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Figure 1
The experimental apparatus consisted of an FPLC system coupled to a home-made SAXS cell made from a quartz capillary and a block of aluminium, (a). The configuration, shown in schematic in (b), was such that the sample was passed over a molecular sieve column and monitored by UV absorption immediately before it was passed through the X-ray beam. Scattered photons were then detected by a phosphor-coupled CCD camera placed behind an evacuated 2 m flight tube.

Journal logoJOURNAL OF
SYNCHROTRON
RADIATION
ISSN: 1600-5775
Volume 11| Part 4| June 2004| Pages 314-318
doi:10.1107/S0909049504014086
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