Analysis of COF-300 synthesis: probing degradation processes and 3D electron diffraction structure

Bourda, L.; Bhandary, S.; Ito, S.; Göb, C.R.; Van Der Voort, P.; Van Hecke, K.

doi:10.1107/S2052252524003713

Figure 2
Normalized background-corrected (a) PXRD and (b) N₂-sorption analysis of COF-300 synthesized via different approaches: intermediate-assisted synthesis at 65°C (green) and room temperature (blue), as well as the conventional synthesis at 65°C (purple) and room temperature (pink). No N₂-sorption isotherm was measured for the conventional method at room temperature as the resulting material was completely amorphous. Calculated PXRD patterns based on the SCXRD structure of COF-300 (Ma et al., 2018b