Figure 3
Analysis of VioC data. (a) Normalized average background count for anaerobic (magenta) and air-exposed setups (black) resulting from ∼3.0 × 1010 photons at 12.8 keV with a beam size of 8 × 8 µm. (b) Rsplit (black) and CC1/2 (magenta) plotted against the resolution for anaerobic VioC:Fe:2OG (solid line) and O2-exposed VioC:Fe:succinate (dashed line) datasets. The analysis was done for 10 200 randomly selected integrated frames. (c) Stereographic projections illustrating the crystal orientation of 6400 randomly selected crystals for air-exposed VioC:Fe:2OG (left) and anaerobic VioC:Fe:succinate (right) datasets. The plots represent the direction of the hkl 001 of each crystal relative to the beam direction (z). For data collected on chips, the direction of hkl 001 to <45° movement away from the beam direction seems to be favoured. |