Figure 1
General view of the TRXRD experimental set-up: XRD and IR coupled devices. (1) X-ray fast detector (using 30° 2θ and 17° 2θ). (2) Reaction chamber under controlled He atmosphere. (3) Tungsten heating elements. (4) Mylar window. (5) Synchrotron radiation, λ = 0.1825 nm (LURE DCI D43, Orsay, France). (6) IR camera. (7) Video camera. (8) Sample. |