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The reaction of Rb2S3, NbO and S yields single crystals of trirubidium tetrathioniobate, Rb3NbS4. The crystal structure is based on discrete tetrahedral NbS4 anions, which are connected via Rb cations. The compound crystallizes with the K3VS4 structure type and is isotypic with previously reported K and Cs analogues.

Supporting information


Crystallographic Information File (CIF)
Contains datablocks ok16, global


Structure factor file (SHELXL table format)
Supplementary material

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