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U3O5P2O7 is orthorhombic, space group Cmca or C2cb(Aba2), with a = 7.018(2), b = 9.057(1), c = 16.009(3) Å, V = 1017.5(6) Å3, Z = 4, Dx = 6.318 Mg m− 3. A Nonius Guinier camera and Cu radiation (λ = 1.5418 Å) was used. Indexed powder data are given and compared with previous data. The JCPDS Diffraction File No. for U3O5P2O7 is 34-1984.
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