organic compounds
The structure of the title compound has been determined as a tetrahydrofuran solvate, C26H28N2O2SSi·C4H8O, at 193 K. This compound, which crystallizes in the monoclinic space group C2/c, is disordered. The distances between the bridgehead atoms were restrained to be 1.510 ± 0.015 Å and refined to 1.515 (11) (C1A-C5A) and 1.505 (12) Å (C1B-C5B). The trans-fusion of the system results in a rather flat geometry, with the two cyclopentane rings adopting envelope conformations.
Supporting information
Crystallographic Information File (CIF) | |
Structure factor file (CIF format) |
CCDC reference: 130666