Figure 7
HS-POM images of the polycrystalline powders after milling for 30 min showing the change in polarization colour at different defect density zones during the heating process. (a) HS-POM image of the pure β form, (b)–(d) rapid first-step phase transition, (d)–(h) slow second-step phase transition [crystals in (h) are α form]. Defect areas are marked by red circles. |