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Crystal structure analysis establishes the configuration of one of two isomers of the thermal dimerization of N-[3-(1,2,2-trifluoroethenyl)-4-phenoxyphenyl]phthalimide to be trans-5,5'-[1,2,3,3,4,4-hexafluorocyclobutane-1,2-diylbis(2-phenoxyphenyl)]-N,N'-bis(phthalimide), C44H24F6N2O6. The cyclobutane ring puckers and has a dihedral angle of 23.5 (4)°. The crystal also contains a diethyl ether molecule of solvation, C4H10O.

Supporting information

cif

Crystallographic Information File (CIF)
Contains datablocks global, bur23

hkl

Structure factor file (CIF format)
Contains datablock bur21

CCDC reference: 129215

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