23—OB19	79.6 (5)
OS41—Ce2—OS48	77.0 (3)	Si31—OS23—OS11^v	149.3 (7)
OS31—Ce2—OS48	137.2 (3)	Ti4^v—OS23—OS11^v	47.7 (3)
OS1—Ce2—OS48	74.8 (3)	Na14^v—OS23—OS11^v	96.1 (6)
OS47—Ce2—OS48	88.3 (3)	Na8^v—OS23—OS11^v	56.1 (4)
OS49—Ce2—OS48	137.9 (3)	OB19—OS23—OS11^v	133.8 (6)
OT2—Ce2—Ti12	30.7 (2)	Si31—OS23—OS18^v	132.3 (7)
OT1—Ce2—Ti12	129.9 (2)	Ti4^v—OS23—OS18^v	46.6 (3)
OT5—Ce2—Ti12	101.94 (19)	Na14^v—OS23—OS18^v	56.3 (5)
OS41—Ce2—Ti12	103.6 (2)	Na8^v—OS23—OS18^v	115.4 (6)
OS31—Ce2—Ti12	106.8 (2)	OB19—OS23—OS18^v	156.6 (6)
OS1—Ce2—Ti12	150.57 (19)	OS11^v—OS23—OS18^v	67.0 (4)
OS47—Ce2—Ti12	33.8 (2)	Si31—OS23—OS21	34.6 (4)
OS49—Ce2—Ti12	68.58 (19)	Ti4^v—OS23—OS21	92.7 (5)
OS48—Ce2—Ti12	76.60 (19)	Na14^v—OS23—OS21	145.0 (6)
OT2—Ce2—Ti9	100.01 (19)	Na8^v—OS23—OS21	107.4 (5)
OT1—Ce2—Ti9	30.19 (19)	OB19—OS23—OS21	60.8 (4)
OT5—Ce2—Ti9	132.85 (19)	OS11^v—OS23—OS21	116.9 (5)
OS41—Ce2—Ti9	33.91 (18)	OS18^v—OS23—OS21	124.7 (5)
OS31—Ce2—Ti9	104.7 (2)	Si31—OS23—OH2	33.6 (4)
OS1—Ce2—Ti9	71.67 (19)	Ti4^v—OS23—OH2	115.9 (6)
OS47—Ce2—Ti9	150.2 (2)	Na14^v—OS23—OH2	86.5 (6)
OS49—Ce2—Ti9	75.61 (19)	Na8^v—OS23—OH2	139.4 (6)
OS48—Ce2—Ti9	107.61 (19)	OB19—OS23—OH2	60.1 (5)
Ti12—Ce2—Ti9	124.50 (6)	OS11^v—OS23—OH2	163.6 (6)
OT2—Ce2—Ti7	30.1 (2)	OS18^v—OS23—OH2	101.8 (6)
OT1—Ce2—Ti7	132.5 (2)	OS21—OS23—OH2	58.5 (4)
OT5—Ce2—Ti7	99.5 (2)	Si31—OS23—OHT4	81.6 (5)
OS41—Ce2—Ti7	70.56 (19)	Ti4^v—OS23—OHT4	44.2 (3)
OS31—Ce2—Ti7	150.6 (2)	Na14^v—OS23—OHT4	109.6 (5)
OS1—Ce2—Ti7	105.1 (2)	Na8^v—OS23—OHT4	138.0 (5)
OS47—Ce2—Ti7	75.2 (2)	OB19—OS23—OHT4	118.2 (5)
OS49—Ce2—Ti7	104.4 (2)	OS11^v—OS23—OHT4	91.2 (4)
OS48—Ce2—Ti7	33.55 (19)	OS18^v—OS23—OHT4	63.5 (4)
Ti12—Ce2—Ti7	50.01 (6)	OS21—OS23—OHT4	61.3 (4)
Ti9—Ce2—Ti7	104.10 (6)	OH2—OS23—OHT4	72.7 (5)
OW14^iii—Ba—OW28	138.4 (3)	Si31—OS23—OT4	94.8 (5)
OW14^iii—Ba—OS3^iii	74.3 (3)	Ti4^v—OS23—OT4	41.3 (3)
OW28—Ba—OS3^iii	70.2 (3)	Na14^v—OS23—OT4	143.3 (6)
OW14^iii—Ba—OW13	68.2 (3)	Na8^v—OS23—OT4	87.5 (4)
OW28—Ba—OW13	135.4 (3)	OB19—OS23—OT4	111.6 (5)
OS3^iii—Ba—OW13	140.4 (3)	OS11^v—OS23—OT4	58.8 (3)
OW14^iii—Ba—OS8	73.3 (3)	OS18^v—OS23—OT4	87.8 (4)
OW28—Ba—OS8	102.0 (3)	OS21—OS23—OT4	60.3 (4)
OS3^iii—Ba—OS8	54.6 (2)	OH2—OS23—OT4	110.6 (5)
OW13—Ba—OS8	122.1 (3)	OHT4—OS23—OT4	51.0 (3)
OW14^iii—Ba—OB28^iii	128.5 (3)	Si31—OS23—OW26^v	84.0 (5)
OW28—Ba—OB28^iii	75.0 (3)	Ti4^v—OS23—OW26^v	86.5 (4)
OS3^iii—Ba—OB28^iii	142.3 (3)	Na14^v—OS23—OW26^v	148.6 (6)
OW13—Ba—OB28^iii	63.6 (3)	Na8^v—OS23—OW26^v	48.2 (4)
OS8—Ba—OB28^iii	150.4 (3)	OB19—OS23—OW26^v	73.6 (4)
OW14^iii—Ba—OS29^iii	65.4 (3)	OS11^v—OS23—OW26^v	67.4 (4)
OW28—Ba—OS29^iii	76.5 (3)	OS18^v—OS23—OW26^v	129.8 (5)
OS3^iii—Ba—OS29^iii	54.5 (2)	OS21—OS23—OW26^v	62.8 (4)
OW13—Ba—OS29^iii	97.2 (3)	OH2—OS23—OW26^v	117.1 (6)
OS8—Ba—OS29^iii	104.2 (2)	OHT4—OS23—OW26^v	97.8 (5)
OB28^iii—Ba—OS29^iii	103.6 (2)	OT4—OS23—OW26^v	50.4 (4)
OW14^iii—Ba—OB2	72.5 (3)	Si30—OS24—Ti12	134.1 (6)
OW28—Ba—OB2	137.7 (3)	Si30—OS24—OB1	33.6 (4)
OS3^iii—Ba—OB2	105.4 (2)	Ti12—OS24—OB1	120.4 (5)
OW13—Ba—OB2	75.3 (3)	Si30—OS24—OB19	35.1 (3)
OS8—Ba—OB2	52.5 (2)	Ti12—OS24—OB19	162.2 (6)
OB28^iii—Ba—OB2	110.1 (3)	OB1—OS24—OB19	59.4 (4)
OS29^iii—Ba—OB2	136.8 (2)	Si30—OS24—OB20	34.7 (3)
OW14^iii—Ba—OS33^iii	94.8 (3)	Ti12—OS24—OB20	105.3 (4)
OW28—Ba—OS33^iii	73.3 (3)	OB1—OS24—OB20	58.4 (5)
OS3^iii—Ba—OS33^iii	103.3 (2)	OB19—OS24—OB20	58.4 (4)
OW13—Ba—OS33^iii	68.5 (3)	Si30—OS24—OS39	160.3 (6)
OS8—Ba—OS33^iii	156.7 (2)	Ti12—OS24—OS39	44.5 (3)
OB28^iii—Ba—OS33^iii	51.7 (2)	OB1—OS24—OS39	126.7 (6)
OS29^iii—Ba—OS33^iii	52.5 (2)	OB19—OS24—OS39	152.2 (5)
OB2—Ba—OS33^iii	143.8 (2)	OB20—OS24—OS39	149.5 (5)
OW14^iii—Ba—OW20	135.0 (4)	Si30—OS24—OHT1	102.5 (5)
OW28—Ba—OW20	67.5 (4)	Ti12—OS24—OHT1	47.2 (3)
OS3^iii—Ba—OW20	91.4 (4)	OB1—OS24—OHT1	75.8 (4)
OW13—Ba—OW20	124.2 (4)	OB19—OS24—OHT1	135.0 (5)
OS8—Ba—OW20	64.0 (4)	OB20—OS24—OHT1	95.8 (4)
OB28^iii—Ba—OW20	88.5 (4)	OS39—OS24—OHT1	61.8 (3)
OS29^iii—Ba—OW20	137.5 (4)	Si30—OS24—OS47	91.5 (5)
OB2—Ba—OW20	70.6 (4)	Ti12—OS24—OS47	46.4 (3)
OS33^iii—Ba—OW20	130.2 (4)	OB1—OS24—OS47	96.8 (5)
OW14^iii—Ba—Si7^iii	67.2 (2)	OB19—OS24—OS47	116.3 (5)
OW28—Ba—Si7^iii	71.3 (2)	OB20—OS24—OS47	59.2 (3)
OS3^iii—Ba—Si7^iii	27.28 (18)	OS39—OS24—OS47	90.9 (4)
OW13—Ba—Si7^iii	120.2 (3)	OHT1—OS24—OS47	62.1 (3)
OS8—Ba—Si7^iii	79.14 (17)	Si30—OS24—OS38	138.6 (6)
OB28^iii—Ba—Si7^iii	125.28 (19)	Ti12—OS24—OS38	41.0 (3)
OS29^iii—Ba—Si7^iii	27.25 (18)	OB1—OS24—OS38	154.8 (5)
OB2—Ba—Si7^iii	123.91 (18)	OB19—OS24—OS38	131.4 (5)
OS33^iii—Ba—Si7^iii	77.75 (17)	OB20—OS24—OS38	105.1 (5)
OW20—Ba—Si7^iii	115.5 (4)	OS39—OS24—OS38	57.1 (3)
OW14^iii—Ba—Si4^iii	116.3 (2)	OHT1—OS24—OS38	88.3 (4)
OW28—Ba—Si4^iii	67.5 (2)	OS47—OS24—OS38	58.3 (3)
OS3^iii—Ba—Si4^iii	121.07 (18)	Si30—OS24—Si28	66.3 (4)
OW13—Ba—Si4^iii	68.1 (3)	Ti12—OS24—Si28	76.9 (3)
OS8—Ba—Si4^iii	169.06 (19)	OB1—OS24—Si28	84.9 (4)
OB28^iii—Ba—Si4^iii	26.76 (19)	OB19—OS24—Si28	85.5 (4)
OS29^iii—Ba—Si4^iii	76.82 (18)	OB20—OS24—Si28	31.6 (3)
OB2—Ba—Si4^iii	133.53 (18)	OS39—OS24—Si28	120.8 (4)
OS33^iii—Ba—Si4^iii	25.75 (18)	OHT1—OS24—Si28	86.7 (3)
OW20—Ba—Si4^iii	107.7 (4)	OS47—OS24—Si28	31.2 (2)
Si7^iii—Ba—Si4^iii	99.37 (9)	OS38—OS24—Si28	74.7 (3)
OS10^ii—Ti1—OS42^ii	100.0 (4)	Si30—OS24—OH23	109.7 (9)
OS10^ii—Ti1—OT6	92.4 (4)	Ti12—OS24—OH23	107.4 (8)
OS42^ii—Ti1—OT6	166.1 (4)	OB1—OS24—OH23	92.4 (9)
OS10^ii—Ti1—OS30	89.0 (4)	OB19—OS24—OH23	90.2 (8)
OS42^ii—Ti1—OS30	89.5 (4)	OB20—OS24—OH23	144.3 (9)
OT6—Ti1—OS30	97.1 (4)	OS39—OS24—OH23	63.6 (8)
OS10^ii—Ti1—OS27^ii	89.2 (4)	OHT1—OS24—OH23	96.0 (6)
OS42^ii—Ti1—OS27^ii	88.9 (3)	OS47—OS24—OH23	153.0 (8)
OT6—Ti1—OS27^ii	84.9 (4)	OS38—OS24—OH23	108.8 (9)
OS30—Ti1—OS27^ii	177.4 (4)	Si28—OS24—OH23	175.6 (8)
OS10^ii—Ti1—OHT3	167.1 (4)	Si30—OS24—OW1^iv	101.7 (10)
OS42^ii—Ti1—OHT3	92.9 (4)	Ti12—OS24—OW1^iv	100.2 (9)
OT6—Ti1—OHT3	75.0 (4)	OB1—OS24—OW1^iv	133.6 (9)
OS30—Ti1—OHT3	90.0 (4)	OB19—OS24—OW1^iv	75.0 (9)
OS27^ii—Ti1—OHT3	92.2 (4)	OB20—OS24—OW1^iv	91.7 (9)
OS10^ii—Ti1—Ti2	126.2 (3)	OS39—OS24—OW1^iv	97.5 (9)
OS42^ii—Ti1—Ti2	133.0 (3)	OHT1—OS24—OW1^iv	147.4 (9)
OT6—Ti1—Ti2	36.8 (3)	OS47—OS24—OW1^iv	95.8 (9)
OS30—Ti1—Ti2	83.7 (3)	OS38—OS24—OW1^iv	59.2 (9)
OS27^ii—Ti1—Ti2	98.9 (3)	Si28—OS24—OW1^iv	83.4 (9)
OHT3—Ti1—Ti2	40.9 (2)	OH23—OS24—OW1^iv	96.1 (10)
OS10^ii—Ti1—Na12	75.9 (5)	Si28—OS25—Ti10	134.7 (6)
OS42^ii—Ti1—Na12	49.4 (4)	Si28—OS25—OB20	36.7 (3)
OT6—Ti1—Na12	141.6 (4)	Ti10—OS25—OB20	154.3 (5)
OS30—Ti1—Na12	47.3 (4)	Si28—OS25—OB21	35.6 (3)
OS27^ii—Ti1—Na12	130.3 (4)	Ti10—OS25—OB21	132.6 (5)
OHT3—Ti1—Na12	112.4 (5)	OB20—OS25—OB21	58.9 (4)
Ti2—Ti1—Na12	128.3 (4)	Si28—OS25—OS26	154.2 (6)
OS10^ii—Ti1—OS29	113.7 (3)	Ti10—OS25—OS26	44.9 (3)
OS42^ii—Ti1—OS29	124.0 (3)	OB20—OS25—OS26	128.2 (5)
OT6—Ti1—OS29	54.7 (3)	OB21—OS25—OS26	170.2 (5)
OS30—Ti1—OS29	50.1 (3)	Si28—OS25—OW36	97.9 (6)
OS27^ii—Ti1—OS29	132.5 (3)	Ti10—OS25—OW36	102.7 (5)
OHT3—Ti1—OS29	56.9 (3)	OB20—OS25—OW36	65.0 (5)
Ti2—Ti1—OS29	33.79 (15)	OB21—OS25—OW36	123.0 (6)
Na12—Ti1—OS29	96.4 (4)	OS26—OS25—OW36	63.2 (5)
OS10^ii—Ti1—OS46^ii	46.2 (3)	Si28—OS25—OS47	33.4 (3)
OS42^ii—Ti1—OS46^ii	129.9 (3)	Ti10—OS25—OS47	102.7 (4)
OT6—Ti1—OS46^ii	56.5 (3)	OB20—OS25—OS47	60.4 (3)
OS30—Ti1—OS46^ii	119.0 (3)	OB21—OS25—OS47	60.4 (3)
OS27^ii—Ti1—OS46^ii	60.8 (3)	OS26—OS25—OS47	128.0 (5)
OHT3—Ti1—OS46^ii	124.5 (3)	OW36—OS25—OS47	100.1 (5)
Ti2—Ti1—OS46^ii	92.88 (17)	Si28—OS25—OS31	92.4 (4)
Na12—Ti1—OS46^ii	122.1 (4)	Ti10—OS25—OS31	48.5 (3)
OS29—Ti1—OS46^ii	105.1 (2)	OB20—OS25—OS31	128.4 (4)
OS10^ii—Ti1—Ce1	87.5 (3)	OB21—OS25—OS31	84.9 (4)
OS42^ii—Ti1—Ce1	133.6 (3)	OS26—OS25—OS31	93.4 (4)
OT6—Ti1—Ce1	39.9 (3)	OW36—OS25—OS31	142.3 (6)
OS30—Ti1—Ce1	136.6 (3)	OS47—OS25—OS31	70.2 (3)
OS27^ii—Ti1—Ce1	45.2 (2)	Si28—OS25—OT5	101.1 (5)
OHT3—Ti1—Ce1	84.4 (3)	Ti10—OS25—OT5	42.8 (3)
Ti2—Ti1—Ce1	64.34 (6)	OB20—OS25—OT5	111.8 (4)
Na12—Ti1—Ce1	163.1 (4)	OB21—OS25—OT5	124.3 (4)
OS29—Ti1—Ce1	92.68 (15)	OS26—OS25—OT5	61.8 (3)
OS46^ii—Ti1—Ce1	41.37 (14)	OW36—OS25—OT5	84.6 (5)
OS10^ii—Ti1—OB5^ii	103.3 (3)	OS47—OS25—OT5	68.2 (3)
OS42^ii—Ti1—OB5^ii	43.3 (3)	OS31—OS25—OT5	57.8 (3)
OT6—Ti1—OB5^ii	127.4 (3)	Si28—OS25—OS34	143.5 (6)
OS30—Ti1—OB5^ii	132.4 (3)	Ti10—OS25—OS34	39.0 (3)
OS27^ii—Ti1—OB5^ii	46.3 (3)	OB20—OS25—OS34	166.7 (5)
OHT3—Ti1—OB5^ii	86.8 (3)	OB21—OS25—OS34	114.0 (5)
Ti2—Ti1—OB5^ii	120.48 (17)	OS26—OS25—OS34	57.5 (4)
Na12—Ti1—OB5^ii	91.0 (3)	OW36—OS25—OS34	118.5 (5)
OS29—Ti1—OB5^ii	143.0 (2)	OS47—OS25—OS34	128.0 (4)
OS46^ii—Ti1—OB5^ii	101.3 (2)	OS31—OS25—OS34	57.8 (3)
Ce1—Ti1—OB5^ii	90.31 (15)	OT5—OS25—OS34	81.5 (3)
OT6—Ti2—OS33	95.5 (4)	Si28—OS25—OW22^xiii	110.4 (7)
OT6—Ti2—OS29	93.8 (4)	Ti10—OS25—OW22^xiii	101.5 (7)
OS33—Ti2—OS29	85.9 (4)	OB20—OS25—OW22^xiii	103.7 (7)
OT6—Ti2—OS12	164.7 (4)	OB21—OS25—OW22^xiii	78.4 (6)
OS33—Ti2—OS12	99.1 (4)	OS26—OS25—OW22^xiii	92.6 (6)
OS29—Ti2—OS12	91.8 (4)	OW36—OS25—OW22^xiii	106.9 (7)
OT6—Ti2—OHT3	76.2 (4)	OS47—OS25—OW22^xiii	138.4 (7)
OS33—Ti2—OHT3	171.7 (4)	OS31—OS25—OW22^xiii	103.1 (6)
OS29—Ti2—OHT3	93.5 (4)	OT5—OS25—OW22^xiii	144.2 (7)
OS12—Ti2—OHT3	89.2 (4)	OS34—OS25—OW22^xiii	63.1 (6)
OT6—Ti2—OS2	85.3 (4)	Si28—OS25—OB24	77.6 (4)
OS33—Ti2—OS2	89.0 (4)	Ti10—OS25—OB24	87.2 (4)
OS29—Ti2—OS2	174.7 (4)	OB20—OS25—OB24	107.6 (4)
OS12—Ti2—OS2	90.3 (4)	OB21—OS25—OB24	48.7 (3)
OHT3—Ti2—OS2	91.4 (4)	OS26—OS25—OB24	123.9 (4)
OT6—Ti2—Ti1	37.2 (3)	OW36—OS25—OB24	169.2 (5)
OS33—Ti2—Ti1	130.0 (3)	OS47—OS25—OB24	81.6 (3)
OS29—Ti2—Ti1	83.4 (3)	OS31—OS25—OB24	48.3 (3)
OS12—Ti2—Ti1	129.9 (3)	OT5—OS25—OB24	105.8 (4)
OHT3—Ti2—Ti1	41.8 (3)	OS34—OS25—OB24	66.8 (3)
OS2—Ti2—Ti1	98.9 (3)	OW22^xiii—OS25—OB24	66.3 (6)
OT6—Ti2—OS30	57.3 (3)	Si36—OS26—Ti10	131.7 (6)
OS33—Ti2—OS30	119.5 (3)	Si36—OS26—Na3	98.8 (5)
OS29—Ti2—OS30	49.6 (3)	Ti10—OS26—Na3	105.1 (5)
OS12—Ti2—OS30	117.8 (3)	Si36—OS26—OH9	34.6 (4)
OHT3—Ti2—OS30	55.2 (3)	Ti10—OS26—OH9	145.4 (6)
OS2—Ti2—OS30	132.9 (3)	Na3—OS26—OH9	64.9 (4)
Ti1—Ti2—OS30	33.97 (14)	Si36—OS26—OH15	36.9 (4)
OT6—Ti2—Ce1	40.7 (2)	Ti10—OS26—OH15	133.9 (6)
OS33—Ti2—Ce1	88.5 (3)	Na3—OS26—OH15	119.9 (5)
OS29—Ti2—Ce1	133.3 (3)	OH9—OS26—OH15	60.2 (4)
OS12—Ti2—Ce1	134.8 (3)	Si36—OS26—OS32	34.4 (3)
OHT3—Ti2—Ce1	85.8 (3)	Ti10—OS26—OS32	97.5 (4)
OS2—Ti2—Ce1	45.0 (3)	Na3—OS26—OS32	110.7 (5)
Ti1—Ti2—Ce1	65.56 (6)	OH9—OS26—OS32	60.2 (4)
OS30—Ti2—Ce1	95.53 (15)	OH15—OS26—OS32	59.4 (4)
OT6—Ti2—OS36	58.9 (3)	Si36—OS26—OS25	142.6 (6)
OS33—Ti2—OS36	46.5 (3)	Ti10—OS26—OS25	43.9 (3)
OS29—Ti2—OS36	114.3 (3)	Na3—OS26—OS25	118.5 (5)
OS12—Ti2—OS36	130.7 (3)	OH9—OS26—OS25	170.5 (5)
OHT3—Ti2—OS36	127.2 (3)	OH15—OS26—OS25	112.5 (5)
OS2—Ti2—OS36	60.8 (3)	OS32—OS26—OS25	122.8 (5)
Ti1—Ti2—OS36	95.61 (17)	Si36—OS26—OS34	143.8 (6)
OS30—Ti2—OS36	110.8 (2)	Ti10—OS26—OS34	44.4 (3)
Ce1—Ti2—OS36	42.15 (15)	Na3—OS26—OS34	61.7 (4)
OT6—Ti2—OB38	127.6 (3)	OH9—OS26—OS34	121.2 (5)
OS33—Ti2—OB38	101.5 (3)	OH15—OS26—OS34	178.4 (6)
OS29—Ti2—OB38	136.2 (3)	OS32—OS26—OS34	120.3 (5)
OS12—Ti2—OB38	44.5 (3)	OS25—OS26—OS34	66.2 (4)
OHT3—Ti2—OB38	84.7 (3)	Si36—OS26—OS44	92.5 (5)
OS2—Ti2—OB38	46.5 (3)	Ti10—OS26—OS44	48.0 (3)
Ti1—Ti2—OB38	119.54 (17)	Na3—OS26—OS44	88.2 (4)
OS30—Ti2—OB38	138.7 (2)	OH9—OS26—OS44	97.5 (4)
Ce1—Ti2—OB38	90.33 (16)	OH15—OS26—OS44	120.5 (5)
OS36—Ti2—OB38	100.9 (2)	OS32—OS26—OS44	61.7 (3)
OT6—Ti2—Na2	133.8 (3)	OS25—OS26—OS44	91.6 (4)
OS33—Ti2—Na2	91.9 (3)	OS34—OS26—OS44	59.0 (3)
OS29—Ti2—Na2	41.4 (3)	Si36—OS26—OT5	93.7 (5)
OS12—Ti2—Na2	50.5 (3)	Ti10—OS26—OT5	42.4 (3)
OHT3—Ti2—Na2	93.2 (3)	Na3—OS26—OT5	138.5 (5)
OS2—Ti2—Na2	140.4 (3)	OH9—OS26—OT5	123.3 (5)
Ti1—Ti2—Na2	110.32 (15)	OH15—OS26—OT5	93.1 (4)
OS30—Ti2—Na2	79.54 (19)	OS32—OS26—OT5	63.1 (3)
Ce1—Ti2—Na2	174.55 (15)	OS25—OS26—OT5	60.9 (3)
OS36—Ti2—Na2	137.5 (2)	OS34—OS26—OT5	85.4 (4)
OB38—Ti2—Na2	94.9 (2)	OS44—OS26—OT5	51.6 (3)
OS4—Ti3—OS13^ii	91.0 (4)	Si36—OS26—OW36	93.0 (6)
OS4—Ti3—OS40	101.8 (4)	Ti10—OS26—OW36	97.6 (5)
OS13^ii—Ti3—OS40	92.7 (4)	Na3—OS26—OW36	136.1 (6)
OS4—Ti3—OT3^ii	95.8 (4)	OH9—OS26—OW36	112.4 (6)
OS13^ii—Ti3—OT3^ii	94.2 (4)	OH15—OS26—OW36	56.5 (5)
OS40—Ti3—OT3^ii	160.9 (4)	OS32—OS26—OW36	102.8 (5)
OS4—Ti3—OS35	90.7 (4)	OS25—OS26—OW36	58.7 (5)
OS13^ii—Ti3—OS35	178.0 (4)	OS34—OS26—OW36	122.5 (5)
OS40—Ti3—OS35	88.1 (4)	OS44—OS26—OW36	133.5 (5)
OT3^ii—Ti3—OS35	84.5 (4)	OT5—OS26—OW36	81.9 (5)
OS4—Ti3—OT7^ii	172.1 (4)	Si36—OS26—OW22	111.6 (7)
OS13^ii—Ti3—OT7^ii	87.7 (4)	Ti10—OS26—OW22	114.7 (6)
OS40—Ti3—OT7^ii	86.0 (4)	Na3—OS26—OW22	43.5 (6)
OT3^ii—Ti3—OT7^ii	76.5 (4)	OH9—OS26—OW22	81.8 (6)
OS35—Ti3—OT7^ii	90.5 (4)	OH15—OS26—OW22	104.9 (6)
OS4—Ti3—Ti5^ii	129.6 (3)	OS32—OS26—OW22	141.9 (6)
OS13^ii—Ti3—Ti5^ii	82.8 (3)	OS25—OS26—OW22	95.1 (6)
OS40—Ti3—Ti5^ii	128.4 (3)	OS34—OS26—OW22	76.4 (6)
OT3^ii—Ti3—Ti5^ii	35.7 (3)	OS44—OS26—OW22	127.1 (7)
OS35—Ti3—Ti5^ii	95.3 (3)	OT5—OS26—OW22	154.5 (6)
OT7^ii—Ti3—Ti5^ii	42.5 (3)	OW36—OS26—OW22	93.0 (7)
OS4—Ti3—OS16^ii	120.3 (4)	Si16—OS27—Ti1^iv	128.5 (5)
OS13^ii—Ti3—OS16^ii	49.5 (3)	Si16—OS27—Ce1^iv	129.7 (5)
OS40—Ti3—OS16^ii	119.6 (3)	Ti1^iv—OS27—Ce1^iv	101.4 (3)
OT3^ii—Ti3—OS16^ii	54.8 (3)	Si16—OS27—OT6^iv	174.2 (5)
OS35—Ti3—OS16^ii	128.6 (3)	Ti1^iv—OS27—OT6^iv	45.8 (3)
OT7^ii—Ti3—OS16^ii	53.6 (3)	Ce1^iv—OS27—OT6^iv	55.8 (2)
Ti5^ii—Ti3—OS16^ii	33.29 (17)	Si16—OS27—OB30	34.9 (3)
OS4—Ti3—Ce1	88.5 (3)	Ti1^iv—OS27—OB30	112.9 (4)
OS13^ii—Ti3—Ce1	135.5 (3)	Ce1^iv—OS27—OB30	125.7 (4)
OS40—Ti3—Ce1	130.8 (3)	OT6^iv—OS27—OB30	142.4 (4)
OT3^ii—Ti3—Ce1	41.8 (3)	Si16—OS27—OS17	33.8 (3)
OS35—Ti3—Ce1	43.4 (3)	Ti1^iv—OS27—OS17	159.2 (5)
OT7^ii—Ti3—Ce1	87.0 (3)	Ce1^iv—OS27—OS17	98.2 (3)
Ti5^ii—Ti3—Ce1	64.15 (7)	OT6^iv—OS27—OS17	151.9 (4)
OS16^ii—Ti3—Ce1	93.72 (16)	OB30—OS27—OS17	59.2 (3)
OS4—Ti3—OS2	46.5 (3)	Si16—OS27—OB5	34.8 (3)
OS13^ii—Ti3—OS2	119.0 (4)	Ti1^iv—OS27—OB5	100.5 (4)
OS40—Ti3—OS2	131.0 (3)	Ce1^iv—OS27—OB5	152.6 (4)
OT3^ii—Ti3—OS2	59.2 (3)	OT6^iv—OS27—OB5	141.4 (4)
OS35—Ti3—OS2	61.6 (3)	OB30—OS27—OB5	58.1 (3)
OT7^ii—Ti3—OS2	128.1 (3)	OS17—OS27—OB5	58.7 (3)
Ti5^ii—Ti3—OS2	94.14 (16)	Si16—OS27—OS42	85.6 (4)
OS16^ii—Ti3—OS2	109.4 (2)	Ti1^iv—OS27—OS42	43.8 (2)
Ce1—Ti3—OS2	42.21 (14)	Ce1^iv—OS27—OS42	144.7 (4)
OS4—Ti3—OB29^ii	142.0 (3)	OT6^iv—OS27—OS42	88.9 (3)
OS13^ii—Ti3—OB29^ii	106.3 (4)	OB30—OS27—OS42	82.7 (4)
OS40—Ti3—OB29^ii	45.2 (4)	OS17—OS27—OS42	115.7 (4)
OT3^ii—Ti3—OB29^ii	115.7 (3)	OB5—OS27—OS42	57.3 (3)
OS35—Ti3—OB29^ii	73.0 (3)	Si16—OS27—OS10	114.7 (5)
OT7^ii—Ti3—OB29^ii	45.5 (3)	Ti1^iv—OS27—OS10	43.5 (2)
Ti5^ii—Ti3—OB29^ii	86.76 (19)	Ce1^iv—OS27—OS10	96.4 (3)
OS16^ii—Ti3—OB29^ii	95.9 (3)	OT6^iv—OS27—OS10	61.0 (3)
Ce1—Ti3—OB29^ii	100.85 (18)	OB30—OS27—OS10	82.6 (4)
OS2—Ti3—OB29^ii	134.4 (2)	OS17—OS27—OS10	140.6 (4)
OS4—Ti3—OB10	102.7 (3)	OB5—OS27—OS10	110.9 (4)
OS13^ii—Ti3—OB10	135.5 (4)	OS42—OS27—OS10	63.8 (3)
OS40—Ti3—OB10	43.3 (3)	Si16—OS27—OHT3^iv	127.0 (5)
OT3^ii—Ti3—OB10	125.5 (3)	Ti1^iv—OS27—OHT3^iv	44.2 (2)
OS35—Ti3—OB10	45.1 (3)	Ce1^iv—OS27—OHT3^iv	91.3 (3)
OT7^ii—Ti3—OB10	83.6 (3)	OT6^iv—OS27—OHT3^iv	50.8 (3)
Ti5^ii—Ti3—OB10	116.51 (19)	OB30—OS27—OHT3^iv	142.4 (4)
OS16^ii—Ti3—OB10	136.9 (3)	OS17—OS27—OHT3^iv	128.9 (4)
Ce1—Ti3—OB10	87.58 (16)	OB5—OS27—OHT3^iv	93.0 (4)
OS2—Ti3—OB10	100.2 (2)	OS42—OS27—OHT3^iv	60.4 (3)
OB29^ii—Ti3—OB10	42.1 (2)	OS10—OS27—OHT3^iv	87.0 (3)
OHT4^i—Ti4—OS23^i	91.3 (5)	Si16—OS27—OT3	90.0 (4)
OHT4^i—Ti4—OT4^i	78.6 (4)	Ti1^iv—OS27—OT3	134.1 (4)
OS23^i—Ti4—OT4^i	97.6 (5)	Ce1^iv—OS27—OT3	51.1 (2)
OHT4^i—Ti4—OS18	95.3 (5)	OT6^iv—OS27—OT3	95.5 (3)
OS23^i—Ti4—OS18	87.0 (4)	OB30—OS27—OT3	113.0 (4)
OT4^i—Ti4—OS18	172.3 (5)	OS17—OS27—OT3	56.9 (3)
OHT4^i—Ti4—OS11	166.8 (5)	OB5—OS27—OT3	101.5 (4)
OS23^i—Ti4—OS11	85.8 (5)	OS42—OS27—OT3	143.1 (4)
OT4^i—Ti4—OS11	89.0 (4)	OS10—OS27—OT3	147.5 (4)
OS18—Ti4—OS11	97.4 (5)	OHT3^iv—OS27—OT3	94.8 (3)
OHT4^i—Ti4—OS36	95.8 (4)	Si16—OS27—OS45	80.9 (4)
OS23^i—Ti4—OS36	172.7 (5)	Ti1^iv—OS27—OS45	144.5 (4)
OT4^i—Ti4—OS36	85.8 (4)	Ce1^iv—OS27—OS45	50.5 (2)
OS18—Ti4—OS36	90.3 (4)	OT6^iv—OS27—OS45	104.1 (4)
OS11—Ti4—OS36	87.8 (4)	OB30—OS27—OS45	78.9 (3)
OHT4^i—Ti4—Ti6^i	40.3 (3)	OS17—OS27—OS45	55.9 (3)
OS23^i—Ti4—Ti6^i	86.8 (4)	OB5—OS27—OS45	113.5 (4)
OT4^i—Ti4—Ti6^i	39.9 (3)	OS42—OS27—OS45	161.4 (4)
OS18—Ti4—Ti6^i	134.9 (4)	OS10—OS27—OS45	110.7 (4)
OS11—Ti4—Ti6^i	126.5 (3)	OHT3^iv—OS27—OS45	138.2 (4)
OS36—Ti4—Ti6^i	99.8 (3)	OT3—OS27—OS45	50.1 (3)
OHT4^i—Ti4—OS21^i	55.1 (4)	Si33—OS28—Ti11	128.8 (5)
OS23^i—Ti4—OS21^i	52.4 (4)	Si33—OS28—Na1^vii	121.8 (5)
OT4^i—Ti4—OS21^i	56.4 (3)	Ti11—OS28—Na1^vii	101.7 (4)
OS18—Ti4—OS21^i	123.6 (4)	Si33—OS28—OB2	36.7 (3)
OS11—Ti4—OS21^i	114.0 (4)	Ti11—OS28—OB2	104.5 (4)
OS36—Ti4—OS21^i	134.0 (3)	Na1^vii—OS28—OB2	153.8 (5)
Ti6^i—Ti4—OS21^i	34.44 (18)	Si33—OS28—OB6	36.9 (3)
OHT4^i—Ti4—Na14	101.8 (4)	Ti11—OS28—OB6	104.3 (4)
OS23^i—Ti4—Na14	44.2 (4)	Na1^vii—OS28—OB6	112.9 (5)
OT4^i—Ti4—Na14	141.6 (4)	OB2—OS28—OB6	60.4 (3)
OS18—Ti4—Na14	43.8 (4)	Si33—OS28—OH3	30.9 (3)
OS11—Ti4—Na14	85.1 (4)	Ti11—OS28—OH3	159.7 (5)
OS36—Ti4—Na14	131.7 (4)	Na1^vii—OS28—OH3	95.8 (4)
Ti6^i—Ti4—Na14	122.4 (3)	OB2—OS28—OH3	58.5 (3)
OS21^i—Ti4—Na14	91.8 (3)	OB6—OS28—OH3	58.8 (3)
OHT4^i—Ti4—Na8	129.1 (4)	Si33—OS28—OS32	146.8 (5)
OS23^i—Ti4—Na8	44.8 (4)	Ti11—OS28—OS32	44.4 (3)
OT4^i—Ti4—Na8	83.1 (3)	Na1^vii—OS28—OS32	58.5 (3)
OS18—Ti4—Na8	104.4 (4)	OB2—OS28—OS32	147.0 (4)
OS11—Ti4—Na8	43.4 (4)	OB6—OS28—OS32	110.0 (4)
OS36—Ti4—Na8	129.8 (4)	OH3—OS28—OS32	147.5 (4)
Ti6^i—Ti4—Na8	102.1 (2)	Si33—OS28—OS44	91.0 (4)
OS21^i—Ti4—Na8	75.2 (3)	Ti11—OS28—OS44	47.9 (3)
Na14—Ti4—Na8	66.8 (3)	Na1^vii—OS28—OS44	107.4 (4)
OHT4^i—Ti4—Ce1	87.2 (3)	OB2—OS28—OS44	90.5 (4)
OS23^i—Ti4—Ce1	138.2 (3)	OB6—OS28—OS44	58.0 (3)
OT4^i—Ti4—Ce1	41.2 (3)	OH3—OS28—OS44	116.8 (4)
OS18—Ti4—Ce1	134.8 (3)	OS32—OS28—OS44	61.2 (3)
OS11—Ti4—Ce1	86.4 (3)	Si33—OS28—OS1	91.6 (4)
OS36—Ti4—Ce1	44.6 (3)	Ti11—OS28—OS1	46.8 (3)
Ti6^i—Ti4—Ce1	65.63 (7)	Na1^vii—OS28—OS1	146.2 (5)
OS21^i—Ti4—Ce1	94.51 (18)	OB2—OS28—OS1	59.1 (3)
Na14—Ti4—Ce1	170.9 (3)	OB6—OS28—OS1	90.2 (4)
Na8—Ti4—Ce1	108.64 (17)	OH3—OS28—OS1	117.6 (4)
OHT4^i—Ti4—OB28	88.9 (4)	OS32—OS28—OS1	91.2 (4)
OS23^i—Ti4—OB28	131.0 (4)	OS44—OS28—OS1	63.3 (3)
OT4^i—Ti4—OB28	130.2 (3)	Si33—OS28—OS43	146.5 (5)
OS18—Ti4—OB28	44.3 (3)	Ti11—OS28—OS43	37.8 (2)
OS11—Ti4—OB28	102.8 (4)	Na1^vii—OS28—OS43	90.8 (4)
OS36—Ti4—OB28	47.4 (3)	OB2—OS28—OS43	109.9 (4)
Ti6^i—Ti4—OB28	121.16 (18)	OB6—OS28—OS43	140.6 (4)
OS21^i—Ti4—OB28	143.1 (2)	OH3—OS28—OS43	153.1 (4)
Na14—Ti4—OB28	88.0 (3)	OS32—OS28—OS43	55.3 (3)
Na8—Ti4—OB28	136.7 (3)	OS44—OS28—OS43	85.7 (3)
Ce1—Ti4—OB28	90.76 (16)	OS1—OS28—OS43	57.3 (3)
OS17—Ti5—OT3	95.9 (4)	Si33—OS28—Si32	69.1 (3)
OS17—Ti5—OS16	89.5 (4)	Ti11—OS28—Si32	78.0 (3)
OT3—Ti5—OS16	95.8 (4)	Na1^vii—OS28—Si32	161.2 (4)
OS17—Ti5—OS19	101.5 (4)	OB2—OS28—Si32	32.5 (2)
OT3—Ti5—OS19	161.2 (4)	OB6—OS28—Si32	85.0 (3)
OS16—Ti5—OS19	91.5 (4)	OH3—OS28—Si32	88.7 (3)
OS17—Ti5—OS45	91.3 (4)	OS32—OS28—Si32	122.2 (4)
OT3—Ti5—OS45	84.9 (4)	OS44—OS28—Si32	86.5 (3)
OS16—Ti5—OS45	178.9 (4)	OS1—OS28—Si32	31.6 (2)
OS19—Ti5—OS45	87.5 (4)	OS43—OS28—Si32	77.4 (3)
OS17—Ti5—OT7	171.1 (4)	Si33—OS28—Si34	67.5 (3)
OT3—Ti5—OT7	76.0 (4)	Ti11—OS28—Si34	78.3 (3)
OS16—Ti5—OT7	87.7 (4)	Na1^vii—OS28—Si34	102.8 (4)
OS19—Ti5—OT7	87.0 (4)	OB2—OS28—Si34	82.8 (3)
OS45—Ti5—OT7	91.7 (4)	OB6—OS28—Si34	30.8 (2)
OS17—Ti5—Ti3^iv	129.8 (3)	OH3—OS28—Si34	87.9 (3)
OT3—Ti5—Ti3^iv	36.3 (3)	OS32—OS28—Si34	79.9 (3)
OS16—Ti5—Ti3^iv	83.8 (3)	OS44—OS28—Si34	30.5 (2)
OS19—Ti5—Ti3^iv	128.2 (3)	OS1—OS28—Si34	84.2 (3)
OS45—Ti5—Ti3^iv	96.3 (3)	OS43—OS28—Si34	116.1 (3)
OT7—Ti5—Ti3^iv	41.4 (3)	Si32—OS28—Si34	95.6 (3)
OS17—Ti5—OS13	119.0 (4)	Si7—OS29—Ti2	131.7 (5)
OT3—Ti5—OS13	54.9 (3)	Si7—OS29—Na2	99.4 (5)
OS16—Ti5—OS13	50.6 (3)	Ti2—OS29—Na2	109.3 (4)
OS19—Ti5—OS13	120.2 (4)	Si7—OS29—OS33	150.3 (6)
OS45—Ti5—OS13	129.5 (3)	Ti2—OS29—OS33	47.0 (3)
OT7—Ti5—OS13	53.2 (3)	Na2—OS29—OS33	108.4 (4)
Ti3^iv—Ti5—OS13	33.25 (16)	Si7—OS29—OS5	36.4 (3)
OS17—Ti5—K3	83.9 (5)	Ti2—OS29—OS5	137.2 (5)
OT3—Ti5—K3	142.9 (5)	Na2—OS29—OS5	63.6 (3)
OS16—Ti5—K3	47.1 (5)	OS33—OS29—OS5	171.3 (5)
OS19—Ti5—K3	47.7 (5)	Si7—OS29—OS30	35.1 (3)
OS45—Ti5—K3	132.2 (5)	Ti2—OS29—OS30	96.8 (4)
OT7—Ti5—K3	100.2 (5)	Na2—OS29—OS30	121.9 (4)
Ti3^iv—Ti5—K3	122.9 (4)	OS33—OS29—OS30	126.6 (4)
OS13—Ti5—K3	92.9 (4)	OS5—OS29—OS30	62.1 (3)
OS17—Ti5—Ce1^iv	89.7 (3)	Si7—OS29—OS3	36.3 (3)
OT3—Ti5—Ce1^iv	41.9 (3)	Ti2—OS29—OS3	142.1 (5)
OS16—Ti5—Ce1^iv	137.4 (3)	Na2—OS29—OS3	108.5 (4)
OS19—Ti5—Ce1^iv	130.3 (3)	OS33—OS29—OS3	121.1 (4)
OS45—Ti5—Ce1^iv	43.5 (3)	OS5—OS29—OS3	61.3 (3)
OT7—Ti5—Ce1^iv	86.7 (3)	OS30—OS29—OS3	59.8 (3)
Ti3^iv—Ti5—Ce1^iv	64.70 (6)	Si7—OS29—OS12	138.4 (5)
OS13—Ti5—Ce1^iv	93.97 (17)	Ti2—OS29—OS12	44.6 (3)
K3—Ti5—Ce1^iv	172.3 (4)	Na2—OS29—OS12	64.7 (3)
OS17—Ti5—OS27	46.8 (3)	OS33—OS29—OS12	66.1 (3)
OT3—Ti5—OS27	59.7 (3)	OS5—OS29—OS12	111.1 (4)
OS16—Ti5—OS27	119.6 (4)	OS30—OS29—OS12	119.5 (4)
OS19—Ti5—OS27	130.1 (4)	OS3—OS29—OS12	172.2 (5)
OS45—Ti5—OS27	61.5 (3)	Si7—OS29—OT6	97.0 (4)
OT7—Ti5—OS27	128.6 (3)	Ti2—OS29—OT6	43.0 (3)
Ti3^iv—Ti5—OS27	95.32 (16)	Na2—OS29—OT6	150.4 (4)
OS13—Ti5—OS27	109.7 (2)	OS33—OS29—OT6	63.1 (3)
K3—Ti5—OS27	130.7 (4)	OS5—OS29—OT6	125.5 (4)
Ce1^iv—Ti5—OS27	42.99 (14)	OS30—OS29—OT6	64.3 (3)
OS17—Ti5—OB34	142.9 (4)	OS3—OS29—OT6	99.3 (4)
OT3—Ti5—OB34	115.4 (3)	OS12—OS29—OT6	86.8 (4)
OS16—Ti5—OB34	105.8 (4)	Si7—OS29—OHT3	91.6 (4)
OS19—Ti5—OB34	45.8 (4)	Ti2—OS29—OHT3	44.7 (3)
OS45—Ti5—OB34	73.1 (3)	Na2—OS29—OHT3	104.1 (4)
OT7—Ti5—OB34	46.0 (3)	OS33—OS29—OHT3	91.4 (4)
Ti3^iv—Ti5—OB34	86.05 (19)	OS5—OS29—OHT3	94.0 (4)
OS13—Ti5—OB34	96.1 (3)	OS30—OS29—OHT3	61.5 (3)
K3—Ti5—OB34	82.6 (4)	OS3—OS29—OHT3	121.3 (4)
Ce1^iv—Ti5—OB34	100.2 (2)	OS12—OS29—OHT3	59.2 (3)
OS27—Ti5—OB34	134.4 (2)	OT6—OS29—OHT3	50.8 (3)
OT4—Ti6—OS21	94.8 (4)	Si7—OS29—Ba^ix	97.8 (4)
OT4—Ti6—OHT4	79.4 (4)	Ti2—OS29—Ba^ix	109.6 (4)
OS21—Ti6—OHT4	92.3 (4)	Na2—OS29—Ba^ix	106.5 (3)
OT4—Ti6—OS20^iv	173.1 (5)	OS33—OS29—Ba^ix	65.0 (3)
OS21—Ti6—OS20^iv	89.0 (4)	OS5—OS29—Ba^ix	112.8 (3)
OHT4—Ti6—OS20^iv	94.8 (5)	OS30—OS29—Ba^ix	112.1 (4)
OT4—Ti6—OS15^iv	90.4 (4)	OS3—OS29—Ba^ix	61.5 (3)
OS21—Ti6—OS15^iv	86.8 (4)	OS12—OS29—Ba^ix	123.2 (4)
OHT4—Ti6—OS15^iv	169.6 (4)	OT6—OS29—Ba^ix	95.5 (3)
OS20^iv—Ti6—OS15^iv	95.5 (5)	OHT3—OS29—Ba^ix	146.0 (4)
OT4—Ti6—OS46^iv	85.3 (4)	Si7—OS29—OW14	92.3 (4)
OS21—Ti6—OS46^iv	173.7 (4)	Ti2—OS29—OW14	136.0 (4)
OHT4—Ti6—OS46^iv	93.9 (4)	Na2—OS29—OW14	52.5 (3)
OS20^iv—Ti6—OS46^iv	91.5 (4)	OS33—OS29—OW14	96.5 (4)
OS15^iv—Ti6—OS46^iv	86.9 (4)	OS5—OS29—OW14	76.0 (3)
OT4—Ti6—Ti4^v	40.8 (3)	OS30—OS29—OW14	127.2 (4)
OS21—Ti6—Ti4^v	85.6 (4)	OS3—OS29—OW14	72.8 (3)
OHT4—Ti6—Ti4^v	40.3 (3)	OS12—OS29—OW14	104.2 (4)
OS20^iv—Ti6—Ti4^v	134.3 (4)	OT6—OS29—OW14	151.0 (4)
OS15^iv—Ti6—Ti4^v	129.4 (3)	OHT3—OS29—OW14	156.5 (4)
OS46^iv—Ti6—Ti4^v	98.5 (3)	Ba^ix—OS29—OW14	55.9 (2)
OT4—Ti6—Na9^iv	87.0 (5)	Si7—OS30—Ti1	131.4 (5)
OS21—Ti6—Na9^iv	43.2 (4)	Si7—OS30—Na12	128.4 (6)
OHT4—Ti6—Na9^iv	132.2 (4)	Ti1—OS30—Na12	98.7 (5)
OS20^iv—Ti6—Na9^iv	99.7 (5)	Si7—OS30—OS3	36.3 (3)
OS15^iv—Ti6—Na9^iv	44.4 (4)	Ti1—OS30—OS3	136.6 (4)
OS46^iv—Ti6—Na9^iv	130.6 (4)	Na12—OS30—OS3	115.5 (5)
Ti4^v—Ti6—Na9^iv	106.7 (4)	Si7—OS30—OS29	35.7 (3)
OT4—Ti6—OS23	58.3 (3)	Ti1—OS30—OS29	95.7 (4)
OS21—Ti6—OS23	51.3 (4)	Na12—OS30—OS29	159.9 (6)
OHT4—Ti6—OS23	53.6 (3)	OS3—OS30—OS29	60.1 (3)
OS20^iv—Ti6—OS23	121.0 (4)	Si7—OS30—OS10^ii	138.3 (5)
OS15^iv—Ti6—OS23	119.3 (4)	Ti1—OS30—OS10^ii	45.2 (3)
OS46^iv—Ti6—OS23	132.8 (3)	Na12—OS30—OS10^ii	83.4 (6)
Ti4^v—Ti6—OS23	34.31 (18)	OS3—OS30—OS10^ii	110.8 (4)
Na9^iv—Ti6—OS23	80.3 (4)	OS29—OS30—OS10^ii	116.7 (4)
OT4—Ti6—Ce1^v	41.1 (3)	Si7—OS30—OS5	33.1 (3)
OS21—Ti6—Ce1^v	135.2 (3)	Ti1—OS30—OS5	139.8 (4)
OHT4—Ti6—Ce1^v	87.4 (3)	Na12—OS30—OS5	101.7 (6)
OS20^iv—Ti6—Ce1^v	135.7 (3)	OS3—OS30—OS5	60.2 (3)
OS15^iv—Ti6—Ce1^v	85.9 (3)	OS29—OS30—OS5	58.5 (3)
OS46^iv—Ti6—Ce1^v	44.3 (3)	OS10^ii—OS30—OS5	170.8 (4)
Ti4^v—Ti6—Ce1^v	65.94 (7)	Si7—OS30—OS42^ii	149.6 (5)
Na9^iv—Ti6—Ce1^v	111.2 (4)	Ti1—OS30—OS42^ii	45.1 (2)
OS23—Ti6—Ce1^v	95.62 (19)	Na12—OS30—OS42^ii	59.5 (4)
OT4—Ti6—OB9^iv	130.1 (3)	OS3—OS30—OS42^ii	173.6 (5)
OS21—Ti6—OB9^iv	134.3 (4)	OS29—OS30—OS42^ii	126.1 (4)
OHT4—Ti6—OB9^iv	88.7 (3)	OS10^ii—OS30—OS42^ii	65.7 (3)
OS20^iv—Ti6—OB9^iv	45.4 (3)	OS5—OS30—OS42^ii	123.5 (4)
OS15^iv—Ti6—OB9^iv	99.2 (3)	Si7—OS30—Na4	90.7 (4)
OS46^iv—Ti6—OB9^iv	47.0 (3)	Ti1—OS30—Na4	100.9 (4)
Ti4^v—Ti6—OB9^iv	121.03 (18)	Na12—OS30—Na4	90.9 (6)
Na9^iv—Ti6—OB9^iv	132.3 (4)	OS3—OS30—Na4	55.2 (3)
OS23—Ti6—OB9^iv	141.3 (3)	OS29—OS30—Na4	100.1 (4)
Ce1^v—Ti6—OB9^iv	90.58 (15)	OS10^ii—OS30—Na4	58.9 (3)
OT4—Ti6—OS45^iv	55.3 (3)	OS5—OS30—Na4	112.9 (4)
OS21—Ti6—OS45^iv	115.8 (4)	OS42^ii—OS30—Na4	119.5 (4)
OHT4—Ti6—OS45^iv	126.6 (3)	Si7—OS30—OHT3	93.8 (4)
OS20^iv—Ti6—OS45^iv	127.7 (4)	Ti1—OS30—OHT3	46.8 (3)
OS15^iv—Ti6—OS45^iv	45.8 (3)	Na12—OS30—OHT3	118.6 (5)
OS46^iv—Ti6—OS45^iv	59.3 (3)	OS3—OS30—OHT3	123.4 (4)
Ti4^v—Ti6—OS45^iv	94.88 (18)	OS29—OS30—OHT3	63.3 (3)
Na9^iv—Ti6—OS45^iv	76.6 (3)	OS10^ii—OS30—OHT3	91.2 (3)
OS23—Ti6—OS45^iv	109.9 (2)	OS5—OS30—OHT3	93.0 (4)
Ce1^v—Ti6—OS45^iv	40.30 (15)	OS42^ii—OS30—OHT3	62.8 (3)
OB9^iv—Ti6—OS45^iv	99.3 (2)	Na4—OS30—OHT3	136.4 (4)
OT2—Ti7—OS7	169.9 (4)	Si7—OS30—OT6	93.7 (4)
OT2—Ti7—OS22	95.0 (4)	Ti1—OS30—OT6	41.4 (2)
OS7—Ti7—OS22	88.0 (4)	Na12—OS30—OT6	137.8 (5)
OT2—Ti7—OS9	93.7 (4)	OS3—OS30—OT6	97.0 (4)
OS7—Ti7—OS9	96.0 (4)	OS29—OS30—OT6	60.4 (3)
OS22—Ti7—OS9	89.6 (4)	OS10^ii—OS30—OT6	59.3 (3)
OT2—Ti7—OHT1	77.6 (4)	OS5—OS30—OT6	118.2 (4)
OS7—Ti7—OHT1	92.7 (4)	OS42^ii—OS30—OT6	85.8 (3)
OS22—Ti7—OHT1	91.5 (4)	Na4—OS30—OT6	86.1 (3)
OS9—Ti7—OHT1	171.3 (4)	OHT3—OS30—OT6	50.3 (3)
OT2—Ti7—OS48	86.3 (4)	Si7—OS30—OW9	98.5 (8)
OS7—Ti7—OS48	91.5 (4)	Ti1—OS30—OW9	106.6 (9)
OS22—Ti7—OS48	175.6 (4)	Na12—OS30—OW9	48.0 (9)
OS9—Ti7—OS48	86.2 (4)	OS3—OS30—OW9	116.0 (9)
OHT1—Ti7—OS48	92.8 (4)	OS29—OS30—OW9	114.1 (8)
OT2—Ti7—Ti12	37.7 (2)	OS10^ii—OS30—OW9	122.9 (8)
OS7—Ti7—Ti12	133.6 (3)	OS5—OS30—OW9	65.4 (8)
OS22—Ti7—Ti12	84.1 (3)	OS42^ii—OS30—OW9	64.2 (8)
OS9—Ti7—Ti12	129.5 (3)	Na4—OS30—OW9	132.9 (9)
OHT1—Ti7—Ti12	42.2 (3)	OHT3—OS30—OW9	89.2 (9)
OS48—Ti7—Ti12	99.3 (3)	OT6—OS30—OW9	138.4 (9)
OT2—Ti7—OS39	55.5 (3)	Si26—OS31—Ti10	127.8 (5)
OS7—Ti7—OS39	121.2 (3)	Si26—OS31—Ce2	129.5 (5)
OS22—Ti7—OS39	50.0 (4)	Ti10—OS31—Ce2	102.2 (3)
OS9—Ti7—OS39	118.6 (3)	Si26—OS31—OB24	35.4 (3)
OHT1—Ti7—OS39	56.6 (3)	Ti10—OS31—OB24	109.8 (4)
OS48—Ti7—OS39	133.3 (3)	Ce2—OS31—OB24	126.9 (4)
Ti12—Ti7—OS39	34.09 (18)	Si26—OS31—OB23	35.4 (3)
OT2—Ti7—Ce2	40.9 (2)	Ti10—OS31—OB23	101.2 (4)
OS7—Ti7—Ce2	136.8 (3)	Ce2—OS31—OB23	150.5 (4)
OS22—Ti7—Ce2	135.2 (3)	OB24—OS31—OB23	59.4 (4)
OS9—Ti7—Ce2	87.1 (3)	Si26—OS31—OT5	172.8 (5)
OHT1—Ti7—Ce2	86.0 (3)	Ti10—OS31—OT5	45.0 (3)
OS48—Ti7—Ce2	45.6 (2)	Ce2—OS31—OT5	57.5 (3)
Ti12—Ti7—Ce2	64.58 (7)	OB24—OS31—OT5	141.1 (4)
OS39—Ti7—Ce2	93.71 (18)	OB23—OS31—OT5	139.8 (4)
OT2—Ti7—OB14	131.1 (3)	Si26—OS31—OS37	32.8 (3)
OS7—Ti7—OB14	45.3 (3)	Ti10—OS31—OS37	158.8 (5)
OS22—Ti7—OB14	133.3 (4)	Ce2—OS31—OS37	98.6 (3)
OS9—Ti7—OB14	94.1 (3)	OB24—OS31—OS37	59.2 (3)
OHT1—Ti7—OB14	91.4 (3)	OB23—OS31—OS37	57.8 (3)
OS48—Ti7—OB14	46.3 (3)	OT5—OS31—OS37	154.3 (4)
Ti12—Ti7—OB14	125.60 (17)	Si26—OS31—OS25	113.1 (5)
OS39—Ti7—OB14	147.1 (2)	Ti10—OS31—OS25	42.5 (3)
Ce2—Ti7—OB14	91.48 (15)	Ce2—OS31—OS25	97.9 (3)
OT2—Ti7—OS41	55.4 (3)	OB24—OS31—OS25	80.1 (4)
OS7—Ti7—OS41	131.3 (3)	OB23—OS31—OS25	111.5 (4)
OS22—Ti7—OS41	116.3 (3)	OT5—OS31—OS25	61.7 (3)
OS9—Ti7—OS41	46.9 (3)	OS37—OS31—OS25	138.0 (4)
OHT1—Ti7—OS41	125.5 (3)	Si26—OS31—OS34	86.0 (4)
OS48—Ti7—OS41	61.1 (3)	Ti10—OS31—OS34	43.5 (3)
Ti12—Ti7—OS41	92.43 (15)	Ce2—OS31—OS34	144.3 (4)
OS39—Ti7—OS41	105.9 (2)	OB24—OS31—OS34	82.6 (4)
Ce2—Ti7—OS41	40.82 (13)	OB23—OS31—OS34	57.9 (3)
OB14—Ti7—OS41	99.1 (2)	OT5—OS31—OS34	87.0 (4)
OT2—Ti7—K2^vi	139.5 (3)	OS37—OS31—OS34	115.3 (4)
OS7—Ti7—K2^vi	43.2 (3)	OS25—OS31—OS34	64.6 (3)
OS22—Ti7—K2^vi	44.9 (4)	Si26—OS31—OS44	125.6 (5)
OS9—Ti7—K2^vi	91.6 (3)	Ti10—OS31—OS44	44.6 (2)
OHT1—Ti7—K2^vi	95.3 (3)	Ce2—OS31—OS44	93.5 (3)
OS48—Ti7—K2^vi	134.2 (3)	OB24—OS31—OS44	138.7 (4)
Ti12—Ti7—K2^vi	116.44 (17)	OB23—OS31—OS44	90.5 (4)
OS39—Ti7—K2^vi	87.0 (2)	OT5—OS31—OS44	51.1 (3)
Ce2—Ti7—K2^vi	178.7 (2)	OS37—OS31—OS44	130.2 (4)
OB14—Ti7—K2^vi	88.4 (2)	OS25—OS31—OS44	86.8 (3)
OS41—Ti7—K2^vi	138.0 (3)	OS34—OS31—OS44	56.5 (3)
OS37—Ti8—OS14	101.7 (4)	Si26—OS31—OT1	87.9 (4)
OS37—Ti8—OT1	90.3 (4)	Ti10—OS31—OT1	138.0 (4)
OS14—Ti8—OT1	166.9 (4)	Ce2—OS31—OT1	52.1 (2)
OS37—Ti8—OS5^iii	89.9 (4)	OB24—OS31—OT1	112.2 (4)
OS14—Ti8—OS5^iii	88.1 (4)	OB23—OS31—OT1	98.4 (4)
OT1—Ti8—OS5^iii	97.3 (4)	OT5—OS31—OT1	98.9 (3)
OS37—Ti8—OHT2	165.6 (4)	OS37—OS31—OT1	55.8 (3)
OS14—Ti8—OHT2	92.7 (4)	OS25—OS31—OT1	149.6 (4)
OT1—Ti8—OHT2	75.5 (4)	OS34—OS31—OT1	142.0 (4)
OS5^iii—Ti8—OHT2	89.8 (4)	OS44—OS31—OT1	98.9 (3)
OS37—Ti8—OS49	89.4 (4)	Si26—OS31—OS47	118.6 (4)
OS14—Ti8—OS49	89.5 (4)	Ti10—OS31—OS47	85.2 (3)
OT1—Ti8—OS49	85.3 (4)	Ce2—OS31—OS47	51.9 (2)
OS5^iii—Ti8—OS49	177.3 (4)	OB24—OS31—OS47	89.4 (4)
OHT2—Ti8—OS49	91.5 (4)	OB23—OS31—OS47	148.6 (4)
OS37—Ti8—Ti9	125.0 (3)	OT5—OS31—OS47	63.3 (3)
OS14—Ti8—Ti9	132.6 (3)	OS37—OS31—OS47	111.3 (4)
OT1—Ti8—Ti9	37.1 (3)	OS25—OS31—OS47	54.3 (3)
OS5^iii—Ti8—Ti9	84.6 (3)	OS34—OS31—OS47	118.8 (4)
OHT2—Ti8—Ti9	40.7 (2)	OS44—OS31—OS47	114.0 (4)
OS49—Ti8—Ti9	97.9 (3)	OT1—OS31—OS47	96.8 (3)
OS37—Ti8—OW25^iii	86.5 (5)	Si36—OS32—Ti11	129.8 (6)
OS14—Ti8—OW25^iii	47.4 (4)	Si36—OS32—Na1^vii	122.4 (5)
OT1—Ti8—OW25^iii	140.1 (4)	Ti11—OS32—Na1^vii	98.6 (4)
OS5^iii—Ti8—OW25^iii	43.0 (4)	Si36—OS32—OH15	37.2 (4)
OHT2—Ti8—OW25^iii	103.0 (5)	Ti11—OS32—OH15	132.1 (5)
OS49—Ti8—OW25^iii	134.3 (4)	Na1^vii—OS32—OH15	127.3 (5)
Ti9—Ti8—OW25^iii	121.3 (4)	Si36—OS32—OH9	33.5 (4)
OS37—Ti8—OS3^iii	114.1 (3)	Ti11—OS32—OH9	143.8 (5)
OS14—Ti8—OS3^iii	122.7 (3)	Na1^vii—OS32—OH9	89.2 (4)
OT1—Ti8—OS3^iii	54.9 (3)	OH15—OS32—OH9	60.0 (4)
OS5^iii—Ti8—OS3^iii	50.8 (3)	Si36—OS32—OS26	34.6 (3)
OHT2—Ti8—OS3^iii	55.8 (3)	Ti11—OS32—OS26	95.4 (4)
OS49—Ti8—OS3^iii	131.7 (3)	Na1^vii—OS32—OS26	139.9 (5)
Ti9—Ti8—OS3^iii	33.93 (15)	OH15—OS32—OS26	59.9 (4)
OW25^iii—Ti8—OS3^iii	90.6 (4)	OH9—OS32—OS26	59.1 (4)
OS37—Ti8—Ce2	86.0 (3)	Si36—OS32—OS43	139.2 (5)
OS14—Ti8—Ce2	133.7 (3)	Ti11—OS32—OS43	44.7 (3)
OT1—Ti8—Ce2	40.9 (3)	Na1^vii—OS32—OS43	96.0 (4)
OS5^iii—Ti8—Ce2	137.9 (3)	OH15—OS32—OS43	109.5 (5)
OHT2—Ti8—Ce2	84.6 (2)	OH9—OS32—OS43	169.1 (5)
OS49—Ti8—Ce2	44.7 (3)	OS26—OS32—OS43	119.7 (4)
Ti9—Ti8—Ce2	64.37 (6)	Si36—OS32—OW31^vii	95.7 (6)
OW25^iii—Ti8—Ce2	172.4 (4)	Ti11—OS32—OW31^vii	95.6 (5)
OS3^iii—Ti8—Ce2	93.33 (15)	Na1^vii—OS32—OW31^vii	110.5 (6)
OS37—Ti8—OB27	103.2 (3)	OH15—OS32—OW31^vii	58.9 (5)
OS14—Ti8—OB27	43.2 (3)	OH9—OS32—OW31^vii	114.7 (6)
OT1—Ti8—OB27	129.0 (3)	OS26—OS32—OW31^vii	105.3 (6)
OS5^iii—Ti8—OB27	131.0 (3)	OS43—OS32—OW31^vii	54.4 (5)
OHT2—Ti8—OB27	87.8 (3)	Si36—OS32—OS28	145.7 (6)
OS49—Ti8—OB27	46.7 (3)	Ti11—OS32—OS28	45.5 (3)
Ti9—Ti8—OB27	121.12 (17)	Na1^vii—OS32—OS28	54.3 (3)
OW25^iii—Ti8—OB27	90.3 (4)	OH15—OS32—OS28	176.6 (5)
OS3^iii—Ti8—OB27	142.7 (2)	OH9—OS32—OS28	123.4 (5)
Ce2—Ti8—OB27	90.50 (15)	OS26—OS32—OS28	121.3 (4)
OS37—Ti8—Na2^iii	46.1 (3)	OS43—OS32—OS28	67.1 (3)
OS14—Ti8—Na2^iii	109.2 (3)	OW31^vii—OS32—OS28	117.9 (6)
OT1—Ti8—Na2^iii	83.0 (3)	Si36—OS32—OS44	92.5 (5)
OS5^iii—Ti8—Na2^iii	46.4 (3)	Ti11—OS32—OS44	47.2 (3)
OHT2—Ti8—Na2^iii	127.9 (3)	Na1^vii—OS32—OS44	103.1 (4)
OS49—Ti8—Na2^iii	133.7 (3)	OH15—OS32—OS44	120.8 (5)
Ti9—Ti8—Na2^iii	99.06 (14)	OH9—OS32—OS44	96.6 (4)
OW25^iii—Ti8—Na2^iii	66.5 (4)	OS26—OS32—OS44	61.5 (3)
OS3^iii—Ti8—Na2^iii	72.9 (2)	OS43—OS32—OS44	91.5 (4)
Ce2—Ti8—Na2^iii	108.57 (13)	OW31^vii—OS32—OS44	133.4 (6)
OB27—Ti8—Na2^iii	139.8 (2)	OS28—OS32—OS44	60.0 (3)
OT1—Ti9—OS3^iii	94.8 (4)	Si36—OS32—OT5	92.1 (4)
OT1—Ti9—OS8	92.3 (4)	Ti11—OS32—OT5	41.5 (2)
OS3^iii—Ti9—OS8	86.3 (4)	Na1^vii—OS32—OT5	139.9 (4)
OT1—Ti9—OS6	167.8 (4)	OH15—OS32—OT5	92.3 (4)
OS3^iii—Ti9—OS6	92.4 (4)	OH9—OS32—OT5	120.3 (4)
OS8—Ti9—OS6	98.0 (4)	OS26—OS32—OT5	61.2 (3)
OT1—Ti9—OHT2	76.8 (4)	OS43—OS32—OT5	60.2 (3)
OS3^iii—Ti9—OHT2	92.8 (4)	OW31^vii—OS32—OT5	82.8 (5)
OS8—Ti9—OHT2	168.9 (4)	OS28—OS32—OT5	85.8 (4)
OS6—Ti9—OHT2	93.1 (4)	OS44—OS32—OT5	51.1 (3)
OT1—Ti9—OS41	84.8 (4)	Si36—OS32—Ti10	67.6 (3)
OS3^iii—Ti9—OS41	175.5 (4)	Ti11—OS32—Ti10	62.4 (3)
OS8—Ti9—OS41	89.3 (4)	Na1^vii—OS32—Ti10	139.2 (4)
OS6—Ti9—OS41	88.9 (4)	OH15—OS32—Ti10	85.8 (4)
OHT2—Ti9—OS41	91.5 (4)	OH9—OS32—Ti10	88.9 (4)
OT1—Ti9—Ti8	37.9 (3)	OS26—OS32—Ti10	33.0 (2)
OS3^iii—Ti9—Ti8	84.5 (3)	OS43—OS32—Ti10	93.3 (3)
OS8—Ti9—Ti8	127.8 (3)	OW31^vii—OS32—Ti10	107.3 (5)
OS6—Ti9—Ti8	133.6 (3)	OS28—OS32—Ti10	94.2 (3)
OHT2—Ti9—Ti8	41.2 (3)	OS44—OS32—Ti10	36.8 (2)
OS41—Ti9—Ti8	97.7 (3)	OT5—OS32—Ti10	33.5 (2)
OT1—Ti9—OS5^iii	57.4 (3)	Si4—OS33—Ti2	134.5 (5)
OS3^iii—Ti9—OS5^iii	50.6 (3)	Si4—OS33—OB28	38.6 (3)
OS8—Ti9—OS5^iii	118.3 (3)	Ti2—OS33—OB28	154.4 (5)
OS6—Ti9—OS5^iii	121.7 (3)	Si4—OS33—OS29	152.9 (6)
OHT2—Ti9—OS5^iii	54.1 (3)	Ti2—OS33—OS29	47.1 (3)
OS41—Ti9—OS5^iii	131.7 (3)	OB28—OS33—OS29	124.4 (5)
Ti8—Ti9—OS5^iii	34.00 (15)	Si4—OS33—OB26	35.2 (3)
OT1—Ti9—Na6^vii	143.5 (3)	Ti2—OS33—OB26	131.9 (5)
OS3^iii—Ti9—Na6^vii	88.1 (3)	OB28—OS33—OB26	60.5 (4)
OS8—Ti9—Na6^vii	51.6 (3)	OS29—OS33—OB26	171.7 (5)
OS6—Ti9—Na6^vii	46.5 (3)	Si4—OS33—OS36	33.9 (3)
OHT2—Ti9—Na6^vii	139.5 (3)	Ti2—OS33—OS36	102.4 (4)
OS41—Ti9—Na6^vii	89.6 (3)	OB28—OS33—OS36	61.7 (4)
Ti8—Ti9—Na6^vii	172.66 (17)	OS29—OS33—OS36	127.0 (5)
OS5^iii—Ti9—Na6^vii	138.7 (2)	OB26—OS33—OS36	60.7 (4)
OT1—Ti9—Ce2	41.7 (3)	Si4—OS33—OS2	93.1 (4)
OS3^iii—Ti9—Ce2	135.5 (3)	Ti2—OS33—OS2	47.2 (3)
OS8—Ti9—Ce2	86.9 (3)	OB28—OS33—OS2	130.8 (4)
OS6—Ti9—Ce2	132.1 (3)	OS29—OS33—OS2	94.4 (4)
OHT2—Ti9—Ce2	86.0 (3)	OB26—OS33—OS2	85.4 (4)
OS41—Ti9—Ce2	43.4 (2)	OS36—OS33—OS2	71.1 (3)
Ti8—Ti9—Ce2	65.81 (6)	Si4—OS33—OT6	101.7 (5)
OS5^iii—Ti9—Ce2	96.01 (16)	Ti2—OS33—OT6	42.2 (3)
Na6^vii—Ti9—Ce2	120.28 (16)	OB28—OS33—OT6	112.6 (4)
OT1—Ti9—OB37	127.3 (3)	OS29—OS33—OT6	61.7 (3)
OS3^iii—Ti9—OB37	135.6 (3)	OB26—OS33—OT6	124.2 (4)
OS8—Ti9—OB37	103.4 (3)	OS36—OS33—OT6	68.2 (3)
OS6—Ti9—OB37	43.7 (3)	OS2—OS33—OT6	57.0 (3)
OHT2—Ti9—OB37	85.0 (3)	Si4—OS33—OS12	143.9 (5)
OS41—Ti9—OB37	46.3 (3)	Ti2—OS33—OS12	41.0 (3)
Ti8—Ti9—OB37	118.54 (16)	OB28—OS33—OS12	164.1 (5)
OS5^iii—Ti9—OB37	138.2 (2)	OS29—OS33—OS12	59.8 (3)
Na6^vii—Ti9—OB37	67.1 (2)	OB26—OS33—OS12	113.6 (4)
Ce2—Ti9—OB37	88.64 (15)	OS36—OS33—OS12	130.4 (4)
OT1—Ti9—Na4^iii	133.9 (3)	OS2—OS33—OS12	59.3 (3)
OS3^iii—Ti9—Na4^iii	40.0 (3)	OT6—OS33—OS12	83.1 (3)
OS8—Ti9—Na4^iii	92.7 (3)	Si4—OS33—Ba^ix	100.0 (4)
OS6—Ti9—Na4^iii	52.4 (3)	Ti2—OS33—Ba^ix	107.4 (4)
OHT2—Ti9—Na4^iii	93.7 (3)	OB28—OS33—Ba^ix	62.9 (3)
OS41—Ti9—Na4^iii	141.1 (3)	OS29—OS33—Ba^ix	62.5 (3)
Ti8—Ti9—Na4^iii	111.21 (15)	OB26—OS33—Ba^ix	120.4 (4)
OS5^iii—Ti9—Na4^iii	80.2 (2)	OS36—OS33—Ba^ix	106.1 (4)
Na6^vii—Ti9—Na4^iii	62.4 (2)	OS2—OS33—Ba^ix	149.7 (4)
Ce2—Ti9—Na4^iii	175.48 (14)	OT6—OS33—Ba^ix	93.4 (3)
OB37—Ti9—Na4^iii	95.84 (19)	OS12—OS33—Ba^ix	115.6 (3)
OS25—Ti10—OS26	91.2 (4)	Si4—OS33—OW13^ix	90.9 (4)
OS25—Ti10—OT5	95.6 (4)	Ti2—OS33—OW13^ix	134.6 (5)
OS26—Ti10—OT5	95.5 (4)	OB28—OS33—OW13^ix	61.2 (4)
OS25—Ti10—OS34	103.1 (4)	OS29—OS33—OW13^ix	94.0 (4)
OS26—Ti10—OS34	91.4 (4)	OB26—OS33—OW13^ix	82.8 (4)
OT5—Ti10—OS34	160.0 (4)	OS36—OS33—OW13^ix	122.0 (4)
OS25—Ti10—OS31	89.0 (4)	OS2—OS33—OW13^ix	153.3 (5)
OS26—Ti10—OS31	179.6 (5)	OT6—OS33—OW13^ix	147.1 (4)
OT5—Ti10—OS31	84.9 (4)	OS12—OS33—OW13^ix	104.3 (4)
OS34—Ti10—OS31	88.2 (4)	Ba^ix—OS33—OW13^ix	54.3 (3)
OS25—Ti10—OS44	171.1 (4)	Si4—OS33—OW21	128.8 (6)
OS26—Ti10—OS44	89.0 (4)	Ti2—OS33—OW21	89.0 (5)
OT5—Ti10—OS44	75.5 (4)	OB28—OS33—OW21	112.7 (5)
OS34—Ti10—OS44	85.8 (4)	OS29—OS33—OW21	73.5 (5)
OS31—Ti10—OS44	90.9 (3)	OB26—OS33—OW21	98.6 (5)
OS25—Ti10—Ti11	129.8 (3)	OS36—OS33—OW21	159.0 (6)
OS26—Ti10—Ti11	82.9 (3)	OS2—OS33—OW21	106.1 (5)
OT5—Ti10—Ti11	36.5 (3)	OT6—OS33—OW21	128.7 (5)
OS34—Ti10—Ti11	126.8 (3)	OS12—OS33—OW21	52.0 (4)
OS31—Ti10—Ti11	97.4 (2)	Ba^ix—OS33—OW21	86.7 (4)
OS44—Ti10—Ti11	41.4 (3)	OW13^ix—OS33—OW21	52.6 (4)
OS25—Ti10—OS32	120.5 (4)	Si35—OS34—Ti10	131.2 (6)
OS26—Ti10—OS32	49.5 (3)	Si35—OS34—OB23	37.0 (3)
OT5—Ti10—OS32	56.0 (3)	Ti10—OS34—OB23	106.4 (4)
OS34—Ti10—OS32	117.8 (3)	Si35—OS34—OB22	37.5 (3)
OS31—Ti10—OS32	130.7 (3)	Ti10—OS34—OB22	104.6 (4)
OS44—Ti10—OS32	53.9 (3)	OB23—OS34—OB22	60.1 (4)
Ti11—Ti10—OS32	33.35 (16)	Si35—OS34—Na3	112.6 (5)
OS25—Ti10—Na3	108.1 (3)	Ti10—OS34—Na3	98.2 (5)
OS26—Ti10—Na3	43.4 (4)	OB23—OS34—Na3	149.6 (5)
OT5—Ti10—Na3	130.8 (3)	OB22—OS34—Na3	96.9 (4)
OS34—Ti10—Na3	49.2 (4)	Si35—OS34—OH16	31.3 (3)
OS31—Ti10—Na3	136.2 (3)	Ti10—OS34—OH16	162.3 (5)
OS44—Ti10—Na3	77.9 (3)	OB23—OS34—OH16	60.0 (4)
Ti11—Ti10—Na3	101.1 (2)	OB22—OS34—OH16	59.5 (4)
OS32—Ti10—Na3	74.9 (2)	Na3—OS34—OH16	91.9 (4)
OS25—Ti10—Ce2	88.2 (3)	Si35—OS34—OS44	94.4 (5)
OS26—Ti10—Ce2	136.9 (3)	Ti10—OS34—OS44	49.6 (3)
OT5—Ti10—Ce2	41.8 (3)	OB23—OS34—OS44	96.4 (4)
OS34—Ti10—Ce2	130.6 (3)	OB22—OS34—OS44	58.6 (3)
OS31—Ti10—Ce2	43.5 (2)	Na3—OS34—OS44	86.0 (4)
OS44—Ti10—Ce2	85.6 (3)	OH16—OS34—OS44	117.3 (4)
Ti11—Ti10—Ce2	65.27 (6)	Si35—OS34—OS26	151.8 (6)
OS32—Ti10—Ce2	95.02 (16)	Ti10—OS34—OS26	44.2 (3)
Na3—Ti10—Ce2	163.48 (18)	OB23—OS34—OS26	150.1 (5)
OS25—Ti10—OW36	47.0 (4)	OB22—OS34—OS26	114.8 (4)
OS26—Ti10—OW36	51.0 (4)	Na3—OS34—OS26	55.0 (4)
OT5—Ti10—OW36	77.6 (4)	OH16—OS34—OS26	146.5 (5)
OS34—Ti10—OW36	120.7 (4)	OS44—OS34—OS26	61.7 (3)
OS31—Ti10—OW36	129.3 (4)	Si35—OS34—OS31	90.0 (5)
OS44—Ti10—OW36	128.4 (4)	Ti10—OS34—OS31	48.3 (3)
Ti11—Ti10—OW36	95.8 (3)	OB23—OS34—OS31	58.5 (3)
OS32—Ti10—OW36	74.6 (3)	OB22—OS34—OS31	85.0 (4)
Na3—Ti10—OW36	87.9 (3)	Na3—OS34—OS31	145.0 (5)
Ce2—Ti10—OW36	102.2 (3)	OH16—OS34—OS31	118.2 (5)
OS25—Ti10—OB22	142.7 (4)	OS44—OS34—OS31	65.1 (3)
OS26—Ti10—OB22	105.4 (4)	OS26—OS34—OS31	92.4 (4)
OT5—Ti10—OB22	115.3 (3)	Si35—OS34—OS25	143.1 (6)
OS34—Ti10—OB22	44.7 (3)	Ti10—OS34—OS25	38.0 (3)
OS31—Ti10—OB22	74.3 (3)	OB23—OS34—OS25	106.1 (4)
OS44—Ti10—OB22	45.3 (3)	OB22—OS34—OS25	138.6 (4)
Ti11—Ti10—OB22	86.03 (16)	Na3—OS34—OS25	104.3 (4)
OS32—Ti10—OB22	94.9 (2)	OH16—OS34—OS25	151.5 (5)
Na3—Ti10—OB22	67.8 (2)	OS44—OS34—OS25	87.6 (4)
Ce2—Ti10—OB22	100.76 (15)	OS26—OS34—OS25	56.3 (3)
OW36—Ti10—OB22	155.5 (3)	OS31—OS34—OS25	57.5 (3)
OS43—Ti11—OS32	89.3 (4)	Si35—OS34—Si34	70.2 (4)
OS43—Ti11—OT5	94.4 (4)	Ti10—OS34—Si34	81.6 (3)
OS32—Ti11—OT5	97.1 (4)	OB23—OS34—Si34	88.8 (4)
OS43—Ti11—OS28	102.5 (4)	OB22—OS34—Si34	32.9 (2)
OS32—Ti11—OS28	90.1 (4)	Na3—OS34—Si34	77.3 (3)
OT5—Ti11—OS28	161.7 (4)	OH16—OS34—Si34	86.6 (4)
OS43—Ti11—OS1	90.3 (4)	OS44—OS34—Si34	32.0 (2)
OS32—Ti11—OS1	179.0 (4)	OS26—OS34—Si34	81.9 (3)
OT5—Ti11—OS1	83.8 (3)	OS31—OS34—Si34	86.6 (3)
OS28—Ti11—OS1	89.1 (4)	OS25—OS34—Si34	119.5 (4)
OS43—Ti11—OS44	170.0 (4)	Si35—OS34—Si26	68.0 (4)
OS32—Ti11—OS44	89.6 (4)	Ti10—OS34—Si26	78.5 (3)
OT5—Ti11—OS44	75.9 (4)	OB23—OS34—Si26	31.5 (2)
OS28—Ti11—OS44	87.4 (4)	OB22—OS34—Si26	80.9 (3)
OS1—Ti11—OS44	90.9 (4)	Na3—OS34—Si26	175.4 (4)
OS43—Ti11—Ti10	128.0 (3)	OH16—OS34—Si26	90.5 (4)
OS32—Ti11—Ti10	84.3 (3)	OS44—OS34—Si26	89.3 (3)
OT5—Ti11—Ti10	36.3 (3)	OS26—OS34—Si26	122.2 (4)
OS28—Ti11—Ti10	128.9 (3)	OS31—OS34—Si26	31.0 (2)
OS1—Ti11—Ti10	96.6 (3)	OS25—OS34—Si26	75.1 (3)
OS44—Ti11—Ti10	42.0 (3)	Si34—OS34—Si26	98.9 (3)
OS43—Ti11—Na1^vii	89.5 (3)	Si1—OS35—Ti3	128.2 (5)
OS32—Ti11—Na1^vii	47.5 (3)	Si1—OS35—Ce1	127.8 (5)
OT5—Ti11—Na1^vii	144.4 (3)	Ti3—OS35—Ce1	102.6 (4)
OS28—Ti11—Na1^vii	44.1 (3)	Si1—OS35—OB10	35.9 (3)
OS1—Ti11—Na1^vii	131.6 (3)	Ti3—OS35—OB10	101.9 (4)
OS44—Ti11—Na1^vii	97.1 (3)	Ce1—OS35—OB10	151.5 (5)
Ti10—Ti11—Na1^vii	120.58 (18)	Si1—OS35—OB7	35.5 (4)
OS43—Ti11—OS26	117.8 (3)	Ti3—OS35—OB7	108.1 (4)
OS32—Ti11—OS26	50.7 (3)	Ce1—OS35—OB7	124.8 (4)
OT5—Ti11—OS26	55.7 (3)	OB10—OS35—OB7	59.0 (4)
OS28—Ti11—OS26	119.7 (3)	Si1—OS35—OT3^ii	173.2 (6)
OS1—Ti11—OS26	130.2 (3)	Ti3—OS35—OT3^ii	45.7 (3)
OS44—Ti11—OS26	54.8 (3)	Ce1—OS35—OT3^ii	57.5 (3)
Ti10—Ti11—OS26	33.55 (17)	OB10—OS35—OT3^ii	142.0 (5)
Na1^vii—Ti11—OS26	91.4 (2)	OB7—OS35—OT3^ii	139.0 (5)
OS43—Ti11—OW31^vii	43.1 (4)	Si1—OS35—OS11	31.7 (3)
OS32—Ti11—OW31^vii	51.1 (4)	Ti3—OS35—OS11	158.8 (5)
OT5—Ti11—OW31^vii	81.1 (4)	Ce1—OS35—OS11	98.5 (4)
OS28—Ti11—OW31^vii	116.1 (4)	OB10—OS35—OS11	57.5 (3)
OS1—Ti11—OW31^vii	128.8 (4)	OB7—OS35—OS11	58.8 (4)
OS44—Ti11—OW31^vii	131.1 (4)	OT3^ii—OS35—OS11	154.9 (5)
Ti10—Ti11—OW31^vii	99.1 (3)	Si1—OS35—OS40	86.5 (4)
Na1^vii—Ti11—OW31^vii	77.8 (4)	Ti3—OS35—OS40	44.0 (3)
OS26—Ti11—OW31^vii	76.6 (4)	Ce1—OS35—OS40	145.8 (4)
OS43—Ti11—OS48	46.9 (3)	OB10—OS35—OS40	58.1 (3)
OS32—Ti11—OS48	120.0 (3)	OB7—OS35—OS40	81.3 (4)
OT5—Ti11—OS48	58.0 (3)	OT3^ii—OS35—OS40	88.4 (4)
OS28—Ti11—OS48	131.4 (3)	OS11—OS35—OS40	114.9 (4)
OS1—Ti11—OS48	60.2 (3)	Si1—OS35—OS4	111.8 (5)
OS44—Ti11—OS48	126.3 (3)	Ti3—OS35—OS4	41.7 (3)
Ti10—Ti11—OS48	93.75 (16)	Ce1—OS35—OS4	97.5 (3)
Na1^vii—Ti11—OS48	136.4 (2)	OB10—OS35—OS4	110.4 (4)
OS26—Ti11—OS48	108.7 (2)	OB7—OS35—OS4	78.2 (4)
OW31^vii—Ti11—OS48	70.4 (4)	OT3^ii—OS35—OS4	61.8 (3)
OS43—Ti11—Ce2	89.1 (3)	OS11—OS35—OS4	135.8 (5)
OS32—Ti11—Ce2	137.8 (3)	OS40—OS35—OS4	63.7 (3)
OT5—Ti11—Ce2	41.0 (3)	Si1—OS35—OT7^ii	127.4 (5)
OS28—Ti11—Ce2	131.3 (3)	Ti3—OS35—OT7^ii	44.8 (3)
OS1—Ti11—Ce2	43.1 (2)	Ce1—OS35—OT7^ii	95.5 (3)
OS44—Ti11—Ce2	85.0 (2)	OB10—OS35—OT7^ii	91.8 (4)
Ti10—Ti11—Ce2	64.16 (6)	OB7—OS35—OT7^ii	138.1 (4)
Na1^vii—Ti11—Ce2	174.53 (16)	OT3^ii—OS35—OT7^ii	52.1 (3)
OS26—Ti11—Ce2	93.93 (17)	OS11—OS35—OT7^ii	132.4 (5)
OW31^vii—Ti11—Ce2	104.7 (3)	OS40—OS35—OT7^ii	57.0 (3)
OS48—Ti11—Ce2	42.35 (14)	OS4—OS35—OT7^ii	86.2 (4)
OS38—Ti12—OT2	98.6 (4)	Si1—OS35—OT4^i	87.7 (4)
OS38—Ti12—OS39	89.3 (4)	Ti3—OS35—OT4^i	139.6 (5)
OT2—Ti12—OS39	94.0 (4)	Ce1—OS35—OT4^i	52.0 (2)
OS38—Ti12—OS24	96.7 (4)	OB10—OS35—OT4^i	99.5 (4)
OT2—Ti12—OS24	164.1 (4)	OB7—OS35—OT4^i	112.3 (4)
OS39—Ti12—OS24	90.8 (4)	OT3^ii—OS35—OT4^i	99.1 (4)
OS38—Ti12—OS47	89.3 (4)	OS11—OS35—OT4^i	56.6 (3)
OT2—Ti12—OS47	85.5 (4)	OS40—OS35—OT4^i	144.5 (5)
OS39—Ti12—OS47	178.3 (4)	OS4—OS35—OT4^i	149.0 (4)
OS24—Ti12—OS47	90.1 (4)	OT7^ii—OS35—OT4^i	101.1 (4)
OS38—Ti12—OHT1	174.1 (4)	Si1—OS35—Si2	65.7 (3)
OT2—Ti12—OHT1	75.5 (4)	Ti3—OS35—Si2	72.2 (3)
OS39—Ti12—OHT1	91.3 (4)	Ce1—OS35—Si2	156.4 (4)
OS24—Ti12—OHT1	89.2 (4)	OB10—OS35—Si2	31.1 (2)
OS47—Ti12—OHT1	90.1 (4)	OB7—OS35—Si2	77.9 (3)
OS38—Ti12—Ti7	134.2 (3)	OT3^ii—OS35—Si2	111.2 (4)
OT2—Ti12—Ti7	37.5 (3)	OS11—OS35—Si2	88.0 (3)
OS39—Ti12—Ti7	83.6 (3)	OS40—OS35—Si2	30.8 (3)
OS24—Ti12—Ti7	128.5 (3)	OS4—OS35—Si2	93.2 (3)
OS47—Ti12—Ti7	96.9 (3)	OT7^ii—OS35—Si2	64.2 (3)
OHT1—Ti12—Ti7	40.1 (3)	OT4^i—OS35—Si2	117.2 (4)
OS38—Ti12—OS22	122.1 (4)	Si4—OS36—Ti4	127.5 (5)
OT2—Ti12—OS22	55.9 (3)	Si4—OS36—Ce1	129.5 (5)
OS39—Ti12—OS22	49.3 (4)	Ti4—OS36—Ce1	102.6 (4)
OS24—Ti12—OS22	118.4 (4)	Si4—OS36—OS33	33.0 (3)
OS47—Ti12—OS22	131.2 (3)	Ti4—OS36—OS33	156.3 (5)
OHT1—Ti12—OS22	54.8 (3)	Ce1—OS36—OS33	99.5 (3)
Ti7—Ti12—OS22	34.31 (17)	Si4—OS36—OT4^i	173.0 (6)
OS38—Ti12—OS49	47.6 (3)	Ti4—OS36—OT4^i	46.4 (3)
OT2—Ti12—OS49	59.7 (3)	Ce1—OS36—OT4^i	56.2 (3)
OS39—Ti12—OS49	116.3 (3)	OS33—OS36—OT4^i	153.9 (5)
OS24—Ti12—OS49	130.7 (4)	Si4—OS36—OB28	35.1 (3)
OS47—Ti12—OS49	62.0 (3)	Ti4—OS36—OB28	99.5 (4)
OHT1—Ti12—OS49	127.3 (3)	Ce1—OS36—OB28	152.3 (4)
Ti7—Ti12—OS49	96.49 (16)	OS33—OS36—OB28	57.0 (3)
OS22—Ti12—OS49	110.2 (2)	OT4^i—OS36—OB28	142.1 (5)
OS38—Ti12—Ce2	89.9 (3)	Si4—OS36—OB26	34.6 (3)
OT2—Ti12—Ce2	41.6 (3)	Ti4—OS36—OB26	112.4 (4)
OS39—Ti12—Ce2	134.7 (3)	Ce1—OS36—OB26	125.3 (4)
OS24—Ti12—Ce2	134.2 (3)	OS33—OS36—OB26	59.4 (3)
OS47—Ti12—Ce2	44.5 (3)	OT4^i—OS36—OB26	140.3 (5)
OHT1—Ti12—Ce2	85.4 (3)	OB28—OS36—OB26	58.5 (4)
Ti7—Ti12—Ce2	65.40 (6)	Si4—OS36—OS11	112.7 (5)
OS22—Ti12—Ce2	94.95 (17)	Ti4—OS36—OS11	45.9 (3)
OS49—Ti12—Ce2	42.82 (15)	Ce1—OS36—OS11	96.7 (4)
OS38—Ti12—OB20	98.7 (4)	OS33—OS36—OS11	139.1 (5)
OT2—Ti12—OB20	127.8 (3)	OT4^i—OS36—OS11	60.8 (4)
OS39—Ti12—OB20	135.0 (3)	OB28—OS36—OS11	110.7 (4)
OS24—Ti12—OB20	44.4 (3)	OB26—OS36—OS11	80.7 (4)
OS47—Ti12—OB20	46.1 (3)	Si4—OS36—OS18	84.0 (4)
OHT1—Ti12—OB20	85.1 (3)	Ti4—OS36—OS18	44.2 (3)
Ti7—Ti12—OB20	117.98 (19)	Ce1—OS36—OS18	146.5 (5)
OS22—Ti12—OB20	138.9 (3)	OS33—OS36—OS18	112.9 (4)
OS49—Ti12—OB20	100.8 (2)	OT4^i—OS36—OS18	90.4 (4)
Ce2—Ti12—OB20	89.78 (16)	OB28—OS36—OS18	56.4 (3)
OS38—Ti12—OS48	128.6 (3)	OB26—OS36—OS18	80.7 (4)
OT2—Ti12—OS48	38.6 (3)	OS11—OS36—OS18	64.3 (4)
OS39—Ti12—OS48	114.2 (3)	Si4—OS36—OHT4^i	127.4 (5)
OS24—Ti12—OS48	126.0 (3)	Ti4—OS36—OHT4^i	41.3 (3)
OS47—Ti12—OS48	66.2 (3)	Ce1—OS36—OHT4^i	93.0 (4)
OHT1—Ti12—OS48	46.1 (3)	OS33—OS36—OHT4^i	129.4 (4)
Ti7—Ti12—OS48	30.74 (14)	OT4^i—OS36—OHT4^i	51.9 (3)
OS22—Ti12—OS48	65.0 (2)	OB28—OS36—OHT4^i	92.6 (4)
OS49—Ti12—OS48	81.21 (19)	OB26—OS36—OHT4^i	140.6 (4)
Ce2—Ti12—OS48	40.62 (12)	OS11—OS36—OHT4^i	86.5 (4)
OB20—Ti12—OS48	94.9 (2)	OS18—OS36—OHT4^i	60.3 (4)
OS11—Si1—OS35	116.1 (5)	Si4—OS36—OT6	90.8 (4)
OS11—Si1—OB7	109.9 (6)	Ti4—OS36—OT6	133.8 (5)
OS35—Si1—OB7	109.4 (6)	Ce1—OS36—OT6	50.9 (2)
OS11—Si1—OB10	106.1 (5)	OS33—OS36—OT6	58.1 (3)
OS35—Si1—OB10	108.9 (5)	OT4^i—OS36—OT6	96.2 (4)
OB7—Si1—OB10	105.8 (6)	OB28—OS36—OT6	101.5 (4)
OS11—Si1—OS40	157.6 (5)	OB26—OS36—OT6	113.6 (4)
OS35—Si1—OS40	62.2 (4)	OS11—OS36—OT6	147.5 (4)
OB7—Si1—OS40	90.6 (4)	OS18—OS36—OT6	144.0 (4)
OB10—Si1—OS40	57.8 (4)	OHT4^i—OS36—OT6	97.0 (4)
OS11—Si1—OS36	58.1 (4)	Si4—OS36—OS2	78.5 (4)
OS35—Si1—OS36	73.4 (4)	Ti4—OS36—OS2	147.7 (5)
OB7—Si1—OS36	90.6 (4)	Ce1—OS36—OS2	52.4 (2)
OB10—Si1—OS36	161.0 (5)	OS33—OS36—OS2	55.5 (3)
OS40—Si1—OS36	133.2 (3)	OT4^i—OS36—OS2	106.0 (4)
OS11—Si1—Na8	44.0 (4)	OB28—OS36—OS2	111.1 (4)
OS35—Si1—Na8	119.9 (4)	OB26—OS36—OS2	77.2 (3)
OB7—Si1—Na8	130.4 (4)	OS11—OS36—OS2	110.6 (4)
OB10—Si1—Na8	63.4 (4)	OS18—OS36—OS2	157.9 (5)
OS40—Si1—Na8	115.4 (3)	OHT4^i—OS36—OS2	141.8 (4)
OS36—Si1—Na8	98.6 (3)	OT6—OS36—OS2	50.4 (3)
OS11—Si1—OT4^i	53.4 (4)	Si26—OS37—Ti8	135.7 (5)
OS35—Si1—OT4^i	63.6 (4)	Si26—OS37—OB23	37.1 (3)
OB7—Si1—OT4^i	138.2 (4)	Ti8—OS37—OB23	154.2 (5)
OB10—Si1—OT4^i	115.5 (5)	Si26—OS37—OB24	35.4 (3)
OS40—Si1—OT4^i	116.1 (3)	Ti8—OS37—OB24	132.4 (5)
OS36—Si1—OT4^i	47.7 (2)	OB23—OS37—OB24	60.0 (4)
Na8—Si1—OT4^i	68.2 (3)	Si26—OS37—OS31	32.7 (3)
OS11—Si1—OB26	76.4 (4)	Ti8—OS37—OS31	104.4 (4)
OS35—Si1—OB26	99.5 (4)	OB23—OS37—OS31	59.8 (3)
OB7—Si1—OB26	45.1 (4)	OB24—OS37—OS31	59.1 (3)
OB10—Si1—OB26	145.9 (5)	Si26—OS37—OS5^iii	157.0 (5)
OS40—Si1—OB26	125.8 (3)	Ti8—OS37—OS5^iii	45.3 (3)
OS36—Si1—OB26	46.6 (2)	OB23—OS37—OS5^iii	128.2 (5)
Na8—Si1—OB26	117.5 (3)	OB24—OS37—OS5^iii	167.5 (5)
OT4^i—Si1—OB26	93.7 (2)	OS31—OS37—OS5^iii	132.1 (4)
OH6—Si2—OS40	114.5 (6)	Si26—OS37—OT1	100.7 (4)
OH6—Si2—OB10	110.1 (6)	Ti8—OS37—OT1	45.1 (3)
OS40—Si2—OB10	107.7 (5)	OB23—OS37—OT1	109.4 (4)
OH6—Si2—OB29^ii	110.9 (6)	OB24—OS37—OT1	124.3 (4)
OS40—Si2—OB29^ii	107.5 (5)	OS31—OS37—OT1	68.8 (3)
OB10—Si2—OB29^ii	105.7 (6)	OS5^iii—OS37—OT1	64.4 (3)
OH6—Si2—OS35	158.0 (5)	Si26—OS37—Na2^iii	105.5 (5)
OS40—Si2—OS35	60.4 (4)	Ti8—OS37—Na2^iii	103.5 (4)
OB10—Si2—OS35	57.0 (4)	OB23—OS37—Na2^iii	69.2 (4)
OB29^ii—Si2—OS35	90.6 (4)	OB24—OS37—Na2^iii	124.1 (4)
OH6—Si2—OT7^ii	144.0 (5)	OS31—OS37—Na2^iii	113.1 (4)
OS40—Si2—OT7^ii	56.4 (4)	OS5^iii—OS37—Na2^iii	60.3 (3)
OB10—Si2—OT7^ii	105.6 (4)	OT1—OS37—Na2^iii	92.6 (4)
OB29^ii—Si2—OT7^ii	53.3 (4)	Si26—OS37—OS49	94.2 (4)
OS35—Si2—OT7^ii	54.0 (2)	Ti8—OS37—OS49	46.9 (3)
OH6—Si2—Na1	33.4 (4)	OB23—OS37—OS49	130.1 (4)
OS40—Si2—Na1	89.9 (4)	OB24—OS37—OS49	86.5 (4)
OB10—Si2—Na1	99.0 (4)	OS31—OS37—OS49	71.6 (3)
OB29^ii—Si2—Na1	143.2 (4)	OS5^iii—OS37—OS49	92.2 (4)
OS35—Si2—Na1	125.9 (3)	OT1—OS37—OS49	58.4 (3)
OT7^ii—Si2—Na1	142.9 (3)	Na2^iii—OS37—OS49	147.8 (4)
OH6—Si2—OW29	74.2 (5)	Si26—OS37—OS14	143.7 (5)
OS40—Si2—OW29	54.5 (5)	Ti8—OS37—OS14	39.3 (2)
OB10—Si2—OW29	90.0 (5)	OB23—OS37—OS14	166.3 (4)
OB29^ii—Si2—OW29	159.8 (5)	OB24—OS37—OS14	113.6 (4)
OS35—Si2—OW29	87.3 (4)	OS31—OS37—OS14	129.3 (4)
OT7^ii—Si2—OW29	110.7 (4)	OS5^iii—OS37—OS14	56.0 (3)
Na1—Si2—OW29	41.3 (3)	OT1—OS37—OS14	84.3 (3)
OS18—Si3—OB28	107.2 (6)	Na2^iii—OS37—OS14	110.1 (4)
OS18—Si3—OH11	112.9 (8)	OS49—OS37—OS14	57.7 (3)
OB28—Si3—OH11	108.2 (8)	Si26—OS37—OW14^iii	85.4 (4)
OS18—Si3—OH10	111.9 (9)	Ti8—OS37—OW14^iii	88.9 (3)
OB28—Si3—OH10	108.5 (8)	OB23—OS37—OW14^iii	67.4 (3)
OH11—Si3—OH10	107.9 (9)	OB24—OS37—OW14^iii	120.5 (4)
OS18—Si3—OS36	55.5 (4)	OS31—OS37—OW14^iii	71.9 (3)
OB28—Si3—OS36	51.7 (4)	OS5^iii—OS37—OW14^iii	71.7 (3)
OH11—Si3—OS36	125.5 (7)	OT1—OS37—OW14^iii	52.3 (3)
OH10—Si3—OS36	126.2 (7)	Na2^iii—OS37—OW14^iii	49.3 (3)
OS18—Si3—OB26	81.7 (5)	OS49—OS37—OW14^iii	109.1 (4)
OB28—Si3—OB26	48.3 (4)	OS14—OS37—OW14^iii	123.4 (4)
OH11—Si3—OB26	156.3 (7)	Si26—OS37—OW7^iii	117.9 (11)
OH10—Si3—OB26	81.5 (7)	Ti8—OS37—OW7^iii	106.3 (10)
OS36—Si3—OB26	46.8 (2)	OB23—OS37—OW7^iii	86.1 (10)
OS18—Si3—Na14	38.2 (4)	OB24—OS37—OW7^iii	107.8 (10)
OB28—Si3—Na14	144.4 (5)	OS31—OS37—OW7^iii	145.8 (10)
OH11—Si3—Na14	97.2 (7)	OS5^iii—OS37—OW7^iii	66.3 (10)
OH10—Si3—Na14	85.9 (7)	OT1—OS37—OW7^iii	126.7 (10)
OS36—Si3—Na14	93.3 (3)	Na2^iii—OS37—OW7^iii	44.5 (10)
OB26—Si3—Na14	105.2 (3)	OS49—OS37—OW7^iii	142.2 (10)
OS18—Si3—OW30	79.9 (10)	OS14—OS37—OW7^iii	84.7 (10)
OB28—Si3—OW30	121.7 (10)	OW14^iii—OS37—OW7^iii	93.8 (10)
OH11—Si3—OW30	122.0 (11)	Si23—OS38—Ti12	134.6 (5)
OH10—Si3—OW30	32.0 (11)	Si23—OS38—OB27	36.7 (3)
OS36—Si3—OW30	108.6 (9)	Ti12—OS38—OB27	151.9 (5)
OB26—Si3—OW30	77.6 (9)	Si23—OS38—OS39	148.9 (6)
Na14—Si3—OW30	57.6 (9)	Ti12—OS38—OS39	46.0 (3)
OS18—Si3—OW38^i	77.6 (7)	OB27—OS38—OS39	123.3 (5)
OB28—Si3—OW38^i	93.7 (7)	Si23—OS38—OB25	35.2 (3)
OH11—Si3—OW38^i	45.4 (8)	Ti12—OS38—OB25	134.3 (5)
OH10—Si3—OW38^i	150.8 (9)	OB27—OS38—OB25	58.8 (3)
OS36—Si3—OW38^i	82.4 (6)	OS39—OS38—OB25	175.6 (5)
OB26—Si3—OW38^i	127.7 (6)	Si23—OS38—OS49	33.9 (3)
Na14—Si3—OW38^i	86.6 (6)	Ti12—OS38—OS49	101.4 (4)
OW30—Si3—OW38^i	142.4 (11)	OB27—OS38—OS49	61.4 (3)
OS18—Si3—OW40^viii	121.5 (9)	OS39—OS38—OS49	124.7 (4)
OB28—Si3—OW40^viii	60.7 (9)	OB25—OS38—OS49	59.6 (3)
OH11—Si3—OW40^viii	125.4 (10)	Si23—OS38—OS47	95.2 (4)
OH10—Si3—OW40^viii	48.0 (10)	Ti12—OS38—OS47	47.6 (3)
OS36—Si3—OW40^viii	91.0 (8)	OB27—OS38—OS47	131.1 (4)
OB26—Si3—OW40^viii	46.0 (8)	OS39—OS38—OS47	93.6 (4)
Na14—Si3—OW40^viii	122.3 (7)	OB25—OS38—OS47	87.0 (4)
OW30—Si3—OW40^viii	66.7 (11)	OS49—OS38—OS47	71.4 (3)
OW38^i—Si3—OW40^viii	150.8 (9)	Si23—OS38—OS24	147.9 (6)
OS33—Si4—OS36	113.1 (5)	Ti12—OS38—OS24	42.3 (3)
OS33—Si4—OB26	111.0 (5)	OB27—OS38—OS24	164.6 (5)
OS36—Si4—OB26	111.3 (5)	OS39—OS38—OS24	59.5 (4)
OS33—Si4—OB28	104.5 (5)	OB25—OS38—OS24	117.3 (5)
OS36—Si4—OB28	110.4 (5)	OS49—OS38—OS24	131.5 (4)
OB26—Si4—OB28	106.1 (5)	OS47—OS38—OS24	60.1 (3)
OS33—Si4—OS18	154.3 (5)	Si23—OS38—OT2	100.4 (4)
OS36—Si4—OS18	64.5 (4)	Ti12—OS38—OT2	41.2 (3)
OB26—Si4—OS18	92.6 (5)	OB27—OS38—OT2	111.4 (4)
OB28—Si4—OS18	57.3 (4)	OS39—OS38—OT2	60.6 (3)
OS33—Si4—OS2	57.7 (4)	OB25—OS38—OT2	123.0 (4)
OS36—Si4—OS2	72.2 (4)	OS49—OS38—OT2	67.2 (3)
OB26—Si4—OS2	91.2 (4)	OS47—OS38—OT2	56.8 (3)
OB28—Si4—OS2	159.4 (4)	OS24—OS38—OT2	83.4 (3)
OS18—Si4—OS2	134.7 (3)	Si23—OS38—OW1^iv	102.0 (10)
OS33—Si4—OB12	77.7 (4)	Ti12—OS38—OW1^iv	110.0 (10)
OS36—Si4—OB12	99.0 (4)	OB27—OS38—OW1^iv	97.7 (9)
OB26—Si4—OB12	45.4 (4)	OS39—OS38—OW1^iv	105.1 (10)
OB28—Si4—OB12	146.1 (4)	OB25—OS38—OW1^iv	70.5 (9)
OS18—Si4—OB12	127.9 (3)	OS49—OS38—OW1^iv	129.9 (10)
OS2—Si4—OB12	46.7 (2)	OS47—OS38—OW1^iv	102.6 (9)
OS33—Si4—OT6	51.9 (4)	OS24—OS38—OW1^iv	67.7 (9)
OS36—Si4—OT6	61.6 (4)	OT2—OS38—OW1^iv	150.9 (9)
OB26—Si4—OT6	137.4 (4)	Si23—OS38—OW17	109.8 (5)
OB28—Si4—OT6	115.8 (4)	Ti12—OS38—OW17	103.9 (4)
OS18—Si4—OT6	116.1 (3)	OB27—OS38—OW17	73.2 (4)
OS2—Si4—OT6	46.2 (2)	OS39—OS38—OW17	57.9 (4)
OB12—Si4—OT6	92.5 (2)	OB25—OS38—OW17	121.4 (4)
OS33—Si4—OW40^viii	98.2 (8)	OS49—OS38—OW17	123.5 (4)
OS36—Si4—OW40^viii	148.3 (8)	OS47—OS38—OW17	151.5 (5)
OB26—Si4—OW40^viii	49.0 (8)	OS24—OS38—OW17	99.9 (4)
OB28—Si4—OW40^viii	63.6 (8)	OT2—OS38—OW17	103.8 (4)
OS18—Si4—OW40^viii	89.5 (8)	OW1^iv—OS38—OW17	85.8 (10)
OS2—Si4—OW40^viii	125.1 (8)	Si23—OS38—OB21	78.4 (4)
OB12—Si4—OW40^viii	82.6 (8)	Ti12—OS38—OB21	89.7 (4)
OT6—Si4—OW40^viii	150.0 (8)	OB27—OS38—OB21	108.0 (4)
OS33—Si4—Ba^ix	54.3 (3)	OS39—OS38—OB21	128.6 (4)
OS36—Si4—Ba^ix	114.2 (4)	OB25—OS38—OB21	49.1 (3)
OB26—Si4—Ba^ix	134.1 (4)	OS49—OS38—OB21	81.7 (3)
OB28—Si4—Ba^ix	52.4 (3)	OS47—OS38—OB21	50.0 (3)
OS18—Si4—Ba^ix	101.9 (2)	OS24—OS38—OB21	70.1 (3)
OS2—Si4—Ba^ix	107.29 (18)	OT2—OS38—OB21	106.1 (3)
OB12—Si4—Ba^ix	128.8 (2)	OW1^iv—OS38—OB21	61.1 (9)
OT6—Si4—Ba^ix	72.69 (15)	OW17—OS38—OB21	146.9 (4)
OW40^viii—Si4—Ba^ix	87.4 (7)	Si20—OS39—Ti12	129.5 (6)
OS33—Si4—OW28^ix	71.3 (4)	Si20—OS39—OS22	35.6 (3)
OS36—Si4—OW28^ix	68.3 (4)	Ti12—OS39—OS22	97.0 (4)
OB26—Si4—OW28^ix	177.4 (4)	Si20—OS39—OB17	36.3 (4)
OB28—Si4—OW28^ix	71.9 (4)	Ti12—OS39—OB17	120.6 (5)
OS18—Si4—OW28^ix	84.9 (3)	OS22—OS39—OB17	60.4 (4)
OS2—Si4—OW28^ix	91.1 (2)	Si20—OS39—OH12	34.0 (4)
OB12—Si4—OW28^ix	137.1 (3)	Ti12—OS39—OH12	153.9 (6)
OT6—Si4—OW28^ix	44.9 (2)	OS22—OS39—OH12	59.6 (4)
OW40^viii—Si4—OW28^ix	130.0 (7)	OB17—OS39—OH12	60.3 (5)
Ba^ix—Si4—OW28^ix	46.01 (17)	Si20—OS39—OS38	158.3 (6)
OB7—Si5—OH7	110.2 (6)	Ti12—OS39—OS38	44.8 (3)
OB7—Si5—OB26	111.5 (6)	OS22—OS39—OS38	125.7 (4)
OH7—Si5—OB26	108.7 (6)	OB17—OS39—OS38	161.3 (6)
OB7—Si5—OB12	109.9 (6)	OH12—OS39—OS38	138.4 (5)
OH7—Si5—OB12	108.1 (6)	Si20—OS39—OS24	130.9 (6)
OB26—Si5—OB12	108.4 (5)	Ti12—OS39—OS24	44.7 (3)
OB7—Si5—OW40	125.6 (9)	OS22—OS39—OS24	121.1 (5)
OH7—Si5—OW40	56.7 (9)	OB17—OS39—OS24	98.0 (5)
OB26—Si5—OW40	52.0 (9)	OH12—OS39—OS24	155.9 (5)
OB12—Si5—OW40	124.5 (9)	OS38—OS39—OS24	63.4 (4)
OB7—Si5—OH3^vii	75.7 (4)	Si20—OS39—OW17	112.5 (6)
OH7—Si5—OH3^vii	40.8 (4)	Ti12—OS39—OW17	113.1 (5)
OB26—Si5—OH3^vii	144.1 (4)	OS22—OS39—OW17	128.2 (5)
OB12—Si5—OH3^vii	101.2 (4)	OB17—OS39—OW17	124.0 (5)
OW40—Si5—OH3^vii	94.3 (8)	OH12—OS39—OW17	78.5 (4)
OB7—Si5—OS36	78.5 (4)	OS38—OS39—OW17	68.3 (4)
OH7—Si5—OS36	150.2 (4)	OS24—OS39—OW17	109.7 (5)
OB26—Si5—OS36	43.9 (4)	Si20—OS39—OT2	98.6 (5)
OB12—Si5—OS36	94.5 (4)	Ti12—OS39—OT2	43.0 (3)
OW40—Si5—OS36	94.6 (8)	OS22—OS39—OT2	63.1 (3)
OH3^vii—Si5—OS36	153.2 (3)	OB17—OS39—OT2	116.0 (5)
OB7—Si5—OS2	93.1 (4)	OH12—OS39—OT2	111.3 (5)
OH7—Si5—OS2	149.4 (5)	OS38—OS39—OT2	63.4 (3)
OB26—Si5—OS2	79.1 (4)	OS24—OS39—OT2	86.7 (4)
OB12—Si5—OS2	43.1 (4)	OW17—OS39—OT2	113.3 (5)
OW40—Si5—OS2	124.5 (8)	Si20—OS39—OHT1	85.8 (5)
OH3^vii—Si5—OS2	136.7 (2)	Ti12—OS39—OHT1	46.3 (3)
OS36—Si5—OS2	51.7 (2)	OS22—OS39—OHT1	61.6 (3)
OB7—Si5—OS4	69.8 (4)	OB17—OS39—OHT1	76.8 (4)
OH7—Si5—OS4	126.2 (4)	OH12—OS39—OHT1	118.6 (5)
OB26—Si5—OS4	121.4 (4)	OS38—OS39—OHT1	90.9 (4)
OB12—Si5—OS4	40.3 (4)	OS24—OS39—OHT1	60.1 (3)
OW40—Si5—OS4	164.0 (8)	OW17—OS39—OHT1	159.0 (5)
OH3^vii—Si5—OS4	94.4 (2)	OT2—OS39—OHT1	51.0 (3)
OS36—Si5—OS4	83.6 (2)	Si20—OS39—OH23	86.3 (5)
OS2—Si5—OS4	43.43 (19)	Ti12—OS39—OH23	109.9 (8)
OB7—Si5—OS35	41.4 (4)	OS22—OS39—OH23	113.5 (5)
OH7—Si5—OS35	149.4 (5)	OB17—OS39—OH23	53.5 (4)
OB26—Si5—OS35	95.7 (4)	OH12—OS39—OH23	91.3 (7)
OB12—Si5—OS35	80.2 (4)	OS38—OS39—OH23	115.4 (5)
OW40—Si5—OS35	142.3 (9)	OS24—OS39—OH23	65.8 (7)
OH3^vii—Si5—OS35	109.3 (2)	OW17—OS39—OH23	95.1 (8)
OS36—Si5—OS35	52.0 (2)	OT2—OS39—OH23	146.2 (9)
OS2—Si5—OS35	52.0 (2)	OHT1—OS39—OH23	96.4 (9)
OS4—Si5—OS35	44.8 (2)	Si20—OS39—Ti7	69.0 (4)
OS4—Si6—OS2	112.9 (5)	Ti12—OS39—Ti7	62.3 (3)
OS4—Si6—OB12	108.5 (5)	OS22—OS39—Ti7	34.7 (2)
OS2—Si6—OB12	110.8 (5)	OB17—OS39—Ti7	81.9 (4)
OS4—Si6—OB38	108.9 (5)	OH12—OS39—Ti7	93.5 (4)
OS2—Si6—OB38	109.9 (5)	OS38—OS39—Ti7	96.3 (3)
OB12—Si6—OB38	105.6 (5)	OS24—OS39—Ti7	93.4 (3)
OS4—Si6—OS12	156.4 (4)	OW17—OS39—Ti7	140.3 (4)
OS2—Si6—OS12	63.3 (4)	OT2—OS39—Ti7	34.2 (2)
OB12—Si6—OS12	94.0 (4)	OHT1—OS39—Ti7	35.4 (2)
OB38—Si6—OS12	56.3 (4)	OH23—OS39—Ti7	124.1 (7)
OS4—Si6—OS35	56.3 (4)	Si2—OS40—Ti3	129.7 (6)
OS2—Si6—OS35	70.8 (4)	Si2—OS40—OB10	36.4 (3)
OB12—Si6—OS35	91.0 (4)	Ti3—OS40—OB10	106.8 (5)
OB38—Si6—OS35	161.3 (4)	Si2—OS40—OB29^ii	36.5 (4)
OS12—Si6—OS35	132.4 (3)	Ti3—OS40—OB29^ii	103.7 (5)
OS4—Si6—OB7	74.7 (4)	OB10—OS40—OB29^ii	59.5 (4)
OS2—Si6—OB7	97.4 (4)	Si2—OS40—OH6	32.3 (3)
OB12—Si6—OB7	45.9 (4)	Ti3—OS40—OH6	161.9 (6)
OB38—Si6—OB7	147.3 (4)	OB10—OS40—OH6	59.4 (4)
OS12—Si6—OB7	128.2 (3)	OB29^ii—OS40—OH6	59.8 (4)
OS35—Si6—OB7	46.0 (2)	Si2—OS40—OT7^ii	93.6 (5)
OS4—Si6—OT3^ii	51.8 (4)	Ti3—OS40—OT7^ii	49.1 (3)
OS2—Si6—OT3^ii	62.3 (4)	OB10—OS40—OT7^ii	97.2 (5)
OB12—Si6—OT3^ii	137.1 (4)	OB29^ii—OS40—OT7^ii	58.6 (4)
OB38—Si6—OT3^ii	116.6 (4)	OH6—OS40—OT7^ii	117.4 (5)
OS12—Si6—OT3^ii	114.9 (2)	Si2—OS40—OS13^ii	150.2 (6)
OS35—Si6—OT3^ii	46.1 (2)	Ti3—OS40—OS13^ii	43.2 (3)
OB7—Si6—OT3^ii	91.5 (2)	OB10—OS40—OS13^ii	149.4 (5)
OS4—Si6—OW27^ii	77.9 (4)	OB29^ii—OS40—OS13^ii	113.9 (5)
OS2—Si6—OW27^ii	66.3 (4)	OH6—OS40—OS13^ii	147.2 (5)
OB12—Si6—OW27^ii	173.5 (4)	OT7^ii—OS40—OS13^ii	60.0 (4)
OB38—Si6—OW27^ii	70.9 (4)	Si2—OS40—OS35	88.8 (5)
OS12—Si6—OW27^ii	79.5 (3)	Ti3—OS40—OS35	48.0 (3)
OS35—Si6—OW27^ii	93.4 (2)	OB10—OS40—OS35	59.1 (3)
OB7—Si6—OW27^ii	139.1 (3)	OB29^ii—OS40—OS35	83.4 (4)
OT3^ii—Si6—OW27^ii	47.6 (2)	OH6—OS40—OS35	118.1 (5)
OS30—Si7—OS5	114.1 (5)	OT7^ii—OS40—OS35	64.4 (4)
OS30—Si7—OS29	109.2 (5)	OS13^ii—OS40—OS35	91.1 (4)
OS5—Si7—OS29	107.0 (5)	Si2—OS40—OW29	98.3 (6)
OS30—Si7—OS3	108.3 (5)	Ti3—OS40—OW29	117.9 (6)
OS5—Si7—OS3	110.4 (5)	OB10—OS40—OW29	89.0 (5)
OS29—Si7—OS3	107.7 (5)	OB29^ii—OS40—OW29	134.0 (6)
OS30—Si7—Na4	59.6 (4)	OH6—OS40—OW29	75.8 (5)
OS5—Si7—Na4	138.8 (4)	OT7^ii—OS40—OW29	166.8 (6)
OS29—Si7—Na4	113.4 (4)	OS13^ii—OS40—OW29	109.7 (5)
OS3—Si7—Na4	49.8 (4)	OS35—OS40—OW29	109.8 (5)
OS30—Si7—Na2	135.9 (4)	Si2—OS40—OW33^vii	119.7 (7)
OS5—Si7—Na2	56.7 (4)	Ti3—OS40—OW33^vii	106.5 (6)
OS29—Si7—Na2	51.1 (4)	OB10—OS40—OW33^vii	145.4 (6)
OS3—Si7—Na2	115.2 (4)	OB29^ii—OS40—OW33^vii	119.9 (6)
Na4—Si7—Na2	158.1 (2)	OH6—OS40—OW33^vii	89.5 (6)
OS30—Si7—OHT2^ix	102.7 (4)	OT7^ii—OS40—OW33^vii	111.5 (6)
OS5—Si7—OHT2^ix	58.4 (4)	OS13^ii—OS40—OW33^vii	65.1 (5)
OS29—Si7—OHT2^ix	148.1 (4)	OS35—OS40—OW33^vii	151.4 (6)
OS3—Si7—OHT2^ix	60.2 (4)	OW29—OS40—OW33^vii	67.4 (6)
Na4—Si7—OHT2^ix	82.3 (2)	Si2—OS40—OS4	143.1 (5)
Na2—Si7—OHT2^ix	104.5 (2)	Ti3—OS40—OS4	38.2 (3)
OS30—Si7—OHT3	57.5 (3)	OB10—OS40—OS4	106.9 (4)
OS5—Si7—OHT3	102.3 (4)	OB29^ii—OS40—OS4	138.0 (5)
OS29—Si7—OHT3	59.2 (3)	OH6—OS40—OS4	151.8 (5)
OS3—Si7—OHT3	147.3 (4)	OT7^ii—OS40—OS4	87.3 (4)
Na4—Si7—OHT3	104.8 (2)	OS13^ii—OS40—OS4	55.8 (3)
Na2—Si7—OHT3	81.2 (2)	OS35—OS40—OS4	58.4 (3)
OHT2^ix—Si7—OHT3	146.4 (2)	OW29—OS40—OS4	79.7 (5)
OS30—Si7—OT6	58.2 (3)	OW33^vii—OS40—OS4	93.8 (6)
OS5—Si7—OT6	144.0 (4)	Si2—OS40—Si10^ii	67.9 (4)
OS29—Si7—OT6	54.6 (4)	Ti3—OS40—Si10^ii	80.1 (3)
OS3—Si7—OT6	105.1 (4)	OB10—OS40—Si10^ii	86.1 (4)
Na4—Si7—OT6	71.6 (2)	OB29^ii—OS40—Si10^ii	31.4 (3)
Na2—Si7—OT6	102.3 (2)	OH6—OS40—Si10^ii	86.8 (4)
OHT2^ix—Si7—OT6	153.0 (2)	OT7^ii—OS40—Si10^ii	31.1 (2)
OHT3—Si7—OT6	42.2 (2)	OS13^ii—OS40—Si10^ii	82.5 (3)
OS30—Si7—OT1^ix	144.7 (4)	OS35—OS40—Si10^ii	82.4 (3)
OS5—Si7—OT1^ix	58.2 (3)	OW29—OS40—Si10^ii	162.0 (5)
OS29—Si7—OT1^ix	105.8 (4)	OW33^vii—OS40—Si10^ii	108.5 (5)
OS3—Si7—OT1^ix	55.1 (3)	OS4—OS40—Si10^ii	118.4 (4)
Na4—Si7—OT1^ix	101.9 (2)	Si22—OS41—Ti9	125.9 (5)
Na2—Si7—OT1^ix	72.4 (2)	Si22—OS41—Ce2	130.5 (4)
OHT2^ix—Si7—OT1^ix	42.4 (2)	Ti9—OS41—Ce2	102.7 (3)
OHT3—Si7—OT1^ix	153.0 (2)	Si22—OS41—OB4	36.6 (3)
OT6—Si7—OT1^ix	149.6 (2)	Ti9—OS41—OB4	106.3 (4)
OS30—Si7—OW25	81.8 (5)	Ce2—OS41—OB4	127.4 (4)
OS5—Si7—OW25	36.0 (5)	Si22—OS41—OT1	170.7 (5)
OS29—Si7—OW25	105.3 (5)	Ti9—OS41—OT1	45.2 (2)
OS3—Si7—OW25	139.4 (5)	Ce2—OS41—OT1	57.8 (3)
Na4—Si7—OW25	131.8 (4)	OB4—OS41—OT1	137.0 (4)
Na2—Si7—OW25	70.1 (4)	Si22—OS41—OB37	34.7 (3)
OHT2^ix—Si7—OW25	79.3 (4)	Ti9—OS41—OB37	100.0 (4)
OHT3—Si7—OW25	71.6 (4)	Ce2—OS41—OB37	152.5 (4)
OT6—Si7—OW25	113.1 (4)	OB4—OS41—OB37	58.7 (3)
OT1^ix—Si7—OW25	93.6 (4)	OT1—OS41—OB37	140.4 (4)
OS30—Si7—Ba^ix	123.3 (4)	Si22—OS41—OS9	32.9 (3)
OS5—Si7—Ba^ix	122.6 (3)	Ti9—OS41—OS9	157.4 (4)
OS29—Si7—Ba^ix	55.0 (3)	Ce2—OS41—OS9	99.7 (3)
OS3—Si7—Ba^ix	52.7 (3)	OB4—OS41—OS9	60.7 (3)
Na4—Si7—Ba^ix	77.34 (17)	OT1—OS41—OS9	156.4 (4)
Na2—Si7—Ba^ix	80.75 (15)	OB37—OS41—OS9	57.8 (3)
OHT2^ix—Si7—Ba^ix	106.24 (17)	Si22—OS41—OS8	111.5 (5)
OHT3—Si7—Ba^ix	107.31 (18)	Ti9—OS41—OS8	43.6 (2)
OT6—Si7—Ba^ix	75.17 (16)	Ce2—OS41—OS8	96.6 (3)
OT1^ix—Si7—Ba^ix	74.43 (16)	OB4—OS41—OS8	76.8 (3)
OW25—Si7—Ba^ix	150.7 (4)	OT1—OS41—OS8	60.7 (3)
OS12—Si8—OB38	108.7 (5)	OB37—OS41—OS8	110.6 (4)
OS12—Si8—OB13	109.1 (5)	OS9—OS41—OS8	135.8 (4)
OB38—Si8—OB13	109.0 (6)	Si22—OS41—OS6	82.8 (4)
OS12—Si8—OH22	113.8 (5)	Ti9—OS41—OS6	44.1 (3)
OB38—Si8—OH22	107.1 (5)	Ce2—OS41—OS6	146.6 (4)
OB13—Si8—OH22	109.0 (6)	OB4—OS41—OS6	76.2 (3)
OS12—Si8—Na11^ii	130.2 (4)	OT1—OS41—OS6	88.8 (3)
OB38—Si8—Na11^ii	57.5 (4)	OB37—OS41—OS6	56.9 (3)
OB13—Si8—Na11^ii	120.7 (4)	OS9—OS41—OS6	113.4 (4)
OH22—Si8—Na11^ii	49.7 (5)	OS8—OS41—OS6	63.1 (3)
OS12—Si8—OS2	57.9 (4)	Si22—OS41—OHT2	126.0 (5)
OB38—Si8—OS2	52.8 (4)	Ti9—OS41—OHT2	43.6 (2)
OB13—Si8—OS2	137.0 (5)	Ce2—OS41—OHT2	94.2 (3)
OH22—Si8—OS2	113.6 (4)	OB4—OS41—OHT2	136.3 (4)
Na11^ii—Si8—OS2	84.6 (3)	OT1—OS41—OHT2	51.4 (3)
OS12—Si8—OHT3	49.2 (4)	OB37—OS41—OHT2	91.5 (4)
OB38—Si8—OHT3	92.9 (4)	OS9—OS41—OHT2	132.1 (4)
OB13—Si8—OHT3	154.3 (4)	OS8—OS41—OHT2	86.7 (3)
OH22—Si8—OHT3	75.4 (4)	OS6—OS41—OHT2	60.3 (3)
Na11^ii—Si8—OHT3	82.1 (2)	Si22—OS41—OT2	90.6 (4)
OS2—Si8—OHT3	49.6 (2)	Ti9—OS41—OT2	136.5 (4)
OS12—Si8—OB12	78.7 (4)	Ce2—OS41—OT2	52.7 (2)
OB38—Si8—OB12	41.2 (4)	OB4—OS41—OT2	117.1 (4)
OB13—Si8—OB12	93.8 (4)	OT1—OS41—OT2	98.6 (4)
OH22—Si8—OB12	147.0 (4)	OB37—OS41—OT2	99.9 (4)
Na11^ii—Si8—OB12	98.3 (3)	OS9—OS41—OT2	58.8 (3)
OS2—Si8—OB12	45.4 (2)	OS8—OS41—OT2	149.1 (4)
OHT3—Si8—OB12	94.3 (2)	OS6—OS41—OT2	144.3 (4)
OS12—Si8—OH29	115.5 (11)	OHT2—OS41—OT2	97.7 (3)
OB38—Si8—OH29	133.5 (10)	Si22—OS41—OS1	115.2 (4)
OB13—Si8—OH29	42.9 (8)	Ti9—OS41—OS1	87.9 (3)
OH22—Si8—OH29	68.0 (9)	Ce2—OS41—OS1	52.2 (2)
Na11^ii—Si8—OH29	100.8 (11)	OB4—OS41—OS1	85.9 (3)
OS2—Si8—OH29	173.4 (10)	OT1—OS41—OS1	65.3 (3)
OHT3—Si8—OH29	126.9 (7)	OB37—OS41—OS1	144.7 (4)
OB12—Si8—OH29	136.4 (7)	OS9—OS41—OS1	108.2 (4)
OS12—Si8—OH19^ii	76.6 (4)	OS8—OS41—OS1	54.1 (3)
OB38—Si8—OH19^ii	119.1 (4)	OS6—OS41—OS1	117.1 (4)
OB13—Si8—OH19^ii	126.8 (5)	OHT2—OS41—OS1	116.3 (3)
OH22—Si8—OH19^ii	37.3 (4)	OT2—OS41—OS1	97.5 (3)
Na11^ii—Si8—OH19^ii	73.2 (3)	Si19—OS42—Ti1^iv	135.6 (5)
OS2—Si8—OH19^ii	92.2 (2)	Si19—OS42—Na12^iv	127.4 (6)
OHT3—Si8—OH19^ii	43.8 (2)	Ti1^iv—OS42—Na12^iv	96.6 (5)
OB12—Si8—OH19^ii	137.5 (2)	Si19—OS42—OB5	36.6 (3)
OH29—Si8—OH19^ii	85.8 (7)	Ti1^iv—OS42—OB5	106.5 (4)
OH19—Si9—OS14	113.4 (5)	Na12^iv—OS42—OB5	149.8 (6)
OH19—Si9—OB8	110.7 (5)	Si19—OS42—OH17	34.0 (3)
OS14—Si9—OB8	111.4 (5)	Ti1^iv—OS42—OH17	167.9 (5)
OH19—Si9—OB27	111.7 (5)	Na12^iv—OS42—OH17	94.8 (5)
OS14—Si9—OB27	106.8 (5)	OB5—OS42—OH17	61.4 (3)
OB8—Si9—OB27	102.2 (5)	Si19—OS42—OB8	34.7 (3)
OH19—Si9—Na10	117.2 (4)	Ti1^iv—OS42—OB8	115.2 (4)
OS14—Si9—Na10	129.3 (4)	Na12^iv—OS42—OB8	128.3 (6)
OB8—Si9—Na10	46.2 (4)	OB5—OS42—OB8	57.8 (3)
OB27—Si9—Na10	56.9 (4)	OH17—OS42—OB8	59.6 (3)
OH19—Si9—OS49	147.9 (4)	Si19—OS42—OS30^iv	155.9 (5)
OS14—Si9—OS49	56.6 (4)	Ti1^iv—OS42—OS30^iv	45.4 (3)
OB8—Si9—OS49	101.0 (4)	Na12^iv—OS42—OS30^iv	56.9 (4)
OB27—Si9—OS49	54.2 (4)	OB5—OS42—OS30^iv	151.1 (4)
Na10—Si9—OS49	81.2 (2)	OH17—OS42—OS30^iv	146.6 (4)
OH19—Si9—OH22^iv	43.1 (4)	OB8—OS42—OS30^iv	121.7 (4)
OS14—Si9—OH22^iv	135.7 (4)	Si19—OS42—OS27	94.0 (4)
OB8—Si9—OH22^iv	112.5 (4)	Ti1^iv—OS42—OS27	47.3 (3)
OB27—Si9—OH22^iv	69.4 (4)	Na12^iv—OS42—OS27	135.5 (5)
Na10—Si9—OH22^iv	87.1 (2)	OB5—OS42—OS27	59.9 (3)
OS49—Si9—OH22^iv	119.0 (3)	OH17—OS42—OS27	120.8 (4)
OH19—Si9—K1^iv	43.8 (6)	OB8—OS42—OS27	94.4 (4)
OS14—Si9—K1^iv	70.3 (5)	OS30^iv—OS42—OS27	92.7 (3)
OB8—Si9—K1^iv	122.2 (7)	Si19—OS42—OHT3^iv	102.7 (4)
OB27—Si9—K1^iv	133.8 (7)	Ti1^iv—OS42—OHT3^iv	45.4 (3)
Na10—Si9—K1^iv	157.9 (5)	Na12^iv—OS42—OHT3^iv	114.0 (6)
OS49—Si9—K1^iv	121.0 (5)	OB5—OS42—OHT3^iv	96.1 (4)
OH22^iv—Si9—K1^iv	81.5 (5)	OH17—OS42—OHT3^iv	131.7 (4)
OH19—Si9—OW25^iv	46.7 (5)	OB8—OS42—OHT3^iv	72.2 (3)
OS14—Si9—OW25^iv	72.7 (5)	OS30^iv—OS42—OHT3^iv	60.4 (3)
OB8—Si9—OW25^iv	107.5 (6)	OS27—OS42—OHT3^iv	62.8 (3)
OB27—Si9—OW25^iv	148.2 (6)	Si19—OS42—OS10	143.9 (5)
Na10—Si9—OW25^iv	147.7 (4)	Ti1^iv—OS42—OS10	39.9 (3)
OS49—Si9—OW25^iv	128.0 (4)	Na12^iv—OS42—OS10	77.6 (5)
OH22^iv—Si9—OW25^iv	88.7 (4)	OB5—OS42—OS10	108.2 (4)
K1^iv—Si9—OW25^iv	14.8 (5)	OH17—OS42—OS10	140.5 (4)
OH19—Si9—OHT3^iv	44.8 (4)	OB8—OS42—OS10	150.8 (4)
OS14—Si9—OHT3^iv	137.8 (4)	OS30^iv—OS42—OS10	56.8 (3)
OB8—Si9—OHT3^iv	66.4 (4)	OS27—OS42—OS10	58.1 (3)
OB27—Si9—OHT3^iv	114.9 (4)	OHT3^iv—OS42—OS10	85.3 (3)
Na10—Si9—OHT3^iv	81.50 (19)	Si19—OS42—OW9^iv	101.2 (8)
OS49—Si9—OHT3^iv	162.7 (2)	Ti1^iv—OS42—OW9^iv	106.1 (7)
OH22^iv—Si9—OHT3^iv	60.0 (2)	Na12^iv—OS42—OW9^iv	47.4 (9)
K1^iv—Si9—OHT3^iv	76.4 (5)	OB5—OS42—OW9^iv	137.4 (8)
OW25^iv—Si9—OHT3^iv	68.8 (4)	OH17—OS42—OW9^iv	84.6 (7)
OH19—Si9—OHT2	151.9 (4)	OB8—OS42—OW9^iv	83.7 (8)
OS14—Si9—OHT2	50.3 (4)	OS30^iv—OS42—OW9^iv	63.4 (7)
OB8—Si9—OHT2	66.1 (4)	OS27—OS42—OW9^iv	149.3 (8)
OB27—Si9—OHT2	95.9 (4)	OHT3^iv—OS42—OW9^iv	87.7 (8)
Na10—Si9—OHT2	81.74 (19)	OS10—OS42—OW9^iv	114.4 (8)
OS49—Si9—OHT2	49.3 (2)	Si19—OS42—Si16	68.8 (3)
OH22^iv—Si9—OHT2	165.0 (2)	Ti1^iv—OS42—Si16	78.1 (3)
K1^iv—Si9—OHT2	112.2 (5)	Na12^iv—OS42—Si16	144.9 (6)
OW25^iv—Si9—OHT2	106.1 (4)	OB5—OS42—Si16	32.2 (2)
OHT3^iv—Si9—OHT2	127.5 (2)	OH17—OS42—Si16	90.2 (3)
OH19—Si9—OB25	104.2 (4)	OB8—OS42—Si16	83.7 (3)
OS14—Si9—OB25	73.9 (4)	OS30^iv—OS42—Si16	123.1 (3)
OB8—Si9—OB25	137.6 (4)	OS27—OS42—Si16	31.2 (2)
OB27—Si9—OB25	40.9 (4)	OHT3^iv—OS42—Si16	87.1 (3)
Na10—Si9—OB25	96.5 (2)	OS10—OS42—Si16	76.7 (3)
OS49—Si9—OB25	45.0 (2)	OW9^iv—OS42—Si16	167.3 (8)
OH22^iv—Si9—OB25	78.0 (2)	Si27—OS43—Ti11	132.3 (5)
K1^iv—Si9—OB25	99.6 (6)	Si27—OS43—OW31^vii	103.6 (6)
OW25^iv—Si9—OB25	113.9 (5)	Ti11—OS43—OW31^vii	105.5 (6)
OHT3^iv—Si9—OB25	138.0 (2)	Si27—OS43—OB14	37.0 (3)
OHT2—Si9—OB25	93.2 (2)	Ti11—OS43—OB14	158.5 (5)
OT7—Si10—OB29	108.7 (6)	OW31^vii—OS43—OB14	70.2 (6)
OT7—Si10—OB35	111.1 (7)	Si27—OS43—OB31	35.4 (3)
OB29—Si10—OB35	109.3 (7)	Ti11—OS43—OB31	125.9 (5)
OT7—Si10—OB34	109.4 (6)	OW31^vii—OS43—OB31	127.9 (6)
OB29—Si10—OB34	108.3 (6)	OB14—OS43—OB31	59.0 (3)
OB35—Si10—OB34	110.0 (7)	Si27—OS43—OS32	158.7 (5)
OT7—Si10—OS40^iv	60.7 (4)	Ti11—OS43—OS32	45.9 (3)
OB29—Si10—OS40^iv	58.2 (4)	OW31^vii—OS43—OS32	63.8 (5)
OB35—Si10—OS40^iv	97.0 (6)	OB14—OS43—OS32	133.9 (4)
OB34—Si10—OS40^iv	152.9 (5)	OB31—OS43—OS32	165.3 (5)
OT7—Si10—OS19	62.5 (4)	Si27—OS43—OS48	33.1 (3)
OB29—Si10—OS19	153.9 (5)	Ti11—OS43—OS48	102.5 (4)
OB35—Si10—OS19	96.7 (6)	OW31^vii—OS43—OS48	104.4 (6)
OB34—Si10—OS19	57.9 (4)	OB14—OS43—OS48	60.1 (3)
OS40^iv—Si10—OS19	122.8 (3)	OB31—OS43—OS48	60.2 (3)
OT7—Si10—OB33	68.4 (4)	OS32—OS43—OS48	129.7 (4)
OB29—Si10—OB33	124.5 (5)	Si27—OS43—OS1	89.2 (4)
OB35—Si10—OB33	42.7 (5)	Ti11—OS43—OS1	47.3 (3)
OB34—Si10—OB33	125.3 (5)	OW31^vii—OS43—OS1	145.9 (6)
OS40^iv—Si10—OB33	76.7 (3)	OB14—OS43—OS1	126.0 (4)
OS19—Si10—OB33	77.0 (3)	OB31—OS43—OS1	79.8 (4)
OB15—Si11—OB36	107.8 (6)	OS32—OS43—OS1	93.2 (4)
OB15—Si11—OS19	108.0 (6)	OS48—OS43—OS1	69.9 (3)
OB36—Si11—OS19	115.1 (6)	Si27—OS43—OT5	100.8 (4)
OB15—Si11—OB34	107.7 (7)	Ti11—OS43—OT5	43.4 (3)
OB36—Si11—OB34	108.3 (6)	OW31^vii—OS43—OT5	89.4 (6)
OS19—Si11—OB34	109.7 (6)	OB14—OS43—OT5	115.1 (4)
OB15—Si11—OS45	57.7 (4)	OB31—OS43—OT5	120.9 (4)
OB36—Si11—OS45	158.0 (5)	OS32—OS43—OT5	63.6 (3)
OS19—Si11—OS45	61.4 (4)	OS48—OS43—OT5	67.7 (3)
OB34—Si11—OS45	92.7 (5)	OS1—OS43—OT5	56.8 (3)
OB15—Si11—OT7	107.2 (5)	Si27—OS43—OS28	138.6 (5)
OB36—Si11—OT7	144.3 (5)	Ti11—OS43—OS28	39.6 (3)
OS19—Si11—OT7	58.8 (4)	OW31^vii—OS43—OS28	117.7 (6)
OB34—Si11—OT7	53.6 (4)	OB14—OS43—OS28	161.2 (4)
OS45—Si11—OT7	55.1 (3)	OB31—OS43—OS28	108.0 (4)
OB15—Si11—OH32	143.8 (8)	OS32—OS43—OS28	57.6 (3)
OB36—Si11—OH32	38.3 (7)	OS48—OS43—OS28	128.0 (4)
OS19—Si11—OH32	85.6 (6)	OS1—OS43—OS28	58.1 (3)
OB34—Si11—OH32	98.2 (9)	OT5—OS43—OS28	82.9 (3)
OS45—Si11—OH32	146.9 (5)	Si27—OS43—OW34	80.3 (4)
OT7—Si11—OH32	108.4 (7)	Ti11—OS43—OW34	90.4 (4)
OB15—Si11—OB32	38.8 (4)	OW31^vii—OS43—OW34	50.0 (5)
OB36—Si11—OB32	112.6 (5)	OB14—OS43—OW34	70.5 (4)
OS19—Si11—OB32	71.5 (4)	OB31—OS43—OW34	115.7 (4)
OB34—Si11—OB32	133.5 (5)	OS32—OS43—OW34	78.4 (4)
OS45—Si11—OB32	45.4 (2)	OS48—OS43—OW34	61.3 (3)
OT7—Si11—OB32	98.9 (2)	OS1—OS43—OW34	103.1 (4)
OH32—Si11—OB32	127.7 (8)	OT5—OS43—OW34	51.4 (3)
OB15—Si11—K3	131.8 (5)	OS28—OS43—OW34	128.1 (4)
OB36—Si11—K3	86.3 (6)	Si27—OS43—OB3	76.2 (4)
OS19—Si11—K3	31.1 (5)	Ti11—OS43—OB3	83.2 (3)
OB34—Si11—K3	110.9 (6)	OW31^vii—OS43—OB3	166.9 (6)
OS45—Si11—K3	92.5 (4)	OB14—OS43—OB3	105.2 (4)
OT7—Si11—K3	75.4 (4)	OB31—OS43—OB3	46.2 (3)
OH32—Si11—K3	54.4 (6)	OS32—OS43—OB3	120.2 (4)
OB32—Si11—K3	93.0 (4)	OS48—OS43—OB3	82.7 (3)
OS15—Si12—OB32	110.6 (6)	OS1—OS43—OB3	46.8 (3)
OS15—Si12—OB15	107.6 (6)	OT5—OS43—OB3	103.5 (3)
OB32—Si12—OB15	105.6 (6)	OS28—OS43—OB3	63.0 (3)
OS15—Si12—OS45	115.8 (5)	OW34—OS43—OB3	141.2 (4)
OB32—Si12—OS45	108.6 (5)	Si34—OS44—Ti11	133.3 (5)
OB15—Si12—OS45	108.1 (6)	Si34—OS44—Ti10	128.6 (5)
OS15—Si12—OS19	158.3 (5)	Ti11—OS44—Ti10	96.6 (4)
OB32—Si12—OS19	89.4 (4)	Si34—OS44—OT5	176.9 (6)
OB15—Si12—OS19	56.9 (5)	Ti11—OS44—OT5	49.6 (3)
OS45—Si12—OS19	62.4 (4)	Ti10—OS44—OT5	49.2 (3)
OS15—Si12—OS46	57.0 (4)	Si34—OS44—OB6	36.2 (3)
OB32—Si12—OS46	92.5 (4)	Ti11—OS44—OB6	101.6 (4)
OB15—Si12—OS46	160.2 (5)	Ti10—OS44—OB6	160.8 (5)
OS45—Si12—OS46	72.7 (4)	OT5—OS44—OB6	145.2 (5)
OS19—Si12—OS46	133.1 (3)	Si34—OS44—OB22	36.6 (3)
OS15—Si12—Na9	43.7 (5)	Ti11—OS44—OB22	158.5 (5)
OB32—Si12—Na9	128.1 (6)	Ti10—OS44—OB22	100.4 (4)
OB15—Si12—Na9	64.5 (5)	OT5—OS44—OB22	140.3 (5)
OS45—Si12—Na9	123.1 (6)	OB6—OS44—OB22	60.5 (3)
OS19—Si12—Na9	117.1 (4)	Si34—OS44—OH34	34.1 (3)
OS46—Si12—Na9	98.0 (3)	Ti11—OS44—OH34	124.9 (4)
OS15—Si12—OT4^ii	52.9 (4)	Ti10—OS44—OH34	112.3 (4)
OB32—Si12—OT4^ii	139.8 (4)	OT5—OS44—OH34	147.1 (5)
OB15—Si12—OT4^ii	114.3 (5)	OB6—OS44—OH34	61.6 (4)
OS45—Si12—OT4^ii	64.2 (4)	OB22—OS44—OH34	59.5 (3)
OS19—Si12—OT4^ii	116.2 (3)	Si34—OS44—OS34	84.2 (4)
OS46—Si12—OT4^ii	47.4 (2)	Ti11—OS44—OS34	140.5 (5)
Na9—Si12—OT4^ii	69.0 (4)	Ti10—OS44—OS34	44.6 (3)
OS15—Si12—OB11	75.6 (4)	OT5—OS44—OS34	93.5 (4)
OB32—Si12—OB11	47.1 (4)	OB6—OS44—OS34	117.9 (4)
OB15—Si12—OB11	148.1 (5)	OB22—OS44—OS34	59.1 (3)
OS45—Si12—OB11	98.0 (4)	OH34—OS44—OS34	76.8 (4)
OS19—Si12—OB11	125.8 (3)	Si34—OS44—OS28	88.7 (4)
OS46—Si12—OB11	46.4 (2)	Ti11—OS44—OS28	44.7 (3)
Na9—Si12—OB11	115.6 (4)	Ti10—OS44—OS28	140.7 (4)
OT4^ii—Si12—OB11	93.3 (2)	OT5—OS44—OS28	94.0 (4)
OS15—Si12—OW35^x	47.8 (5)	OB6—OS44—OS28	58.3 (3)
OB32—Si12—OW35^x	73.7 (5)	OB22—OS44—OS28	118.8 (4)
OB15—Si12—OW35^x	89.8 (6)	OH34—OS44—OS28	91.5 (4)
OS45—Si12—OW35^x	160.0 (5)	OS34—OS44—OS28	167.4 (4)
OS19—Si12—OW35^x	137.4 (4)	Si34—OS44—OS26	115.4 (5)
OS46—Si12—OW35^x	87.4 (4)	Ti11—OS44—OS26	88.3 (4)
Na9—Si12—OW35^x	56.3 (6)	Ti10—OS44—OS26	43.0 (3)
OT4^ii—Si12—OW35^x	100.7 (4)	OT5—OS44—OS26	64.8 (4)
OB11—Si12—OW35^x	68.6 (4)	OB6—OS44—OS26	143.1 (5)
OB11—Si13—OH8	110.0 (6)	OB22—OS44—OS26	113.1 (4)
OB11—Si13—OB32	109.8 (6)	OH34—OS44—OS26	83.6 (4)
OH8—Si13—OB32	110.1 (6)	OS34—OS44—OS26	59.4 (4)
OB11—Si13—OB30	108.7 (5)	OS28—OS44—OS26	115.4 (4)
OH8—Si13—OB30	107.5 (6)	Si34—OS44—OS32	116.8 (5)
OB32—Si13—OB30	110.8 (5)	Ti11—OS44—OS32	43.1 (3)
OB11—Si13—OS27	77.1 (4)	Ti10—OS44—OS32	89.3 (4)
OH8—Si13—OS27	149.3 (5)	OT5—OS44—OS32	66.0 (3)
OB32—Si13—OS27	94.2 (4)	OB6—OS44—OS32	108.3 (4)
OB30—Si13—OS27	44.2 (4)	OB22—OS44—OS32	149.2 (4)
OB11—Si13—OS45	92.7 (4)	OH34—OS44—OS32	89.8 (4)
OH8—Si13—OS45	150.6 (5)	OS34—OS44—OS32	115.7 (4)
OB32—Si13—OS45	42.4 (4)	OS28—OS44—OS32	58.8 (3)
OB30—Si13—OS45	81.1 (4)	OS26—OS44—OS32	56.8 (3)
OS27—Si13—OS45	52.1 (2)	Si34—OS44—OS1	122.2 (5)
OB11—Si13—OS17	119.0 (4)	Ti11—OS44—OS1	44.4 (2)
OH8—Si13—OS17	127.5 (5)	Ti10—OS44—OS1	100.9 (4)
OB32—Si13—OS17	70.4 (4)	OT5—OS44—OS1	58.3 (3)
OB30—Si13—OS17	40.7 (4)	OB6—OS44—OS1	87.8 (4)
OS27—Si13—OS17	43.47 (19)	OB22—OS44—OS1	118.6 (4)
OS45—Si13—OS17	44.8 (2)	OH34—OS44—OS1	146.6 (4)
OB11—Si13—OS46	40.7 (4)	OS34—OS44—OS1	133.6 (4)
OH8—Si13—OS46	148.7 (5)	OS28—OS44—OS1	59.0 (3)
OB32—Si13—OS46	79.7 (4)	OS26—OS44—OS1	121.5 (4)
OB30—Si13—OS46	95.6 (4)	OS32—OS44—OS1	87.5 (3)
OS27—Si13—OS46	51.8 (2)	Si12—OS45—Ti5	128.9 (6)
OS45—Si13—OS46	52.2 (2)	Si12—OS45—Ce1^iv	127.3 (5)
OS17—Si13—OS46	83.7 (2)	Ti5—OS45—Ce1^iv	102.9 (4)
OB11—Si13—OS15	69.0 (4)	Si12—OS45—OT3	174.0 (6)
OH8—Si13—OS15	126.9 (5)	Ti5—OS45—OT3	45.4 (3)
OB32—Si13—OS15	40.9 (4)	Ce1^iv—OS45—OT3	57.9 (3)
OB30—Si13—OS15	123.5 (4)	Si12—OS45—OB15	35.9 (3)
OS27—Si13—OS15	83.8 (2)	Ti5—OS45—OB15	102.1 (4)
OS45—Si13—OS15	44.2 (2)	Ce1^iv—OS45—OB15	150.1 (5)
OS17—Si13—OS15	88.9 (2)	OT3—OS45—OB15	141.4 (5)
OS46—Si13—OS15	44.2 (2)	Si12—OS45—OB32	35.7 (3)
OS20—Si14—OH21	111.9 (6)	Ti5—OS45—OB32	108.7 (4)
OS20—Si14—OB9	109.7 (5)	Ce1^iv—OS45—OB32	126.2 (4)
OH21—Si14—OB9	104.5 (6)	OT3—OS45—OB32	140.0 (5)
OS20—Si14—OB18^x	110.7 (6)	OB15—OS45—OB32	58.8 (4)
OH21—Si14—OB18^x	111.2 (6)	Si12—OS45—OS15	31.6 (3)
OB9—Si14—OB18^x	108.6 (6)	Ti5—OS45—OS15	159.5 (5)
OS20—Si14—OS7^x	89.2 (4)	Ce1^iv—OS45—OS15	97.6 (4)
OH21—Si14—OS7^x	76.9 (4)	OT3—OS45—OS15	154.3 (5)
OB9—Si14—OS7^x	158.3 (4)	OB15—OS45—OS15	57.9 (4)
OB18^x—Si14—OS7^x	52.7 (4)	OB32—OS45—OS15	58.9 (4)
OS20—Si14—OS46	58.0 (4)	Si12—OS45—OS19	85.8 (5)
OH21—Si14—OS46	121.3 (5)	Ti5—OS45—OS19	45.1 (3)
OB9—Si14—OS46	51.6 (4)	Ce1^iv—OS45—OS19	146.9 (5)
OB18^x—Si14—OS46	126.7 (4)	OT3—OS45—OS19	89.1 (4)
OS7^x—Si14—OS46	145.9 (3)	OB15—OS45—OS19	57.4 (4)
OS20—Si14—OB11	83.6 (4)	OB32—OS45—OS19	80.2 (4)
OH21—Si14—OB11	151.6 (5)	OS15—OS45—OS19	114.5 (5)
OB9—Si14—OB11	47.1 (4)	Si12—OS45—OS17	113.1 (5)
OB18^x—Si14—OB11	82.8 (4)	Ti5—OS45—OS17	41.7 (3)
OS7^x—Si14—OB11	128.6 (3)	Ce1^iv—OS45—OS17	98.3 (4)
OS46—Si14—OB11	46.2 (2)	OT3—OS45—OS17	61.5 (3)
OS20—Si14—K2	45.4 (4)	OB15—OS45—OS17	111.3 (4)
OH21—Si14—K2	84.0 (5)	OB32—OS45—OS17	79.3 (4)
OB9—Si14—K2	154.2 (4)	OS15—OS45—OS17	136.7 (5)
OB18^x—Si14—K2	90.2 (5)	OS19—OS45—OS17	64.3 (3)
OS7^x—Si14—K2	47.0 (2)	Si12—OS45—OT7	127.1 (5)
OS46—Si14—K2	102.9 (2)	Ti5—OS45—OT7	45.1 (3)
OB11—Si14—K2	121.6 (3)	Ce1^iv—OS45—OT7	94.5 (4)
OS46—Si15—OS10	113.4 (5)	OT3—OS45—OT7	51.7 (3)
OS46—Si15—OB11	110.4 (5)	OB15—OS45—OT7	91.6 (4)
OS10—Si15—OB11	110.9 (5)	OB32—OS45—OT7	138.2 (5)
OS46—Si15—OB9	111.2 (5)	OS15—OS45—OT7	131.9 (4)
OS10—Si15—OB9	106.0 (5)	OS19—OS45—OT7	58.3 (3)
OB11—Si15—OB9	104.4 (5)	OS17—OS45—OT7	86.5 (4)
OS46—Si15—OS20	64.4 (4)	Si12—OS45—OT4^ii	87.0 (4)
OS10—Si15—OS20	154.9 (4)	Ti5—OS45—OT4^ii	138.7 (5)
OB11—Si15—OS20	92.2 (4)	Ce1^iv—OS45—OT4^ii	51.7 (3)
OB9—Si15—OS20	56.8 (4)	OT3—OS45—OT4^ii	99.0 (4)
OS46—Si15—OS27	73.1 (4)	OB15—OS45—OT4^ii	98.4 (4)
OS10—Si15—OS27	58.7 (4)	OB32—OS45—OT4^ii	112.6 (4)
OB11—Si15—OS27	88.3 (4)	OS15—OS45—OT4^ii	56.2 (3)
OB9—Si15—OS27	163.4 (4)	OS19—OS45—OT4^ii	143.1 (5)
OS20—Si15—OS27	134.7 (3)	OS17—OS45—OT4^ii	149.6 (4)
OS46—Si15—OT6^iv	61.4 (4)	OT7—OS45—OT4^ii	99.4 (4)
OS10—Si15—OT6^iv	52.3 (4)	Si12—OS45—Si11	65.3 (3)
OB11—Si15—OT6^iv	135.3 (4)	Ti5—OS45—Si11	73.0 (3)
OB9—Si15—OT6^iv	119.7 (4)	Ce1^iv—OS45—Si11	154.8 (4)
OS20—Si15—OT6^iv	116.9 (3)	OT3—OS45—Si11	111.3 (4)
OS27—Si15—OT6^iv	47.1 (2)	OB15—OS45—Si11	30.4 (3)
OS46—Si15—Na4^iv	112.2 (4)	OB32—OS45—Si11	77.5 (3)
OS10—Si15—Na4^iv	49.6 (4)	OS15—OS45—Si11	87.7 (3)
OB11—Si15—Na4^iv	137.4 (4)	OS19—OS45—Si11	31.1 (3)
OB9—Si15—Na4^iv	60.2 (4)	OS17—OS45—Si11	94.4 (3)
OS20—Si15—Na4^iv	106.6 (3)	OT7—OS45—Si11	64.6 (3)
OS27—Si15—Na4^iv	103.2 (2)	OT4^ii—OS45—Si11	115.1 (4)
OT6^iv—Si15—Na4^iv	68.6 (2)	Si15—OS46—Ti6^ii	127.4 (5)
OS46—Si15—OW28^xi	68.5 (4)	Si15—OS46—Ce1^iv	130.1 (5)
OS10—Si15—OW28^xi	71.3 (4)	Ti6^ii—OS46—Ce1^iv	101.7 (4)
OB11—Si15—OW28^xi	177.8 (4)	Si15—OS46—OB11	35.4 (3)
OB9—Si15—OW28^xi	74.5 (4)	Ti6^ii—OS46—OB11	111.5 (4)
OS20—Si15—OW28^xi	85.6 (3)	Ce1^iv—OS46—OB11	123.6 (4)
OS27—Si15—OW28^xi	93.2 (2)	Si15—OS46—OB9	35.0 (3)
OT6^iv—Si15—OW28^xi	46.1 (2)	Ti6^ii—OS46—OB9	99.0 (4)
Na4^iv—Si15—OW28^xi	43.8 (2)	Ce1^iv—OS46—OB9	155.7 (4)
OS46—Si15—OB30	100.1 (4)	OB11—OS46—OB9	58.4 (3)
OS10—Si15—OB30	78.2 (4)	Si15—OS46—OS10	33.5 (3)
OB11—Si15—OB30	43.3 (4)	Ti6^ii—OS46—OS10	157.0 (5)
OB9—Si15—OB30	142.6 (4)	Ce1^iv—OS46—OS10	100.2 (3)
OS20—Si15—OB30	126.8 (3)	OB11—OS46—OS10	60.3 (3)
OS27—Si15—OB30	46.1 (2)	OB9—OS46—OS10	58.2 (3)
OT6^iv—Si15—OB30	92.7 (2)	Si15—OS46—OT4^ii	171.2 (6)
Na4^iv—Si15—OB30	125.8 (2)	Ti6^ii—OS46—OT4^ii	45.2 (3)
OW28^xi—Si15—OB30	138.4 (2)	Ce1^iv—OS46—OT4^ii	56.5 (3)
OS46—Si15—OS15	44.9 (4)	OB11—OS46—OT4^ii	137.8 (5)
OS10—Si15—OS15	147.4 (4)	OB9—OS46—OT4^ii	141.5 (4)
OB11—Si15—OS15	69.3 (4)	OS10—OS46—OT4^ii	155.1 (5)
OB9—Si15—OS15	105.2 (4)	Si15—OS46—OS15	111.0 (5)
OS20—Si15—OS15	49.6 (2)	Ti6^ii—OS46—OS15	45.3 (3)
OS27—Si15—OS15	89.1 (2)	Ce1^iv—OS46—OS15	96.3 (3)
OT6^iv—Si15—OS15	103.2 (2)	OB11—OS46—OS15	78.6 (4)
Na4^iv—Si15—OS15	149.8 (2)	OB9—OS46—OS15	107.4 (4)
OW28^xi—Si15—OS15	109.0 (3)	OS10—OS46—OS15	138.2 (5)
OB30—Si15—OS15	82.6 (2)	OT4^ii—OS46—OS15	60.7 (3)
OS27—Si16—OS17	112.8 (5)	Si15—OS46—OS20	85.4 (4)
OS27—Si16—OB30	111.1 (5)	Ti6^ii—OS46—OS20	42.8 (3)
OS17—Si16—OB30	108.7 (5)	Ce1^iv—OS46—OS20	144.3 (4)
OS27—Si16—OB5	111.5 (5)	OB11—OS46—OS20	81.8 (4)
OS17—Si16—OB5	107.5 (5)	OB9—OS46—OS20	56.9 (3)
OB30—Si16—OB5	104.8 (5)	OS10—OS46—OS20	114.8 (4)
OS27—Si16—OS42	63.2 (4)	OT4^ii—OS46—OS20	87.8 (4)
OS17—Si16—OS42	156.1 (4)	OS15—OS46—OS20	61.9 (3)
OB30—Si16—OS42	94.0 (4)	Si15—OS46—OHT4^ii	127.7 (5)
OB5—Si16—OS42	57.9 (4)	Ti6^ii—OS46—OHT4^ii	41.5 (3)
OS27—Si16—OS45	70.6 (4)	Ce1^iv—OS46—OHT4^ii	93.7 (3)
OS17—Si16—OS45	56.7 (4)	OB11—OS46—OHT4^ii	140.7 (4)
OB30—Si16—OS45	91.3 (4)	OB9—OS46—OHT4^ii	93.2 (4)
OB5—Si16—OS45	161.0 (4)	OS10—OS46—OHT4^ii	130.1 (4)
OS42—Si16—OS45	132.2 (2)	OT4^ii—OS46—OHT4^ii	51.9 (3)
OS27—Si16—OT3	62.6 (4)	OS15—OS46—OHT4^ii	86.3 (4)
OS17—Si16—OT3	51.3 (4)	OS20—OS46—OHT4^ii	59.3 (4)
OB30—Si16—OT3	137.0 (4)	Si15—OS46—OT6^iv	90.9 (4)
OB5—Si16—OT3	117.2 (4)	Ti6^ii—OS46—OT6^iv	135.2 (4)
OS42—Si16—OT3	115.4 (2)	Ce1^iv—OS46—OT6^iv	52.0 (2)
OS45—Si16—OT3	45.8 (2)	OB11—OS46—OT6^iv	113.3 (4)
OS27—Si16—OB32	97.1 (4)	OB9—OS46—OT6^iv	103.8 (4)
OS17—Si16—OB32	74.9 (4)	OS10—OS46—OT6^iv	57.6 (3)
OB30—Si16—OB32	46.4 (4)	OT4^ii—OS46—OT6^iv	97.8 (4)
OB5—Si16—OB32	146.6 (4)	OS15—OS46—OT6^iv	148.1 (4)
OS42—Si16—OB32	128.1 (3)	OS20—OS46—OT6^iv	146.1 (4)
OS45—Si16—OB32	45.7 (2)	OHT4^ii—OS46—OT6^iv	98.6 (4)
OT3—Si16—OB32	90.8 (2)	Si15—OS46—OS27	78.1 (4)
OS27—Si16—OW27	65.8 (4)	Ti6^ii—OS46—OS27	146.4 (4)
OS17—Si16—OW27	77.3 (4)	Ce1^iv—OS46—OS27	53.3 (2)
OB30—Si16—OW27	174.0 (4)	OB11—OS46—OS27	75.4 (3)
OB5—Si16—OW27	72.5 (4)	OB9—OS46—OS27	111.6 (4)
OS42—Si16—OW27	80.1 (2)	OS10—OS46—OS27	55.7 (3)
OS45—Si16—OW27	92.4 (3)	OT4^ii—OS46—OS27	106.8 (4)
OT3—Si16—OW27	47.0 (2)	OS15—OS46—OS27	109.4 (4)
OB32—Si16—OW27	137.9 (3)	OS20—OS46—OS27	156.9 (5)
OB35—Si17—OH14	110.7 (12)	OHT4^ii—OS46—OS27	143.7 (4)
OB35—Si17—OH1	111.7 (11)	OT6^iv—OS46—OS27	51.1 (3)
OH14—Si17—OH1	108.8 (13)	Si28—OS47—Ti12	128.3 (5)
OB35—Si17—OB33	111.0 (7)	Si28—OS47—Ce2	128.8 (5)
OH14—Si17—OB33	107.6 (11)	Ti12—OS47—Ce2	101.8 (4)
OH1—Si17—OB33	106.9 (10)	Si28—OS47—OT2	173.4 (6)
OB35—Si17—OH31^xii	166.5 (8)	Ti12—OS47—OT2	45.5 (3)
OH14—Si17—OH31^xii	63.0 (13)	Ce2—OS47—OT2	56.7 (2)
OH1—Si17—OH31^xii	62.6 (13)	Si28—OS47—OB21	34.0 (3)
OB33—Si17—OH31^xii	82.4 (7)	Ti12—OS47—OB21	111.6 (4)
OB35—Si17—OT7	45.6 (5)	Ce2—OS47—OB21	124.1 (4)
OH14—Si17—OT7	145.3 (11)	OT2—OS47—OB21	141.5 (5)
OH1—Si17—OT7	104.5 (9)	Si28—OS47—OB20	35.0 (3)
OB33—Si17—OT7	70.9 (5)	Ti12—OS47—OB20	101.2 (4)
OH31^xii—Si17—OT7	145.7 (7)	Ce2—OS47—OB20	153.4 (4)
OB35—Si17—OS16	90.6 (5)	OT2—OS47—OB20	141.9 (5)
OH14—Si17—OS16	150.2 (11)	OB21—OS47—OB20	57.4 (4)
OH1—Si17—OS16	80.5 (9)	Si28—OS47—OS25	33.2 (3)
OB33—Si17—OS16	43.3 (5)	Ti12—OS47—OS25	159.4 (5)
OH31^xii—Si17—OS16	100.0 (7)	Ce2—OS47—OS25	98.5 (3)
OT7—Si17—OS16	45.7 (2)	OT2—OS47—OS25	153.4 (4)
OB35—Si17—K3	106.8 (7)	OB21—OS47—OS25	58.3 (3)
OH14—Si17—K3	138.7 (11)	OB20—OS47—OS25	58.2 (3)
OH1—Si17—K3	38.8 (9)	Si28—OS47—OS38	110.0 (5)
OB33—Si17—K3	73.4 (6)	Ti12—OS47—OS38	43.1 (3)
OH31^xii—Si17—K3	76.6 (10)	Ce2—OS47—OS38	99.0 (3)
OT7—Si17—K3	75.4 (4)	OT2—OS47—OS38	64.0 (3)
OS16—Si17—K3	41.8 (4)	OB21—OS47—OS38	78.9 (4)
OS16—Si18—OS13	109.7 (5)	OB20—OS47—OS38	106.9 (4)
OS16—Si18—OB33	111.2 (6)	OS25—OS47—OS38	136.4 (5)
OS13—Si18—OB33	109.8 (6)	Si28—OS47—OS24	86.5 (4)
OS16—Si18—OB16	112.4 (6)	Ti12—OS47—OS24	43.5 (3)
OS13—Si18—OB16	108.8 (7)	Ce2—OS47—OS24	144.7 (4)
OB33—Si18—OB16	104.8 (7)	OT2—OS47—OS24	88.0 (4)
OS16—Si18—Si40	137.7 (5)	OB21—OS47—OS24	83.2 (4)
OS13—Si18—Si40	107.2 (5)	OB20—OS47—OS24	58.0 (3)
OB33—Si18—Si40	73.9 (6)	OS25—OS47—OS24	115.9 (4)
OB16—Si18—Si40	33.8 (5)	OS38—OS47—OS24	61.6 (3)
OS16—Si18—OT7	65.2 (4)	Si28—OS47—OHT1	127.4 (5)
OS13—Si18—OT7	63.4 (4)	Ti12—OS47—OHT1	45.3 (3)
OB33—Si18—OT7	86.3 (6)	Ce2—OS47—OHT1	93.6 (3)
OB16—Si18—OT7	168.5 (5)	OT2—OS47—OHT1	51.7 (3)
Si40—Si18—OT7	154.0 (4)	OB21—OS47—OHT1	141.4 (4)
OS16—Si18—OT3	55.3 (4)	OB20—OS47—OHT1	93.0 (4)
OS13—Si18—OT3	54.5 (4)	OS25—OS47—OHT1	129.9 (4)
OB33—Si18—OT3	130.8 (6)	OS38—OS47—OHT1	88.3 (4)
OB16—Si18—OT3	124.2 (5)	OS24—OS47—OHT1	58.9 (3)
Si40—Si18—OT3	151.0 (4)	Si28—OS47—OT5	89.8 (4)
OT7—Si18—OT3	44.5 (2)	Ti12—OS47—OT5	136.4 (4)
OS16—Si18—OH28	165.1 (6)	Ce2—OS47—OT5	51.8 (2)
OS13—Si18—OH28	84.5 (7)	OT2—OS47—OT5	96.9 (4)
OB33—Si18—OH28	66.1 (8)	OB21—OS47—OT5	112.0 (4)
OB16—Si18—OH28	56.8 (7)	OB20—OS47—OT5	101.8 (4)
Si40—Si18—OH28	27.9 (5)	OS25—OS47—OT5	57.1 (3)
OT7—Si18—OH28	127.7 (5)	OS38—OS47—OT5	150.5 (4)
OT3—Si18—OH28	138.1 (6)	OS24—OS47—OT5	144.1 (4)
OS16—Si18—OH27^xii	122.8 (6)	OHT1—OS47—OT5	97.0 (4)
OS13—Si18—OH27^xii	127.4 (6)	Si28—OS47—OS31	78.9 (4)
OB33—Si18—OH27^xii	56.3 (8)	Ti12—OS47—OS31	143.5 (4)
OB16—Si18—OH27^xii	48.8 (8)	Ce2—OS47—OS31	51.3 (2)
Si40—Si18—OH27^xii	24.9 (5)	OT2—OS47—OS31	105.5 (4)
OT7—Si18—OH27^xii	142.5 (7)	OB21—OS47—OS31	76.7 (3)
OT3—Si18—OH27^xii	172.7 (7)	OB20—OS47—OS31	112.1 (4)
OH28—Si18—OH27^xii	42.9 (7)	OS25—OS47—OS31	55.5 (3)
OS16—Si18—K3	41.3 (5)	OS38—OS47—OS31	110.1 (4)
OS13—Si18—K3	144.4 (5)	OS24—OS47—OS31	159.6 (4)
OB33—Si18—K3	75.8 (6)	OHT1—OS47—OS31	141.5 (4)
OB16—Si18—K3	103.1 (6)	OT5—OS47—OS31	51.0 (3)
Si40—Si18—K3	108.1 (5)	Si27—OS48—Ti7	129.4 (5)
OT7—Si18—K3	82.4 (4)	Si27—OS48—Ce2	128.1 (5)
OT3—Si18—K3	94.4 (4)	Ti7—OS48—Ce2	100.9 (3)
OH28—Si18—K3	127.2 (7)	Si27—OS48—OB14	35.6 (3)
OH27^xii—Si18—K3	85.8 (5)	Ti7—OS48—OB14	100.4 (4)
OS42—Si19—OH17	112.4 (5)	Ce2—OS48—OB14	156.9 (4)
OS42—Si19—OB8	111.5 (5)	Si27—OS48—OB31	34.1 (3)
OH17—Si19—OB8	109.6 (5)	Ti7—OS48—OB31	113.9 (4)
OS42—Si19—OB5	107.9 (5)	Ce2—OS48—OB31	119.9 (4)
OH17—Si19—OB5	112.3 (5)	OB14—OS48—OB31	57.9 (3)
OB8—Si19—OB5	102.7 (5)	Si27—OS48—OT2	170.8 (6)
OS42—Si19—OS27	57.0 (3)	Ti7—OS48—OT2	45.1 (3)
OH17—Si19—OS27	147.0 (4)	Ce2—OS48—OT2	55.9 (2)
OB8—Si19—OS27	103.1 (4)	OB14—OS48—OT2	143.6 (4)
OB5—Si19—OS27	54.4 (4)	OB31—OS48—OT2	137.3 (4)
OS42—Si19—Na10	130.1 (4)	Si27—OS48—OS43	33.0 (3)
OH17—Si19—Na10	117.0 (4)	Ti7—OS48—OS43	158.7 (4)
OB8—Si19—Na10	44.2 (4)	Ce2—OS48—OS43	99.8 (3)
OB5—Si19—Na10	59.3 (4)	OB14—OS48—OS43	58.4 (3)
OS27—Si19—Na10	83.8 (2)	OB31—OS48—OS43	58.6 (3)
OS42—Si19—Na12^iii	69.4 (4)	OT2—OS48—OS43	154.4 (4)
OH17—Si19—Na12^iii	45.0 (4)	Si27—OS48—OS9	108.0 (5)
OB8—Si19—Na12^iii	115.2 (6)	Ti7—OS48—OS9	45.8 (3)
OB5—Si19—Na12^iii	140.4 (6)	Ce2—OS48—OS9	97.4 (3)
OS27—Si19—Na12^iii	122.5 (3)	OB14—OS48—OS9	103.9 (4)
Na10—Si19—Na12^iii	152.6 (4)	OB31—OS48—OS9	77.3 (4)
OS42—Si19—OH4	132.2 (4)	OT2—OS48—OS9	62.8 (3)
OH17—Si19—OH4	42.2 (4)	OS43—OS48—OS9	135.6 (4)
OB8—Si19—OH4	115.3 (4)	Si27—OS48—OS7	88.5 (4)
OB5—Si19—OH4	70.4 (4)	Ti7—OS48—OS7	42.7 (3)
OS27—Si19—OH4	118.0 (2)	Ce2—OS48—OS7	143.2 (4)
Na10—Si19—OH4	91.5 (2)	OB14—OS48—OS7	57.8 (3)
Na12^iii—Si19—OH4	82.8 (4)	OB31—OS48—OS7	87.2 (4)
OS42—Si19—OHT2	136.1 (4)	OT2—OS48—OS7	87.4 (4)
OH17—Si19—OHT2	43.3 (4)	OS43—OS48—OS7	116.2 (4)
OB8—Si19—OHT2	66.9 (4)	OS9—OS48—OS7	62.4 (3)
OB5—Si19—OHT2	115.2 (4)	Si27—OS48—OHT1	131.8 (5)
OS27—Si19—OHT2	165.0 (2)	Ti7—OS48—OHT1	42.8 (2)
Na10—Si19—OHT2	81.25 (19)	Ce2—OS48—OHT1	92.3 (3)
Na12^iii—Si19—OHT2	72.5 (3)	OB14—OS48—OHT1	97.1 (4)
OH4—Si19—OHT2	60.9 (2)	OB31—OS48—OHT1	145.9 (4)
OS42—Si19—OHT3^iv	51.5 (4)	OT2—OS48—OHT1	51.5 (3)
OH17—Si19—OHT3^iv	151.5 (4)	OS43—OS48—OHT1	131.1 (4)
OB8—Si19—OHT3^iv	65.8 (4)	OS9—OS48—OHT1	88.3 (4)
OB5—Si19—OHT3^iv	95.9 (4)	OS7—OS48—OHT1	58.9 (3)
OS27—Si19—OHT3^iv	50.5 (2)	Si27—OS48—OT5	90.5 (4)
Na10—Si19—OHT3^iv	80.36 (19)	Ti7—OS48—OT5	135.5 (4)
Na12^iii—Si19—OHT3^iv	109.5 (3)	Ce2—OS48—OT5	52.1 (2)
OH4—Si19—OHT3^iv	166.3 (2)	OB14—OS48—OT5	105.5 (4)
OHT2—Si19—OHT3^iv	127.7 (2)	OB31—OS48—OT5	110.5 (4)
OS42—Si19—OB30	76.1 (4)	OT2—OS48—OT5	97.6 (4)
OH17—Si19—OB30	103.7 (4)	OS43—OS48—OT5	57.5 (3)
OB8—Si19—OB30	138.6 (4)	OS9—OS48—OT5	148.9 (4)
OB5—Si19—OB30	40.3 (4)	OS7—OS48—OT5	145.1 (4)
OS27—Si19—OB30	45.2 (2)	OHT1—OS48—OT5	97.8 (3)
Na10—Si19—OB30	98.6 (2)	Si27—OS48—OS1	77.2 (4)
Na12^iii—Si19—OB30	105.7 (4)	Ti7—OS48—OS1	143.9 (4)
OH4—Si19—OB30	75.2 (2)	Ce2—OS48—OS1	51.7 (2)
OHT2—Si19—OB30	136.0 (2)	OB14—OS48—OS1	111.7 (4)
OHT3^iv—Si19—OB30	95.0 (2)	OB31—OS48—OS1	72.9 (3)
OH12—Si20—OS39	111.6 (6)	OT2—OS48—OS1	104.6 (3)
OH12—Si20—OS22	109.3 (6)	OS43—OS48—OS1	56.3 (3)
OS39—Si20—OS22	109.2 (6)	OS9—OS48—OS1	108.3 (4)
OH12—Si20—OB17	110.0 (7)	OS7—OS48—OS1	159.8 (4)
OS39—Si20—OB17	108.3 (7)	OHT1—OS48—OS1	141.2 (4)
OS22—Si20—OB17	108.3 (6)	OT5—OS48—OS1	50.6 (3)
OH12—Si20—OHT1	165.9 (5)	Si23—OS49—Ti8	126.6 (5)
OS39—Si20—OHT1	63.9 (4)	Si23—OS49—Ce2	130.2 (5)
OS22—Si20—OHT1	62.5 (4)	Ti8—OS49—Ce2	102.3 (4)
OB17—Si20—OHT1	83.9 (5)	Si23—OS49—OB25	35.5 (3)
OH12—Si20—OT2	122.9 (5)	Ti8—OS49—OB25	109.2 (4)
OS39—Si20—OT2	54.0 (4)	Ce2—OS49—OB25	125.1 (4)
OS22—Si20—OT2	55.4 (4)	Si23—OS49—OT1	171.7 (5)
OB17—Si20—OT2	127.0 (6)	Ti8—OS49—OT1	45.9 (3)
OHT1—Si20—OT2	43.1 (2)	Ce2—OS49—OT1	56.6 (3)
OH12—Si20—OH23	105.4 (9)	OB25—OS49—OT1	138.3 (5)
OS39—Si20—OH23	66.3 (6)	Si23—OS49—OS38	33.5 (3)
OS22—Si20—OH23	143.6 (8)	Ti8—OS49—OS38	158.2 (5)
OB17—Si20—OH23	47.8 (6)	Ce2—OS49—OS38	99.2 (3)
OHT1—Si20—OH23	85.4 (8)	OB25—OS49—OS38	59.8 (4)
OT2—Si20—OH23	112.3 (6)	OT1—OS49—OS38	154.6 (4)
OH12—Si20—K2^vi	100.9 (5)	Si23—OS49—OB27	33.9 (3)
OS39—Si20—K2^vi	146.3 (5)	Ti8—OS49—OB27	100.4 (4)
OS22—Si20—K2^vi	49.1 (4)	Ce2—OS49—OB27	153.6 (4)
OB17—Si20—K2^vi	66.3 (5)	OB25—OS49—OB27	57.7 (3)
OHT1—Si20—K2^vi	82.4 (3)	OT1—OS49—OB27	142.5 (4)
OT2—Si20—K2^vi	101.0 (2)	OS38—OS49—OB27	57.9 (3)
OH23—Si20—K2^vi	113.9 (6)	Si23—OS49—OS37	112.5 (5)
OH12—Si20—OH24^xii	150.1 (6)	Ti8—OS49—OS37	43.7 (3)
OS39—Si20—OH24^xii	87.1 (6)	Ce2—OS49—OS37	95.3 (3)
OS22—Si20—OH24^xii	84.3 (6)	OB25—OS49—OS37	79.3 (4)
OB17—Si20—OH24^xii	40.3 (6)	OT1—OS49—OS37	60.0 (3)
OHT1—Si20—OH24^xii	43.7 (4)	OS38—OS49—OS37	137.6 (4)
OT2—Si20—OH24^xii	86.8 (4)	OB27—OS49—OS37	110.4 (4)
OH23—Si20—OH24^xii	59.8 (8)	Si23—OS49—OS14	84.1 (4)
K2^vi—Si20—OH24^xii	67.4 (5)	Ti8—OS49—OS14	43.8 (3)
OH12—Si20—OH26	66.8 (6)	Ce2—OS49—OS14	145.7 (4)
OS39—Si20—OH26	82.1 (6)	OB25—OS49—OS14	80.5 (4)
OS22—Si20—OH26	168.6 (7)	OT1—OS49—OS14	89.1 (4)
OB17—Si20—OH26	64.9 (7)	OS38—OS49—OS14	114.4 (4)
OHT1—Si20—OH26	123.6 (4)	OB27—OS49—OS14	56.9 (3)
OT2—Si20—OH26	136.0 (5)	OS37—OS49—OS14	64.9 (3)
OH23—Si20—OH26	38.6 (8)	Si23—OS49—OHT2	127.8 (5)
K2^vi—Si20—OH26	120.1 (6)	Ti8—OS49—OHT2	44.2 (2)
OH24^xii—Si20—OH26	94.6 (6)	Ce2—OS49—OHT2	92.5 (3)
OS6—Si21—OH5	111.8 (5)	OB25—OS49—OHT2	140.7 (4)
OS6—Si21—OH4	114.0 (5)	OT1—OS49—OHT2	51.3 (3)
OH5—Si21—OH4	109.9 (5)	OS38—OS49—OHT2	131.5 (4)
OS6—Si21—OB37	107.0 (5)	OB27—OS49—OHT2	94.4 (4)
OH5—Si21—OB37	106.7 (5)	OS37—OS49—OHT2	87.0 (3)
OH4—Si21—OB37	107.0 (5)	OS14—OS49—OHT2	60.3 (3)
OS6—Si21—Na5	128.4 (4)	Si23—OS49—OT2	92.1 (4)
OH5—Si21—Na5	119.8 (4)	Ti8—OS49—OT2	135.1 (4)
OH4—Si21—Na5	49.3 (4)	Ce2—OS49—OT2	51.0 (2)
OB37—Si21—Na5	57.8 (4)	OB25—OS49—OT2	115.7 (4)
OS6—Si21—OS41	56.5 (3)	OT1—OS49—OT2	96.2 (4)
OH5—Si21—OS41	134.4 (4)	OS38—OS49—OT2	59.3 (3)
OH4—Si21—OS41	114.8 (4)	OB27—OS49—OT2	102.9 (4)
OB37—Si21—OS41	52.1 (3)	OS37—OS49—OT2	146.3 (4)
Na5—Si21—OS41	84.9 (2)	OS14—OS49—OT2	143.9 (4)
OS6—Si21—Na6^vii	48.0 (4)	OHT2—OS49—OT2	95.9 (3)
OH5—Si21—Na6^vii	69.7 (4)	Si23—OS49—OS47	80.0 (4)
OH4—Si21—Na6^vii	153.2 (4)	Ti8—OS49—OS47	145.1 (4)
OB37—Si21—Na6^vii	98.3 (4)	Ce2—OS49—OS47	51.4 (2)
Na5—Si21—Na6^vii	155.3 (3)	OB25—OS49—OS47	78.8 (3)
OS41—Si21—Na6^vii	74.3 (2)	OT1—OS49—OS47	105.4 (4)
OS6—Si21—OB4	73.9 (4)	OS38—OS49—OS47	55.1 (3)
OH5—Si21—OB4	89.2 (4)	OB27—OS49—OS47	111.7 (4)
OH4—Si21—OB4	152.7 (4)	OS37—OS49—OS47	109.4 (4)
OB37—Si21—OB4	47.1 (4)	OS14—OS49—OS47	159.3 (4)
Na5—Si21—OB4	104.5 (3)	OHT2—OS49—OS47	140.4 (4)
OS41—Si21—OB4	45.8 (2)	OT2—OS49—OS47	50.6 (3)
Na6^vii—Si21—OB4	51.2 (2)	Ti9—OT1—Ti8	105.0 (4)
OS6—Si21—OH20^vii	104.1 (4)	Ti9—OT1—OHT2	53.6 (3)
OH5—Si21—OH20^vii	37.1 (4)	Ti8—OT1—OHT2	53.9 (3)
OH4—Si21—OH20^vii	81.8 (4)	Ti9—OT1—Ce2	108.1 (4)
OB37—Si21—OH20^vii	140.1 (4)	Ti8—OT1—Ce2	108.8 (4)
Na5—Si21—OH20^vii	117.2 (2)	OHT2—OT1—Ce2	107.7 (4)
OS41—Si21—OH20^vii	157.8 (2)	Ti9—OT1—OS41	50.1 (3)
Na6^vii—Si21—OH20^vii	84.5 (2)	Ti8—OT1—OS41	114.6 (4)
OB4—Si21—OH20^vii	123.0 (2)	OHT2—OT1—OS41	69.4 (3)
OS6—Si21—OHT2	49.4 (4)	Ce2—OT1—OS41	58.4 (3)
OH5—Si21—OHT2	158.8 (4)	Ti9—OT1—OS49	114.5 (4)
OH4—Si21—OHT2	75.9 (4)	Ti8—OT1—OS49	48.8 (3)
OB37—Si21—OHT2	90.2 (4)	OHT2—OT1—OS49	69.0 (4)
Na5—Si21—OHT2	79.9 (2)	Ce2—OT1—OS49	60.2 (3)
OS41—Si21—OHT2	48.9 (2)	OS41—OT1—OS49	84.4 (4)
Na6^vii—Si21—OHT2	95.7 (2)	Ti9—OT1—OW14^iii	110.4 (4)
OB4—Si21—OHT2	93.3 (2)	Ti8—OT1—OW14^iii	107.8 (4)
OH20^vii—Si21—OHT2	129.3 (2)	OHT2—OT1—OW14^iii	136.1 (5)
OS6—Si21—OH17	77.4 (4)	Ce2—OT1—OW14^iii	116.1 (4)
OH5—Si21—OH17	133.4 (4)	OS41—OT1—OW14^iii	136.6 (4)
OH4—Si21—OH17	37.1 (4)	OS49—OT1—OW14^iii	133.3 (4)
OB37—Si21—OH17	114.0 (4)	Ti9—OT1—OS37	145.6 (5)
Na5—Si21—OH17	68.8 (2)	Ti8—OT1—OS37	44.6 (3)
OS41—Si21—OH17	89.8 (2)	OHT2—OT1—OS37	98.5 (4)
Na6^vii—Si21—OH17	123.1 (2)	Ce2—OT1—OS37	98.9 (3)
OB4—Si21—OH17	135.4 (2)	OS41—OT1—OS37	146.0 (4)
OH20^vii—Si21—OH17	96.6 (2)	OS49—OT1—OS37	61.7 (3)
OHT2—Si21—OH17	42.4 (2)	OW14^iii—OT1—OS37	74.3 (4)
OS6—Si21—OW24^iii	55.6 (4)	Ti9—OT1—OS8	44.3 (3)
OH5—Si21—OW24^iii	58.7 (4)	Ti8—OT1—OS8	145.5 (4)
OH4—Si21—OW24^iii	117.0 (5)	OHT2—OT1—OS8	97.9 (4)
OB37—Si21—OW24^iii	135.9 (4)	Ce2—OT1—OS8	98.0 (3)
Na5—Si21—OW24^iii	166.1 (3)	OS41—OT1—OS8	62.1 (3)
OS41—Si21—OW24^iii	105.7 (3)	OS49—OT1—OS8	146.5 (4)
Na6^vii—Si21—OW24^iii	38.5 (3)	OW14^iii—OT1—OS8	77.8 (4)
OB4—Si21—OW24^iii	89.4 (3)	OS37—OT1—OS8	151.6 (4)
OH20^vii—Si21—OW24^iii	52.2 (3)	Ti9—OT1—OS3^iii	43.1 (3)
OHT2—Si21—OW24^iii	100.2 (3)	Ti8—OT1—OS3^iii	90.9 (4)
OH17—Si21—OW24^iii	101.7 (3)	OHT2—OT1—OS3^iii	65.3 (3)
OS41—Si22—OS9	114.3 (5)	Ce2—OT1—OS3^iii	149.8 (4)
OS41—Si22—OB37	111.0 (5)	OS41—OT1—OS3^iii	93.0 (4)
OS9—Si22—OB37	106.5 (5)	OS49—OT1—OS3^iii	131.9 (4)
OS41—Si22—OB4	107.8 (5)	OW14^iii—OT1—OS3^iii	76.9 (4)
OS9—Si22—OB4	111.7 (5)	OS37—OT1—OS3^iii	111.0 (4)
OB37—Si22—OB4	105.2 (5)	OS8—OT1—OS3^iii	56.5 (3)
OS41—Si22—OS6	65.5 (4)	Ti9—OT1—OS5^iii	89.2 (4)
OS9—Si22—OS6	160.6 (4)	Ti8—OT1—OS5^iii	41.4 (2)
OB37—Si22—OS6	58.7 (4)	OHT2—OT1—OS5^iii	62.5 (3)
OB4—Si22—OS6	85.6 (4)	Ce2—OT1—OS5^iii	149.7 (4)
OS41—Si22—OS48	72.3 (3)	OS41—OT1—OS5^iii	130.1 (4)
OS9—Si22—OS48	55.0 (4)	OS49—OT1—OS5^iii	90.2 (4)
OB37—Si22—OS48	158.0 (4)	OW14^iii—OT1—OS5^iii	78.3 (3)
OB4—Si22—OS48	93.9 (4)	OS37—OT1—OS5^iii	57.7 (3)
OS6—Si22—OS48	135.3 (3)	OS8—OT1—OS5^iii	111.5 (4)
OS41—Si22—OB31	97.6 (4)	OS3^iii—OT1—OS5^iii	55.8 (3)
OS9—Si22—OB31	74.5 (4)	Ti9—OT1—OS31	158.5 (4)
OB37—Si22—OB31	146.9 (4)	Ti8—OT1—OS31	92.0 (3)
OB4—Si22—OB31	48.2 (4)	OHT2—OT1—OS31	136.0 (4)
OS6—Si22—OB31	124.9 (3)	Ce2—OT1—OS31	52.9 (2)
OS48—Si22—OB31	46.9 (2)	OS41—OT1—OS31	111.0 (4)
OS41—Si22—OT2	61.3 (3)	OS49—OT1—OS31	67.4 (3)
OS9—Si22—OT2	54.6 (4)	OW14^iii—OT1—OS31	75.5 (3)
OB37—Si22—OT2	114.0 (4)	OS37—OT1—OS31	55.4 (3)
OB4—Si22—OT2	140.7 (4)	OS8—OT1—OS31	121.8 (4)
OS6—Si22—OT2	117.0 (2)	OS3^iii—OT1—OS31	151.8 (4)
OS48—Si22—OT2	47.2 (2)	OS5^iii—OT1—OS31	112.3 (4)
OB31—Si22—OT2	93.8 (2)	Ti7—OT2—Ti12	104.8 (4)
OS41—Si22—OW11	65.6 (4)	Ti7—OT2—OHT1	52.3 (3)
OS9—Si22—OW11	81.6 (4)	Ti12—OT2—OHT1	54.8 (3)
OB37—Si22—OW11	68.6 (4)	Ti7—OT2—Ce2	109.0 (4)
OB4—Si22—OW11	166.6 (4)	Ti12—OT2—Ce2	107.7 (4)
OS6—Si22—OW11	81.0 (2)	OHT1—OT2—Ce2	107.8 (4)
OS48—Si22—OW11	94.9 (2)	Ti7—OT2—OS47	112.7 (4)
OB31—Si22—OW11	141.7 (2)	Ti12—OT2—OS47	49.0 (3)
OT2—Si22—OW11	47.9 (2)	OHT1—OT2—OS47	68.6 (4)
OS41—Si22—OH21^vi	156.3 (4)	Ce2—OT2—OS47	59.2 (3)
OS9—Si22—OH21^vi	46.4 (4)	Ti7—OT2—OS48	48.6 (3)
OB37—Si22—OH21^vi	90.1 (4)	Ti12—OT2—OS48	115.0 (4)
OB4—Si22—OH21^vi	75.2 (4)	OHT1—OT2—OS48	68.5 (3)
OS6—Si22—OH21^vi	137.7 (3)	Ce2—OT2—OS48	60.5 (3)
OS48—Si22—OH21^vi	84.1 (2)	OS47—OT2—OS48	84.3 (4)
OB31—Si22—OH21^vi	66.3 (2)	Ti7—OT2—OS39	90.3 (4)
OT2—Si22—OH21^vi	101.0 (2)	Ti12—OT2—OS39	43.0 (3)
OW11—Si22—OH21^vi	115.8 (3)	OHT1—OT2—OS39	65.3 (3)
OS38—Si23—OS49	112.5 (5)	Ce2—OT2—OS39	149.6 (4)
OS38—Si23—OB27	107.3 (5)	OS47—OT2—OS39	92.1 (4)
OS49—Si23—OB27	112.4 (5)	OS48—OT2—OS39	131.6 (4)
OS38—Si23—OB25	110.4 (5)	Ti7—OT2—OS9	43.7 (3)
OS49—Si23—OB25	109.3 (5)	Ti12—OT2—OS9	145.6 (4)
OB27—Si23—OB25	104.7 (5)	OHT1—OT2—OS9	96.0 (4)
OS38—Si23—OS14	157.1 (4)	Ce2—OT2—OS9	97.9 (3)
OS49—Si23—OS14	64.1 (4)	OS47—OT2—OS9	143.3 (4)
OB27—Si23—OS14	58.4 (4)	OS48—OT2—OS9	59.0 (3)
OB25—Si23—OS14	91.4 (4)	OS39—OT2—OS9	112.1 (4)
OS38—Si23—OS47	55.8 (4)	Ti7—OT2—OW11	117.7 (4)
OS49—Si23—OS47	71.0 (4)	Ti12—OT2—OW11	113.2 (4)
OB27—Si23—OS47	160.5 (4)	OHT1—OT2—OW11	148.0 (5)
OB25—Si23—OS47	91.4 (4)	Ce2—OT2—OW11	104.1 (3)
OS14—Si23—OS47	133.3 (2)	OS47—OT2—OW11	129.5 (4)
OS38—Si23—OB21	75.0 (4)	OS48—OT2—OW11	131.8 (4)
OS49—Si23—OB21	97.9 (4)	OS39—OT2—OW11	86.1 (4)
OB27—Si23—OB21	144.9 (4)	OS9—OT2—OW11	81.1 (3)
OB25—Si23—OB21	46.0 (4)	Ti7—OT2—OS22	42.9 (3)
OS14—Si23—OB21	127.5 (3)	Ti12—OT2—OS22	90.1 (4)
OS47—Si23—OB21	46.6 (2)	OHT1—OT2—OS22	63.7 (3)
OS38—Si23—OT2	53.1 (3)	Ce2—OT2—OS22	151.1 (4)
OS49—Si23—OT2	60.5 (4)	OS47—OT2—OS22	130.0 (4)
OB27—Si23—OT2	117.7 (4)	OS48—OT2—OS22	91.5 (4)
OB25—Si23—OT2	137.2 (4)	OS39—OT2—OS22	55.3 (3)
OS14—Si23—OT2	114.8 (2)	OS9—OT2—OS22	58.0 (3)
OS47—Si23—OT2	45.9 (2)	OW11—OT2—OS22	88.7 (4)
OB21—Si23—OT2	92.2 (2)	Ti7—OT2—OS38	142.6 (4)
OS38—Si23—OW11	78.6 (4)	Ti12—OT2—OS38	40.2 (3)
OS49—Si23—OW11	64.3 (4)	OHT1—OT2—OS38	95.0 (4)
OB27—Si23—OW11	73.3 (4)	Ce2—OT2—OS38	97.3 (3)
OB25—Si23—OW11	170.8 (4)	OS47—OT2—OS38	59.1 (3)
OS14—Si23—OW11	79.9 (2)	OS48—OT2—OS38	143.4 (4)
OS47—Si23—OW11	92.4 (2)	OS39—OT2—OS38	56.0 (3)
OB21—Si23—OW11	138.9 (2)	OS9—OT2—OS38	157.5 (4)
OT2—Si23—OW11	46.7 (2)	OW11—OT2—OS38	79.1 (3)
OH18—Si24—OB21	110.0 (6)	OS22—OT2—OS38	110.7 (4)
OH18—Si24—OB24	111.3 (6)	Ti7—OT2—OS41	93.0 (3)
OB21—Si24—OB24	108.2 (5)	Ti12—OT2—OS41	158.4 (4)
OH18—Si24—OB25	109.8 (6)	OHT1—OT2—OS41	136.2 (4)
OB21—Si24—OB25	108.0 (6)	Ce2—OT2—OS41	53.8 (2)
OB24—Si24—OB25	109.5 (6)	OS47—OT2—OS41	112.8 (4)
OH18—Si24—OW37	45.6 (5)	OS48—OT2—OS41	68.1 (3)
OB21—Si24—OW37	107.9 (5)	OS39—OT2—OS41	151.2 (4)
OB24—Si24—OW37	142.6 (5)	OS9—OT2—OS41	55.5 (3)
OB25—Si24—OW37	67.5 (4)	OW11—OT2—OS41	67.1 (3)
OH18—Si24—OS31	150.6 (5)	OS22—OT2—OS41	111.4 (4)
OB21—Si24—OS31	77.9 (4)	OS38—OT2—OS41	124.2 (4)
OB24—Si24—OS31	41.5 (4)	Ti5—OT3—Ti3^iv	108.0 (4)
OB25—Si24—OS31	93.5 (4)	Ti5—OT3—OT7	55.8 (3)
OW37—Si24—OS31	161.0 (3)	Ti3^iv—OT3—OT7	54.1 (3)
OH18—Si24—OS49	149.7 (5)	Ti5—OT3—Ce1^iv	107.7 (4)
OB21—Si24—OS49	92.3 (4)	Ti3^iv—OT3—Ce1^iv	107.4 (4)
OB24—Si24—OS49	79.0 (4)	OT7—OT3—Ce1^iv	108.7 (4)
OB25—Si24—OS49	41.6 (4)	Ti5—OT3—OS45	49.7 (3)
OW37—Si24—OS49	108.9 (3)	Ti3^iv—OT3—OS45	115.0 (4)
OS31—Si24—OS49	52.2 (2)	OT7—OT3—OS45	70.7 (4)
OH18—Si24—OW1^iv	80.9 (9)	Ce1^iv—OT3—OS45	58.4 (3)
OB21—Si24—OW1^iv	65.4 (8)	Ti5—OT3—OS35^iv	114.3 (4)
OB24—Si24—OW1^iv	167.8 (8)	Ti3^iv—OT3—OS35^iv	49.8 (3)
OB25—Si24—OW1^iv	65.0 (8)	OT7—OT3—OS35^iv	69.0 (4)
OW37—Si24—OW1^iv	47.2 (8)	Ce1^iv—OT3—OS35^iv	58.2 (3)
OS31—Si24—OW1^iv	126.5 (8)	OS45—OT3—OS35^iv	82.2 (4)
OS49—Si24—OW1^iv	90.7 (8)	Ti5—OT3—OS17	41.4 (3)
OH20—Si25—OB31	112.9 (5)	Ti3^iv—OT3—OS17	145.9 (4)
OH20—Si25—OB4	110.5 (5)	OT7—OT3—OS17	97.1 (4)
OB31—Si25—OB4	107.5 (5)	Ce1^iv—OT3—OS17	98.7 (3)
OH20—Si25—OB3	108.9 (5)	OS45—OT3—OS17	61.5 (3)
OB31—Si25—OB3	108.2 (5)	OS35^iv—OT3—OS17	143.7 (4)
OB4—Si25—OB3	108.8 (5)	Ti5—OT3—OS13	91.4 (4)
OH20—Si25—OH5^vii	47.3 (4)	Ti3^iv—OT3—OS13	42.3 (3)
OB31—Si25—OH5^vii	156.1 (4)	OT7—OT3—OS13	62.3 (4)
OB4—Si25—OH5^vii	74.7 (4)	Ce1^iv—OT3—OS13	149.2 (4)
OB3—Si25—OH5^vii	92.9 (4)	OS45—OT3—OS13	131.3 (4)
OH20—Si25—Na6^vii	88.6 (4)	OS35^iv—OT3—OS13	92.1 (4)
OB31—Si25—Na6^vii	157.6 (4)	OS17—OT3—OS13	111.4 (4)
OB4—Si25—Na6^vii	56.6 (4)	Ti5—OT3—OS4^iv	146.1 (4)
OB3—Si25—Na6^vii	67.8 (4)	Ti3^iv—OT3—OS4^iv	41.1 (3)
OH5^vii—Si25—Na6^vii	42.3 (2)	OT7—OT3—OS4^iv	95.2 (4)
OH20—Si25—OS1	152.0 (4)	Ce1^iv—OT3—OS4^iv	97.5 (3)
OB31—Si25—OS1	73.9 (4)	OS45—OT3—OS4^iv	143.1 (4)
OB4—Si25—OS1	91.8 (4)	OS35^iv—OT3—OS4^iv	60.9 (3)
OB3—Si25—OS1	45.6 (3)	OS17—OT3—OS4^iv	155.4 (4)
OH5^vii—Si25—OS1	130.0 (2)	OS13—OT3—OS4^iv	56.9 (3)
Na6^vii—Si25—OS1	89.9 (2)	Ti5—OT3—OS16	42.2 (3)
OH20—Si25—OS8	128.4 (4)	Ti3^iv—OT3—OS16	91.3 (4)
OB31—Si25—OS8	116.5 (4)	OT7—OT3—OS16	63.0 (4)
OB4—Si25—OS8	67.7 (4)	Ce1^iv—OT3—OS16	149.4 (4)
OB3—Si25—OS8	41.3 (4)	OS45—OT3—OS16	92.0 (4)
OH5^vii—Si25—OS8	86.7 (2)	OS35^iv—OT3—OS16	130.7 (4)
Na6^vii—Si25—OS8	45.4 (2)	OS17—OT3—OS16	56.3 (3)
OS1—Si25—OS8	44.48 (19)	OS13—OT3—OS16	56.3 (3)
OH20—Si25—OS41	149.9 (4)	OS4^iv—OT3—OS16	112.2 (4)
OB31—Si25—OS41	88.8 (4)	Ti5—OT3—OW27	116.0 (4)
OB4—Si25—OS41	40.4 (3)	Ti3^iv—OT3—OW27	113.5 (4)
OB3—Si25—OS41	81.8 (4)	OT7—OT3—OW27	147.6 (5)
OH5^vii—Si25—OS41	105.6 (2)	Ce1^iv—OT3—OW27	103.6 (3)
Na6^vii—Si25—OS41	68.9 (2)	OS45—OT3—OW27	131.4 (4)
OS1—Si25—OS41	51.73 (19)	OS35^iv—OT3—OW27	129.6 (4)
OS8—Si25—OS41	45.14 (19)	OS17—OT3—OW27	80.1 (4)
OS31—Si26—OS37	114.4 (5)	OS13—OT3—OW27	88.5 (4)
OS31—Si26—OB24	109.6 (5)	OS4^iv—OT3—OW27	78.1 (3)
OS37—Si26—OB24	109.5 (5)	OS16—OT3—OW27	90.0 (4)
OS31—Si26—OB23	109.7 (5)	Ti5—OT3—OS2^iv	159.2 (4)
OS37—Si26—OB23	106.1 (5)	Ti3^iv—OT3—OS2^iv	88.5 (3)
OB24—Si26—OB23	107.3 (5)	OT7—OT3—OS2^iv	134.4 (4)
OS31—Si26—OS34	62.9 (4)	Ce1^iv—OT3—OS2^iv	53.8 (2)
OS37—Si26—OS34	156.3 (4)	OS45—OT3—OS2^iv	112.2 (4)
OB24—Si26—OS34	92.7 (4)	OS35^iv—OT3—OS2^iv	66.6 (3)
OB23—Si26—OS34	57.6 (4)	OS17—OT3—OS2^iv	125.1 (4)
OS31—Si26—OS49	72.2 (4)	OS13—OT3—OS2^iv	109.4 (4)
OS37—Si26—OS49	56.7 (4)	OS4^iv—OT3—OS2^iv	54.0 (3)
OB24—Si26—OS49	91.0 (4)	OS16—OT3—OS2^iv	153.4 (4)
OB23—Si26—OS49	158.9 (5)	OW27—OT3—OS2^iv	65.9 (3)
OS34—Si26—OS49	133.5 (3)	Ti6—OT4—Ti4^v	99.3 (4)
OS31—Si26—OT1	64.0 (3)	Ti6—OT4—OHT4	50.6 (3)
OS37—Si26—OT1	51.6 (3)	Ti4^v—OT4—OHT4	50.4 (3)
OB24—Si26—OT1	137.9 (4)	Ti6—OT4—Ce1^v	108.5 (4)
OB23—Si26—OT1	113.9 (4)	Ti4^v—OT4—Ce1^v	107.7 (4)
OS34—Si26—OT1	115.8 (2)	OHT4—OT4—Ce1^v	107.9 (4)
OS49—Si26—OT1	46.9 (2)	Ti6—OT4—OS36^v	111.6 (4)
OS31—Si26—OB25	98.2 (4)	Ti4^v—OT4—OS36^v	47.8 (3)
OS37—Si26—OB25	74.7 (4)	OHT4—OT4—OS36^v	68.8 (4)
OB24—Si26—OB25	46.4 (4)	Ce1^v—OT4—OS36^v	59.9 (3)
OB23—Si26—OB25	148.0 (4)	Ti6—OT4—OS46^iv	49.4 (3)
OS34—Si26—OB25	128.5 (3)	Ti4^v—OT4—OS46^iv	110.3 (4)
OS49—Si26—OB25	45.7 (2)	OHT4—OT4—OS46^iv	68.7 (4)
OT1—Si26—OB25	92.0 (2)	Ce1^v—OT4—OS46^iv	59.1 (3)
OS31—Si26—Na2^iii	119.6 (4)	OS36^v—OT4—OS46^iv	83.9 (4)
OS37—Si26—Na2^iii	48.3 (4)	Ti6—OT4—OW26^v	106.7 (5)
OB24—Si26—Na2^iii	130.8 (4)	Ti4^v—OT4—OW26^v	107.9 (5)
OB23—Si26—Na2^iii	58.9 (4)	OHT4—OT4—OW26^v	128.1 (5)
OS34—Si26—Na2^iii	110.6 (2)	Ce1^v—OT4—OW26^v	124.0 (5)
OS49—Si26—Na2^iii	101.3 (2)	OS36^v—OT4—OW26^v	137.1 (5)
OT1—Si26—Na2^iii	69.2 (2)	OS46^iv—OT4—OW26^v	137.5 (5)
OB25—Si26—Na2^iii	119.8 (2)	Ti6—OT4—OS15^iv	45.5 (3)
OS31—Si26—OW14^iii	77.3 (4)	Ti4^v—OT4—OS15^iv	142.3 (5)
OS37—Si26—OW14^iii	67.5 (4)	OHT4—OT4—OS15^iv	96.1 (4)
OB24—Si26—OW14^iii	173.0 (4)	Ce1^v—OT4—OS15^iv	98.2 (4)
OB23—Si26—OW14^iii	68.5 (4)	OS36^v—OT4—OS15^iv	144.8 (5)
OS34—Si26—OW14^iii	89.6 (3)	OS46^iv—OT4—OS15^iv	60.9 (3)
OS49—Si26—OW14^iii	92.2 (2)	OW26^v—OT4—OS15^iv	77.5 (5)
OT1—Si26—OW14^iii	45.5 (2)	Ti6—OT4—OS11^v	141.7 (5)
OB25—Si26—OW14^iii	135.2 (3)	Ti4^v—OT4—OS11^v	46.0 (3)
Na2^iii—Si26—OW14^iii	42.4 (2)	OHT4—OT4—OS11^v	96.3 (4)
OS43—Si27—OS48	113.8 (5)	Ce1^v—OT4—OS11^v	99.2 (4)
OS43—Si27—OB31	109.3 (5)	OS36^v—OT4—OS11^v	60.9 (4)
OS48—Si27—OB31	111.8 (5)	OS46^iv—OT4—OS11^v	144.7 (5)
OS43—Si27—OB14	106.9 (5)	OW26^v—OT4—OS11^v	77.1 (5)
OS48—Si27—OB14	109.6 (5)	OS15^iv—OT4—OS11^v	154.3 (5)
OB31—Si27—OB14	104.8 (5)	Ti6—OT4—OS21	42.7 (3)
OS43—Si27—OS1	60.6 (4)	Ti4^v—OT4—OS21	88.5 (4)
OS48—Si27—OS1	73.4 (4)	OHT4—OT4—OS21	63.1 (4)
OB31—Si27—OS1	85.9 (4)	Ce1^v—OT4—OS21	150.1 (4)
OB14—Si27—OS1	166.2 (4)	OS36^v—OT4—OS21	129.7 (5)
OS43—Si27—OS7	151.2 (4)	OS46^iv—OT4—OS21	92.0 (4)
OS48—Si27—OS7	61.4 (4)	OW26^v—OT4—OS21	71.0 (4)
OB31—Si27—OS7	97.9 (4)	OS15^iv—OT4—OS21	57.2 (4)
OB14—Si27—OS7	55.5 (4)	OS11^v—OT4—OS21	109.9 (4)
OS1—Si27—OS7	132.7 (3)	Ti6—OT4—OS23	87.8 (4)
OS43—Si27—OW31^vii	47.6 (5)	Ti4^v—OT4—OS23	41.1 (3)
OS48—Si27—OW31^vii	109.8 (5)	OHT4—OT4—OS23	61.1 (4)
OB31—Si27—OW31^vii	138.2 (5)	Ce1^v—OT4—OS23	148.0 (5)
OB14—Si27—OW31^vii	63.9 (5)	OS36^v—OT4—OS23	88.7 (4)
OS1—Si27—OW31^vii	102.3 (4)	OS46^iv—OT4—OS23	128.4 (5)
OS7—Si27—OW31^vii	105.2 (4)	OW26^v—OT4—OS23	73.8 (4)
OS43—Si27—OT5	52.1 (3)	OS15^iv—OT4—OS23	112.3 (4)
OS48—Si27—OT5	61.8 (4)	OS11^v—OT4—OS23	56.0 (3)
OB31—Si27—OT5	132.5 (4)	OS21—OT4—OS23	55.8 (4)
OB14—Si27—OT5	122.0 (4)	Ti6—OT4—OS35^v	160.5 (5)
OS1—Si27—OT5	46.7 (2)	Ti4^v—OT4—OS35^v	93.7 (4)
OS7—Si27—OT5	114.1 (2)	OHT4—OT4—OS35^v	135.7 (5)
OW31^vii—Si27—OT5	66.8 (4)	Ce1^v—OT4—OS35^v	53.3 (2)
OS43—Si27—OB18	140.3 (4)	OS36^v—OT4—OS35^v	67.4 (3)
OS48—Si27—OB18	103.4 (4)	OS46^iv—OT4—OS35^v	112.3 (4)
OB31—Si27—OB18	66.3 (4)	OW26^v—OT4—OS35^v	82.8 (4)
OB14—Si27—OB18	44.6 (4)	OS15^iv—OT4—OS35^v	124.0 (4)
OS1—Si27—OB18	148.9 (3)	OS11^v—OT4—OS35^v	56.2 (3)
OS7—Si27—OB18	45.3 (3)	OS21—OT4—OS35^v	153.0 (4)
OW31^vii—Si27—OB18	107.6 (4)	OS23—OT4—OS35^v	111.4 (4)
OT5—Si27—OB18	158.2 (3)	Ti10—OT5—Ti11	107.3 (4)
OS43—Si27—OS9	149.4 (4)	Ti10—OT5—OS44	55.3 (3)
OS48—Si27—OS9	46.5 (4)	Ti11—OT5—OS44	54.6 (3)
OB31—Si27—OS9	69.9 (4)	Ti10—OT5—Ce2	107.7 (4)
OB14—Si27—OS9	102.5 (4)	Ti11—OT5—Ce2	108.9 (4)
OS1—Si27—OS9	89.2 (2)	OS44—OT5—Ce2	107.8 (4)
OS7—Si27—OS9	49.8 (2)	Ti10—OT5—OS1	116.3 (4)
OW31^vii—Si27—OS9	149.5 (4)	Ti11—OT5—OS1	50.1 (3)
OT5—Si27—OS9	104.6 (2)	OS44—OT5—OS1	69.8 (4)
OB18—Si27—OS9	69.0 (2)	Ce2—OT5—OS1	59.1 (3)
OS43—Si27—OW34	73.5 (4)	Ti10—OT5—OS31	50.1 (3)
OS48—Si27—OW34	64.0 (4)	Ti11—OT5—OS31	116.0 (4)
OB31—Si27—OW34	175.8 (5)	OS44—OT5—OS31	70.1 (3)
OB14—Si27—OW34	76.9 (4)	Ce2—OT5—OS31	58.1 (3)
OS1—Si27—OW34	93.1 (3)	OS1—OT5—OS31	84.4 (3)
OS7—Si27—OW34	79.8 (3)	Ti10—OT5—OS43	145.4 (5)
OW31^vii—Si27—OW34	45.9 (4)	Ti11—OT5—OS43	42.2 (3)
OT5—Si27—OW34	46.6 (2)	OS44—OT5—OS43	96.7 (4)
OB18—Si27—OW34	113.7 (3)	Ce2—OT5—OS43	99.8 (3)
OS9—Si27—OW34	106.1 (3)	OS1—OT5—OS43	61.5 (3)
OS43—Si27—OB3	78.3 (4)	OS31—OT5—OS43	145.9 (4)
OS48—Si27—OB3	101.9 (4)	Ti10—OT5—OW34	113.9 (4)
OB31—Si27—OB3	41.5 (4)	Ti11—OT5—OW34	113.7 (5)
OB14—Si27—OB3	141.8 (4)	OS44—OT5—OW34	147.1 (5)
OS1—Si27—OB3	45.7 (2)	Ce2—OT5—OW34	105.1 (4)
OS7—Si27—OB3	130.1 (3)	OS1—OT5—OW34	129.8 (5)
OW31^vii—Si27—OB3	124.5 (4)	OS31—OT5—OW34	130.4 (4)
OT5—Si27—OB3	91.6 (2)	OS43—OT5—OW34	77.4 (4)
OB18—Si27—OB3	107.8 (2)	Ti10—OT5—OS25	41.7 (3)
OS9—Si27—OB3	83.6 (2)	Ti11—OT5—OS25	145.6 (5)
OW34—Si27—OB3	138.2 (3)	OS44—OT5—OS25	97.0 (4)
OB21—Si28—OS25	108.8 (6)	Ce2—OT5—OS25	97.4 (3)
OB21—Si28—OS47	111.8 (5)	OS1—OT5—OS25	144.9 (4)
OS25—Si28—OS47	113.4 (5)	OS31—OT5—OS25	60.5 (3)
OB21—Si28—OB20	104.8 (6)	OS43—OT5—OS25	153.6 (4)
OS25—Si28—OB20	107.3 (5)	OW34—OT5—OS25	78.8 (4)
OS47—Si28—OB20	110.4 (5)	Ti10—OT5—OS26	42.1 (3)
OB21—Si28—OS24	94.2 (4)	Ti11—OT5—OS26	90.1 (4)
OS25—Si28—OS24	155.8 (4)	OS44—OT5—OS26	63.5 (4)
OS47—Si28—OS24	62.3 (4)	Ce2—OT5—OS26	149.3 (4)
OB20—Si28—OS24	57.7 (4)	OS1—OT5—OS26	131.3 (4)
OB21—Si28—OS31	90.1 (4)	OS31—OT5—OS26	92.2 (4)
OS25—Si28—OS31	57.8 (4)	OS43—OT5—OS26	110.3 (4)
OS47—Si28—OS31	71.6 (4)	OW34—OT5—OS26	87.9 (4)
OB20—Si28—OS31	162.3 (4)	OS25—OT5—OS26	57.3 (3)
OS24—Si28—OS31	131.8 (3)	Ti10—OT5—OS32	90.5 (4)
OB21—Si28—OW36	139.6 (5)	Ti11—OT5—OS32	41.4 (3)
OS25—Si28—OW36	53.4 (5)	OS44—OT5—OS32	62.9 (3)
OS47—Si28—OW36	108.6 (5)	Ce2—OT5—OS32	149.8 (4)
OB20—Si28—OW36	59.2 (5)	OS1—OT5—OS32	91.5 (4)
OS24—Si28—OW36	103.8 (4)	OS31—OT5—OS32	131.1 (4)
OS31—Si28—OW36	103.2 (4)	OS43—OT5—OS32	56.1 (3)
OB21—Si28—OT5	136.8 (4)	OW34—OT5—OS32	88.2 (4)
OS25—Si28—OT5	51.8 (4)	OS25—OT5—OS32	111.8 (4)
OS47—Si28—OT5	62.3 (4)	OS26—OT5—OS32	55.6 (3)
OB20—Si28—OT5	117.5 (4)	Ti10—OT5—OS48	159.7 (4)