Download citation
Download citation
link to html
The pyrrolidine ring of the title compound, C30H24N2O5, adopts a half-chair conformation. The structure is stabilized by C—H...O intramolecular interactions and the packing of the mol­ecules is stabilized by C—H...O and N—H...O intermolecular interactions.

Supporting information

cif

Crystallographic Information File (CIF) https://doi.org/10.1107/S160053680302302X/bt6365sup1.cif
Contains datablocks I, global

hkl

Structure factor file (CIF format) https://doi.org/10.1107/S160053680302302X/bt6365Isup2.hkl
Contains datablock I

CCDC reference: 227007

Key indicators

  • Single-crystal X-ray study
  • T = 293 K
  • Mean [sigma](C-C) = 0.002 Å
  • R factor = 0.049
  • wR factor = 0.139
  • Data-to-parameter ratio = 16.6

checkCIF/PLATON results

No syntax errors found



Alert level A PLAT029_ALERT_3_A _diffrn_measured_fraction_theta_full Low ....... 0.95
Alert level C ABSTY02_ALERT_1_C An _exptl_absorpt_correction_type has been given without a literature citation. This should be contained in the _exptl_absorpt_process_details field. Absorption correction given as multi-scan REFLT03_ALERT_3_C Reflection count < 95% complete From the CIF: _diffrn_reflns_theta_max 27.99 From the CIF: _diffrn_reflns_theta_full 0.00 From the CIF: _reflns_number_total 5528 TEST2: Reflns within _diffrn_reflns_theta_max Count of symmetry unique reflns 5828 Completeness (_total/calc) 94.85% PLAT066_ALERT_1_C Predicted and Reported Transmissions Identical . ? PLAT241_ALERT_2_C Check High U(eq) as Compared to Neighbors .... C33
1 ALERT level A = In general: serious problem 0 ALERT level B = Potentially serious problem 4 ALERT level C = Check and explain 0 ALERT level G = General alerts; check 2 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 1 ALERT type 2 Indicator that the structure model may be wrong or deficient 2 ALERT type 3 Indicator that the structure quality may be low 0 ALERT type 4 Improvement, methodology, query or suggestion

Computing details top

Data collection: SMART (Bruker, 2001); cell refinement: SAINT (Bruker, 2001); data reduction: SAINT; program(s) used to solve structure: SHELXS97 (Sheldrick, 1997); program(s) used to refine structure: SHELXL97 (Sheldrick, 1997); molecular graphics: ORTEP-3 (Farrugia, 1997) and PLATON (Spek, 1990); software used to prepare material for publication: SHELXL97 and PARST (Nardelli, 1995).

2'-(p-Methoxybenzoyl)-1',2,2',3,5',6',7',7a'-octahydro-1H-indan-2-spiro-3'- (3'H-pyrrolizine)-1'-spiro-3''-1H-indoline-1,2'',3-trione top
Crystal data top
C30H24N2O5F(000) = 1032
Mr = 492.51Dx = 1.352 Mg m3
Monoclinic, P21/cMo Kα radiation, λ = 0.71073 Å
Hall symbol: -P 2ybcCell parameters from 3592 reflections
a = 11.4931 (8) Åθ = 2.3–26°
b = 13.6374 (9) ŵ = 0.09 mm1
c = 15.5377 (10) ÅT = 293 K
β = 96.351 (1)°Prisms, yellow
V = 2420.4 (3) Å30.23 × 0.20 × 0.17 mm
Z = 4
Data collection top
CCD Area Detector
diffractometer
5528 independent reflections
Radiation source: fine-focus sealed tube3764 reflections with I > 2σ(I)
Graphite monochromatorRint = 0.027
ω scansθmax = 28.0°, θmin = 1.8°
Absorption correction: multi-scanh = 1414
Tmin = 0.979, Tmax = 0.984k = 1717
14548 measured reflectionsl = 2013
Refinement top
Refinement on F2Primary atom site location: structure-invariant direct methods
Least-squares matrix: fullSecondary atom site location: difference Fourier map
R[F2 > 2σ(F2)] = 0.049Hydrogen site location: inferred from neighbouring sites
wR(F2) = 0.139H-atom parameters constrained
S = 1.00 w = 1/[σ2(Fo2) + (0.0798P)2 + 0.041P]
where P = (Fo2 + 2Fc2)/3
5528 reflections(Δ/σ)max = 0.001
334 parametersΔρmax = 0.27 e Å3
0 restraintsΔρmin = 0.16 e Å3
Special details top

Geometry. All e.s.d.'s (except the e.s.d. in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell e.s.d.'s are taken into account individually in the estimation of e.s.d.'s in distances, angles and torsion angles; correlations between e.s.d.'s in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell e.s.d.'s is used for estimating e.s.d.'s involving l.s. planes.

Refinement. Refinement of F2 against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F2, conventional R-factors R are based on F, with F set to zero for negative F2. The threshold expression of F2 > σ(F2) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F2 are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger.

Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å2) top
xyzUiso*/Ueq
N10.34651 (13)0.45085 (11)0.02912 (10)0.0450 (4)
H10.38180.50290.04380.054*
C20.39982 (15)0.37685 (12)0.01661 (10)0.0354 (4)
O30.50239 (10)0.37660 (9)0.04859 (8)0.0421 (3)
C40.31036 (14)0.29370 (12)0.02195 (10)0.0343 (4)
C50.19908 (14)0.34145 (13)0.01848 (10)0.0368 (4)
C60.08488 (16)0.30866 (14)0.03079 (12)0.0468 (5)
H60.06520.24730.01070.056*
C70.00001 (17)0.36872 (16)0.07364 (14)0.0588 (6)
H70.07740.34770.08170.071*
C80.02888 (19)0.45914 (17)0.10443 (14)0.0636 (6)
H80.02930.49840.13300.076*
C90.14330 (19)0.49249 (16)0.09349 (13)0.0584 (5)
H90.16310.55320.11490.070*
C100.22643 (16)0.43324 (13)0.05017 (11)0.0425 (4)
C110.31411 (14)0.25104 (11)0.11563 (10)0.0316 (4)
H110.38770.27420.14690.038*
C120.21902 (14)0.27534 (12)0.17327 (11)0.0359 (4)
O130.15552 (13)0.20928 (10)0.19249 (10)0.0604 (4)
C140.21215 (13)0.37325 (11)0.21284 (10)0.0332 (4)
C150.28086 (15)0.45256 (13)0.19315 (12)0.0421 (4)
H150.33200.44550.15120.051*
C160.27441 (16)0.54110 (13)0.23467 (12)0.0457 (4)
H160.31940.59370.21960.055*
C170.20125 (14)0.55203 (12)0.29868 (11)0.0380 (4)
C180.13261 (16)0.47423 (13)0.31983 (11)0.0429 (4)
H180.08310.48110.36290.051*
C190.13832 (15)0.38662 (13)0.27653 (11)0.0411 (4)
H190.09120.33480.29050.049*
C200.32788 (14)0.13979 (11)0.10581 (10)0.0329 (4)
C210.21731 (14)0.07491 (12)0.08790 (11)0.0360 (4)
O220.13732 (11)0.08654 (9)0.03124 (8)0.0484 (3)
C230.23388 (15)0.01185 (12)0.14532 (11)0.0376 (4)
C240.16536 (17)0.09573 (13)0.14597 (12)0.0469 (5)
H240.09730.10280.10810.056*
C250.2021 (2)0.16837 (14)0.20501 (14)0.0564 (5)
H250.15760.22520.20700.068*
C260.3031 (2)0.15828 (15)0.26099 (14)0.0583 (6)
H260.32630.20900.29910.070*
C270.37036 (18)0.07499 (14)0.26171 (12)0.0498 (5)
H270.43760.06790.30040.060*
C280.33427 (15)0.00196 (12)0.20270 (11)0.0381 (4)
C290.39017 (15)0.09307 (12)0.18893 (11)0.0370 (4)
O300.46823 (11)0.13134 (9)0.23561 (8)0.0508 (3)
N310.39098 (12)0.12556 (10)0.03008 (9)0.0372 (3)
C320.51955 (15)0.13827 (14)0.04253 (12)0.0462 (5)
H32A0.55850.07730.06050.055*
H32B0.54210.18840.08540.055*
C330.54875 (19)0.1692 (2)0.04613 (15)0.0671 (6)
H33A0.57590.11340.07700.081*
H33B0.60980.21870.04080.081*
C340.43745 (18)0.21049 (15)0.09419 (12)0.0519 (5)
H34A0.41560.17400.14710.062*
H34B0.44790.27880.10880.062*
C350.34382 (15)0.19991 (12)0.03212 (11)0.0386 (4)
H350.27230.17420.06450.046*
O360.20315 (12)0.64125 (9)0.33735 (9)0.0537 (4)
C370.1288 (2)0.65794 (18)0.40243 (16)0.0761 (7)
H37A0.13930.72380.42370.114*
H37B0.14770.61260.44920.114*
H37C0.04880.64870.37870.114*
Atomic displacement parameters (Å2) top
U11U22U33U12U13U23
N10.0444 (9)0.0412 (8)0.0488 (9)0.0065 (7)0.0024 (7)0.0145 (7)
C20.0377 (9)0.0396 (9)0.0291 (9)0.0039 (7)0.0046 (7)0.0014 (7)
O30.0357 (7)0.0460 (7)0.0434 (7)0.0077 (5)0.0009 (5)0.0029 (5)
C40.0328 (8)0.0374 (9)0.0320 (9)0.0033 (7)0.0000 (7)0.0012 (7)
C50.0350 (9)0.0433 (10)0.0310 (9)0.0006 (7)0.0009 (7)0.0035 (7)
C60.0398 (10)0.0505 (11)0.0480 (11)0.0027 (8)0.0045 (8)0.0040 (8)
C70.0387 (11)0.0724 (15)0.0617 (14)0.0015 (10)0.0110 (9)0.0063 (11)
C80.0519 (12)0.0739 (15)0.0613 (14)0.0150 (11)0.0104 (10)0.0178 (11)
C90.0603 (13)0.0548 (12)0.0581 (13)0.0057 (10)0.0020 (10)0.0231 (10)
C100.0427 (10)0.0480 (10)0.0363 (10)0.0004 (8)0.0019 (8)0.0090 (8)
C110.0317 (8)0.0321 (8)0.0301 (8)0.0010 (7)0.0008 (6)0.0020 (6)
C120.0354 (9)0.0375 (9)0.0344 (9)0.0012 (7)0.0025 (7)0.0039 (7)
O130.0691 (9)0.0436 (8)0.0750 (10)0.0146 (7)0.0365 (8)0.0077 (7)
C140.0299 (8)0.0361 (9)0.0328 (9)0.0031 (7)0.0001 (7)0.0030 (7)
C150.0386 (9)0.0427 (10)0.0475 (11)0.0019 (8)0.0163 (8)0.0030 (8)
C160.0446 (10)0.0382 (10)0.0566 (12)0.0074 (8)0.0163 (9)0.0021 (8)
C170.0374 (9)0.0363 (9)0.0400 (10)0.0033 (7)0.0032 (7)0.0007 (7)
C180.0459 (10)0.0444 (10)0.0409 (10)0.0010 (8)0.0162 (8)0.0010 (8)
C190.0439 (10)0.0399 (10)0.0410 (10)0.0033 (8)0.0113 (8)0.0050 (7)
C200.0340 (8)0.0326 (8)0.0314 (9)0.0004 (7)0.0004 (7)0.0013 (6)
C210.0360 (9)0.0350 (9)0.0373 (9)0.0016 (7)0.0053 (7)0.0048 (7)
O220.0438 (7)0.0473 (7)0.0508 (8)0.0050 (6)0.0092 (6)0.0029 (6)
C230.0427 (9)0.0358 (9)0.0359 (9)0.0025 (7)0.0116 (7)0.0013 (7)
C240.0497 (11)0.0401 (10)0.0527 (12)0.0025 (8)0.0143 (9)0.0027 (8)
C250.0717 (14)0.0383 (10)0.0625 (14)0.0058 (10)0.0217 (11)0.0047 (9)
C260.0769 (15)0.0450 (11)0.0550 (13)0.0085 (10)0.0155 (11)0.0150 (9)
C270.0611 (12)0.0469 (11)0.0414 (11)0.0073 (9)0.0056 (9)0.0085 (8)
C280.0448 (10)0.0374 (9)0.0328 (9)0.0052 (7)0.0076 (7)0.0001 (7)
C290.0388 (9)0.0385 (9)0.0336 (9)0.0075 (7)0.0029 (7)0.0019 (7)
O300.0517 (8)0.0494 (8)0.0468 (8)0.0001 (6)0.0141 (6)0.0031 (6)
N310.0382 (8)0.0392 (8)0.0340 (8)0.0025 (6)0.0034 (6)0.0030 (6)
C320.0373 (10)0.0506 (11)0.0509 (12)0.0064 (8)0.0062 (8)0.0044 (8)
C330.0545 (13)0.0885 (17)0.0619 (14)0.0093 (12)0.0224 (11)0.0015 (12)
C340.0619 (13)0.0592 (12)0.0365 (10)0.0023 (10)0.0133 (9)0.0058 (9)
C350.0425 (10)0.0408 (10)0.0315 (9)0.0030 (7)0.0003 (7)0.0020 (7)
O360.0604 (9)0.0410 (7)0.0630 (9)0.0026 (6)0.0217 (7)0.0120 (6)
C370.0943 (19)0.0598 (14)0.0815 (17)0.0012 (13)0.0424 (15)0.0217 (12)
Geometric parameters (Å, º) top
N1—C21.342 (2)C20—N311.462 (2)
N1—C101.403 (2)C20—C291.543 (2)
N1—H10.8600C20—C211.548 (2)
C2—O31.228 (2)C21—O221.211 (2)
C2—C41.539 (2)C21—C231.481 (2)
C4—C51.509 (2)C23—C281.385 (2)
C4—C111.564 (2)C23—C241.389 (2)
C4—C351.600 (2)C24—C251.384 (3)
C5—C61.380 (2)C24—H240.9300
C5—C101.394 (2)C25—C261.379 (3)
C6—H60.9300C25—H250.9300
C7—C61.386 (3)C26—C271.373 (3)
C7—H70.9300C26—H260.9300
C8—C71.377 (3)C27—C281.386 (2)
C8—H80.9300C27—H270.9300
C9—C81.384 (3)C28—C291.473 (2)
C9—H90.9300C29—O301.208 (2)
C10—C91.370 (3)N31—C351.463 (2)
C11—C121.524 (2)N31—C321.479 (2)
C11—C201.535 (2)C32—C331.514 (3)
C11—H110.9800C32—H32A0.9700
C12—O131.217 (2)C32—H32B0.9700
C12—C141.476 (2)C33—C341.516 (3)
C14—C191.385 (2)C33—H33A0.9700
C14—C151.393 (2)C33—H33B0.9700
C15—C161.375 (2)C34—C351.529 (2)
C15—H150.9300C34—H34A0.9700
C16—C171.380 (2)C34—H34B0.9700
C16—H160.9300C35—H350.9800
C17—O361.356 (2)O36—C371.413 (2)
C17—C181.383 (2)C37—H37A0.9600
C18—C191.376 (2)C37—H37B0.9600
C18—H180.9300C37—H37C0.9600
C19—H190.9300
C2—N1—C10112.0 (1)C11—C20—C21119.42 (13)
C2—N1—H1124.0C29—C20—C21102.12 (13)
C10—N1—H1124.0O22—C21—C23125.4 (2)
O3—C2—N1125.31 (15)O22—C21—C20126.7 (2)
O3—C2—C4126.4 (2)C23—C21—C20107.45 (14)
N1—C2—C4108.3 (1)C28—C23—C24120.54 (16)
C5—C4—C2101.55 (13)C28—C23—C21110.64 (15)
C5—C4—C11118.88 (13)C24—C23—C21128.81 (17)
C2—C4—C11112.00 (13)C25—C24—C23117.56 (19)
C5—C4—C35111.60 (13)C25—C24—H24121.2
C2—C4—C35111.09 (13)C23—C24—H24121.2
C11—C4—C35101.99 (12)C26—C25—C24121.36 (19)
C6—C5—C10119.36 (16)C26—C25—H25119.3
C6—C5—C4131.87 (16)C24—C25—H25119.3
C10—C5—C4108.71 (15)C27—C26—C25121.45 (19)
C5—C6—C7118.89 (18)C27—C26—H26119.3
C5—C6—H6120.6C25—C26—H26119.3
C7—C6—H6120.6C26—C27—C28117.53 (19)
C8—C7—C6120.81 (19)C26—C27—H27121.2
C8—C7—H7119.6C28—C27—H27121.2
C6—C7—H7119.6C23—C28—C27121.54 (17)
C7—C8—C9120.93 (18)C23—C28—C29109.76 (14)
C7—C8—H8119.5C27—C28—C29128.70 (17)
C9—C8—H8119.5O30—C29—C28126.9 (2)
C10—C9—C8117.91 (19)O30—C29—C20124.7 (2)
C10—C9—H9121.0C28—C29—C20108.39 (14)
C8—C9—H9121.0C20—N31—C35105.0 (1)
C9—C10—C5122.08 (18)C20—N31—C32117.2 (1)
C9—C10—N1128.9 (2)C35—N31—C32107.27 (13)
C5—C10—N1109.01 (15)N31—C32—C33103.5 (2)
C12—C11—C20111.22 (13)N31—C32—H32A111.1
C12—C11—C4121.22 (13)C33—C32—H32A111.1
C20—C11—C4105.53 (12)N31—C32—H32B111.1
C12—C11—H11105.9C33—C32—H32B111.1
C20—C11—H11105.9H32A—C32—H32B109.0
C4—C11—H11105.9C32—C33—C34106.96 (15)
O13—C12—C14120.4 (2)C32—C33—H33A110.3
O13—C12—C11118.1 (2)C34—C33—H33A110.3
C14—C12—C11121.09 (14)C32—C33—H33B110.3
C19—C14—C15117.50 (15)C34—C33—H33B110.3
C19—C14—C12118.81 (15)H33A—C33—H33B108.6
C15—C14—C12123.59 (15)C33—C34—C35105.58 (16)
C16—C15—C14121.17 (16)C33—C34—H34A110.6
C16—C15—H15119.4C35—C34—H34A110.6
C14—C15—H15119.4C33—C34—H34B110.6
C15—C16—C17120.13 (16)C35—C34—H34B110.6
C15—C16—H16119.9H34A—C34—H34B108.8
C17—C16—H16119.9N31—C35—C34104.3 (1)
O36—C17—C16115.8 (2)N31—C35—C4107.5 (1)
O36—C17—C18124.4 (2)C34—C35—C4118.84 (14)
C16—C17—C18119.84 (16)N31—C35—H35108.6
C19—C18—C17119.36 (16)C34—C35—H35108.6
C19—C18—H18120.3C4—C35—H35108.6
C17—C18—H18120.3C17—O36—C37118.7 (2)
C18—C19—C14121.98 (16)O36—C37—H37A109.5
C18—C19—H19119.0O36—C37—H37B109.5
C14—C19—H19119.0H37A—C37—H37B109.5
N31—C20—C11106.09 (13)O36—C37—H37C109.5
N31—C20—C29113.2 (1)H37A—C37—H37C109.5
C11—C20—C29111.61 (13)H37B—C37—H37C109.5
N31—C20—C21104.5 (1)
C10—N1—C2—O3174.39 (16)C4—C11—C20—C2188.38 (16)
C10—N1—C2—C45.41 (19)N31—C20—C21—O2266.2 (2)
O3—C2—C4—C5173.03 (16)C11—C20—C21—O2252.1 (2)
N1—C2—C4—C56.76 (17)C29—C20—C21—O22175.68 (16)
O3—C2—C4—C1145.1 (2)N31—C20—C21—C23106.45 (14)
N1—C2—C4—C11134.66 (14)C11—C20—C21—C23135.25 (14)
O3—C2—C4—C3568.2 (2)C29—C20—C21—C2311.64 (16)
N1—C2—C4—C35112.02 (15)O22—C21—C23—C28179.77 (16)
C2—C4—C5—C6177.01 (18)C20—C21—C23—C286.97 (18)
C11—C4—C5—C653.7 (3)O22—C21—C23—C241.0 (3)
C35—C4—C5—C664.6 (2)C20—C21—C23—C24171.84 (17)
C2—C4—C5—C105.87 (18)C28—C23—C24—C250.7 (3)
C11—C4—C5—C10129.18 (16)C21—C23—C24—C25178.01 (17)
C35—C4—C5—C10112.55 (16)C23—C24—C25—C260.3 (3)
C6—C5—C10—C90.1 (3)C24—C25—C26—C271.3 (3)
C4—C5—C10—C9177.49 (18)C25—C26—C27—C281.3 (3)
C6—C5—C10—N1179.31 (16)C24—C23—C28—C270.6 (3)
C4—C5—C10—N13.1 (2)C21—C23—C28—C27178.28 (15)
C2—N1—C10—C9177.8 (2)C24—C23—C28—C29179.77 (15)
C2—N1—C10—C51.5 (2)C21—C23—C28—C291.31 (19)
C5—C10—C9—C80.8 (3)C26—C27—C28—C230.4 (3)
N1—C10—C9—C8178.4 (2)C26—C27—C28—C29179.13 (18)
C10—C9—C8—C70.8 (3)C23—C28—C29—O30168.03 (17)
C9—C8—C7—C60.0 (4)C27—C28—C29—O3012.4 (3)
C10—C5—C6—C70.7 (3)C23—C28—C29—C209.14 (18)
C4—C5—C6—C7177.61 (18)C27—C28—C29—C20170.42 (17)
C8—C7—C6—C50.8 (3)N31—C20—C29—O3083.6 (2)
C5—C4—C11—C1213.1 (2)C11—C20—C29—O3036.0 (2)
C2—C4—C11—C12104.92 (16)C21—C20—C29—O30164.72 (16)
C35—C4—C11—C12136.24 (15)N31—C20—C29—C2899.18 (15)
C5—C4—C11—C20114.35 (15)C11—C20—C29—C28141.23 (13)
C2—C4—C11—C20127.66 (14)C21—C20—C29—C2812.52 (16)
C35—C4—C11—C208.81 (15)C11—C20—N31—C3538.52 (15)
C20—C11—C12—O1311.1 (2)C29—C20—N31—C35161.22 (13)
C4—C11—C12—O13113.75 (18)C21—C20—N31—C3588.52 (14)
C20—C11—C12—C14162.14 (14)C11—C20—N31—C3280.38 (17)
C4—C11—C12—C1473.0 (2)C29—C20—N31—C3242.32 (19)
O13—C12—C14—C194.5 (2)C21—C20—N31—C32152.58 (14)
C11—C12—C14—C19168.55 (15)C20—N31—C32—C33152.71 (16)
O13—C12—C14—C15179.13 (17)C35—N31—C32—C3335.03 (19)
C11—C12—C14—C157.8 (2)N31—C32—C33—C3421.6 (2)
C19—C14—C15—C160.8 (3)C32—C33—C34—C351.4 (2)
C12—C14—C15—C16177.21 (16)C20—N31—C35—C34159.65 (13)
C14—C15—C16—C171.7 (3)C32—N31—C35—C3434.30 (17)
C15—C16—C17—O36178.37 (16)C20—N31—C35—C432.63 (16)
C15—C16—C17—C181.3 (3)C32—N31—C35—C492.72 (15)
O36—C17—C18—C19179.61 (16)C33—C34—C35—N3119.6 (2)
C16—C17—C18—C190.0 (3)C33—C34—C35—C4100.03 (19)
C17—C18—C19—C140.9 (3)C5—C4—C35—N31141.98 (14)
C15—C14—C19—C180.5 (3)C2—C4—C35—N31105.47 (15)
C12—C14—C19—C18176.09 (16)C11—C4—C35—N3114.02 (16)
C12—C11—C20—N31162.32 (13)C5—C4—C35—C34100.06 (18)
C4—C11—C20—N3129.09 (15)C2—C4—C35—C3412.5 (2)
C12—C11—C20—C2974.00 (17)C11—C4—C35—C34131.98 (16)
C4—C11—C20—C29152.76 (13)C16—C17—O36—C37178.91 (19)
C12—C11—C20—C2144.86 (19)C18—C17—O36—C371.5 (3)
Hydrogen-bond geometry (Å, º) top
D—H···AD—HH···AD···AD—H···A
N1—H1···O3i0.862.122.960 (2)165
C6—H6···O220.932.413.215 (2)145
C11—H11···O30.982.543.033 (2)111
C11—H11···O300.982.502.924 (2)106
C16—H16···O300.932.523.190 (2)130
C26—H26···O360.932.593.241 (2)127
C27—H27···O30.932.493.211 (2)134
C35—H35···O220.982.563.084 (2)113
Symmetry code: (i) x+1, y+1, z.
 

Follow Acta Cryst. E
Sign up for e-alerts
Follow Acta Cryst. on Twitter
Follow us on facebook
Sign up for RSS feeds