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Figure 4
(a) In situ GI-PDFs from total scattering at some selected measurement temperatures for the ZSA2 film over the range 0–30 Å. The corresponding PDF data over 0–15 and 0–60 Å are shown in Fig. S13(a)–S13(b). Fits (red solid curve) to the experimental PDF data (blue open circles): (b) at 573 K after a dwell time of 1 h, and (c)–(d) at 525 K. In (b), (c) and (d), the difference between the experimental data and model fit is shown in green, and the refined parameters for the fits are given in Tables S7, S8 and S9.

IUCrJ
Volume 8| Part 3| May 2021| Pages 444-454
ISSN: 2052-2525
https://doi.org/10.1107/S2052252521002852