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Figure 3
(a) Rietveld refinement of the ninth vertical strip of the imaging plate, corresponding to about 8 min of catalyst treatment at 773 K (λ = 0.72384 Å). Upper tick marks: tetragonal phase. Lower tick marks: cubic phase. The amorphous halo at 10° 2θ is due to the capillary scattering. (b) Enlargement of the 20–25° 2θ interval, demonstrating the presence of two phases.

Journal logoJOURNAL OF
SYNCHROTRON
RADIATION
ISSN: 1600-5775
Volume 10| Part 2| March 2003| Pages 177-182
https://doi.org/10.1107/S0909049502019167
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