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Figure 4
(a) HAADF–STEM image of a typical crystal of com­pound I, used for 3D ED data acquisition. (b)/(c)/(d) Reconstructed 3D ED data viewed along the main crystallographic directions. Note that these are projections of a 3D diffraction volume and not 2D oriented ED patterns, and therefore axial extinctions are not visible.

IUCrJ
Volume 10| Part 1| January 2023| Pages 131-142
ISSN: 2052-2525