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Figure 2
X-ray data statistics as a function of resolution and data-collection time. The plots indicate that the quality of the data set has been limited by the small crystal volume exposed to X-ray radiation, reflected by moderate I/σ statistics. I/σ values and R-merge as output by the program SCALEPACK (Otkinowski, 1993BB9). (a) I/σ and (b) R-merge in resolution bins; (c) scale factor (thin line) and temperature factor (in bold, dimension in Å2) as a function of frame number. The data set consists of 68110 unique reflections in the range 20.0–1.85 Å resolution with a redundancy of 8.9 and overall completeness of 98.2%. For further details on the data collection, see Mayans et al. (1998BB8).

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