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Figure 3
Geometry of the high-pressure single-crystal diffraction experiment at APS 13-BM-C. X-ray direction together with φ, χ and 2θ angles are labelled. Inset: image of the DAC sample chamber after He gas loading, showing four Lb crystals and one ruby sphere. The diameter of the sample chamber was 0.274 mm, indicated by the red scale bar.

IUCrJ
Volume 9| Part 1| January 2022| Pages 146-162
ISSN: 2052-2525
https://doi.org/10.1107/S2052252521012628